CN108991597A - A kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle - Google Patents
A kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle Download PDFInfo
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- CN108991597A CN108991597A CN201810515890.8A CN201810515890A CN108991597A CN 108991597 A CN108991597 A CN 108991597A CN 201810515890 A CN201810515890 A CN 201810515890A CN 108991597 A CN108991597 A CN 108991597A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
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- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
A kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle, includes the following steps: the preparation of S1, raw material Chinese herbal medicine and strain；S2, inoculation；S3, fermentation: carrying out ferment at constant temperature, and the fermentation temperature is 30 DEG C -35 DEG C, and fermentation time is -72h for 24 hours, obtains tunning；S4, dries pulverizing: by the weight content that tunning is dried to moisture it is 8%-10% at being 30 DEG C -80 DEG C in drying temperature, is then crushed to -80 mesh of 10 mesh, obtains filling product；S5, composite filter preparation: glyceride will be sprayed after the abundant shredding of the tow of acetate fiber, then the filling product that S4 is obtained is sprayed on tow, then wrapped up with forming paper and composite filter is made.The present invention carries out fermentation process to Chinese herbal medicine using microorganism, and particle is then made and is evenly distributed in filter stick, will not generate air flow resistance, has the function that drop evil by the double action of Chinese herbal medicine and microorganism.
Description
Technical field:
The present invention relates to a kind of preparation methods of fermentation of Chinese herbal medicine binary compound filter candle.
Background technique:
Carcinogenic components in cigarette smoke are present in tar more, therefore tar content is considered as the weight of cigarette harmfulness size
Want index.With the continuous improvement of living standards, people's health consciousness is constantly promoted, and the pressure that tobacco business faces is increasingly
Greatly, how in reducing cigarette tar and while other harmful components, and be able to satisfy requirement of the consumer to cigarette odor-absorbing at
The problem of to be concerned.Cigarette filter rod plays very important effect in the design of reducing tar and reducing harm, can effectively retain
Granule phase substance matter in flue gas reduces the tar content of human body intake.A main composition of the cellulose acetate filter rod as cigarette material
Part has obtained universal application, but practices and find that its filter effect is not highly desirable.In order to enhance cellulose acetate filter rod
Absorption property mostly uses add the tobaccos such as inorganic substances or offal, expanded cabo, expanded cut tobacco such as active carbon in filter stick at present
Particle etc. increases the effect of filter stick adsorption capacity using these complex solid particles.But according to the viewpoint of cigarette fragrance field, volume
For the fragrance matter of cigarette also in tar, the content for reducing tar and nicotine means that the taste for reducing tobacco, is difficult simultaneously
The two is taken into account.Therefore needing to develop one kind can be in the fragrance and taste that guarantee cigarette and the filter tip for mitigating harm to the human body.
Developed the filter stick containing Chinese herbal medicine particle at present, but grain graininess size and active constituent use aspects there is also
Problem.If Chinese herbal medicine granularity is meticulous, facilitate the release of active constituent, but filter stick can generate very big retardance to flue gas.Such as
The excessively thick then effect of fruit granule is bad, and since cigarette suction time is shorter, is difficult to excite the active constituent of Chinese herbal medicine
Out.There is no the plans of solution to this for the prior art.
Summary of the invention:
The present invention provides a kind of preparation methods of fermentation of Chinese herbal medicine binary compound filter candle, and it is living can to greatly improve Chinese herbal medicine
The release of property, solves problems of the prior art.
Used technical solution is the present invention to solve above-mentioned technical problem:
A kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle, includes the following steps:
The preparation of S1, raw material Chinese herbal medicine and strain:
The raw material Chinese herbal medicine includes rhizoma polygonati, American Ginseng, tendril-leaved fritillary bulb, the root of straight ladybell, lily, dendrobium nobile, radix polygonati officinalis, Radix Glycyrrhizae, winter wheat, campanulaceae
At least one of, the parts by weight of above-mentioned each raw material Chinese herbal medicine component are as follows: 0-15 parts of rhizoma polygonati, 0-15 parts of American Ginseng, river
0-15 parts of shellfish, 0-15 parts of the root of straight ladybell, 0-20 parts of lily, 0-20 parts of dendrobium nobile, 0-20 parts of radix polygonati officinalis, 0-30 parts of Radix Glycyrrhizae, 0-30 parts of winter wheat, tangerine
0-30 parts of stalk；
The strain includes lactobacillus plantarum, lactobacillus acidophilus, bifidobacterium longum, bacillus licheniformis, condensation gemma bar
Bacterium, candida utili, saccharomyces cerevisiae at least one, above-mentioned each strain component is as follows according to the number of viable bacteria amount: plant
0-40 parts of lactobacillus, 0-40 parts of lactobacillus acidophilus, 0-40 parts of bifidobacterium longum, 0-30 parts of bacillus licheniformis, condensation gemma bar
0-30 parts of bacterium, 0-10 parts of candida utili, 0-10 parts of saccharomyces cerevisiae；
S2, inoculation: the sugar of adding raw materials Chinese herbal medicine quality 3%-10% obtains raw material base in herbal medicine in the feed, by raw material
Base is uniformly mixed, and the strain that 5%vol-15%vol is then put into raw material base obtains fermentation base, and fermentation base is uniformly mixed；
S3, fermentation: carrying out ferment at constant temperature, and the fermentation temperature is 30 DEG C -35 DEG C, and fermentation time is -72h for 24 hours, is sent out
Ferment product；
S4, dries pulverizing: it is by the weight content that tunning is dried to moisture at being 30 DEG C -80 DEG C in drying temperature
Then 8%-10% is crushed to -80 mesh of 10 mesh, obtains filling product；
S5, composite filter preparation: glyceride will be sprayed after the abundant shredding of the tow of acetate fiber, is then filled out what S4 was obtained
It fills product to be sprayed on tow, is then wrapped up with forming paper and composite filter is made.
Preferably, in S1, the final viable bacteria amount of the strain is 0.1-10 × 108cfu/g。
Preferably, in S2, the sugar is glucose and/or maltose and/or lactose and/or sucrose and/or fructose.
Preferably, in S2, fermentation base after mixing is added to 30 DEG C -35 DEG C of warm water, adjusts the water of fermentation base
Part mass fraction is to 30%-50%.
Preferably, in S1, the raw material Chinese herbal medicine is to handle by removal of impurities, and individually crushed, and partial size is 50 mesh-
200 mesh.
Preferably, in S5, in the composite filter, the mass fraction of the filling product is 1-40 parts；The matter of tow
Measure number are as follows: 60-99 parts.
Composite filter prepared by the present invention carries out fermentation process to Chinese herbal medicine using microorganism, it is uniform that particle is then made
It is distributed in filter stick, air flow resistance will not be generated, drop evil is haved the function that by the double action of Chinese herbal medicine and microorganism, simultaneously
Fermentation promotes the release of Chinese herbal medicine active constituent and the generation of microorganism beneficial metabolic product, plays the work of flavouring humectation
With being repaired to organs such as human lungs, so that the function of filter stick be substantially improved.
Specific embodiment:
In order to clarify the technical characteristics of the invention, being explained in detail below by specific embodiment the present invention
It states.
Prepare embodiment 1:
The preparation of S1, raw material Chinese herbal medicine and strain:
The quality of the component of each raw material Chinese herbal medicine is as follows: 8 kilograms of rhizoma polygonati, 8 kilograms of American Ginseng, 8 kilograms of tendril-leaved fritillary bulb, the root of straight ladybell 8
Kilogram, 10 kilograms of lily, 10 kilograms of dendrobium nobile, 10 kilograms of radix polygonati officinalis, 15 kilograms of Radix Glycyrrhizae, 15 kilograms of winter wheat, 15 kilograms of campanulaceae；The original
Material Chinese herbal medicine is to handle by removal of impurities, and individually crushed, and partial size is -100 mesh of 50 mesh；
The number according to viable bacteria amount of each strain component is as follows: 20 parts of lactobacillus plantarum, 20 parts of lactobacillus acidophilus, long pair
20 parts of discrimination bacillus, 15 parts of bacillus licheniformis, 15 parts of bacillus coagulans, 5 parts of candida utili, 5 parts of saccharomyces cerevisiae, it is described
The final viable bacteria amount of strain is 5 × 108cfu/g；
S2, inoculation: the sugar of adding raw materials Chinese herbal medicine quality 5.5% obtains raw material base in herbal medicine in the feed, and the sugar is
Glucose, maltose, lactose, sucrose, fructose respectively account for 20%, and raw material base is uniformly mixed, and are then put into 10% into raw material base
Strain (volume) obtain fermentation base, fermentation base is uniformly mixed, 33 DEG C of warm water is added in fermentation base after mixing, is adjusted
The moisture content mass fraction of section fermentation base is to 40%；
S3, fermentation: carrying out ferment at constant temperature, and the fermentation temperature is 31 DEG C, and fermentation time 48h obtains tunning；
S4, dries pulverizing: by the weight content that tunning is dried to moisture being 9% at being 55 DEG C in drying temperature, so
After be crushed to -50 mesh of 10 mesh, obtain filling product；
S5, composite filter preparation: glyceride will be sprayed after the abundant shredding of the tow of acetate fiber, is then filled out what S4 was obtained
It fills product to be sprayed on tow, is then wrapped up with forming paper and composite filter, in composite filter, the filling product and silk is made
The mass ratio of beam is 20:80, and gained composite filter is No. 1 filter stick.
Prepare embodiment 2:
The preparation of S1, raw material Chinese herbal medicine and strain:
The quality of the component of each raw material Chinese herbal medicine is as follows: 15 kilograms of rhizoma polygonati, 15 kilograms of American Ginseng, 15 kilograms of tendril-leaved fritillary bulb, sand
Join 15 kilograms, 20 kilograms of lily, 20 kilograms of dendrobium nobile, 10 kilograms of radix polygonati officinalis, 30 kilograms of Radix Glycyrrhizae, 30 kilograms of winter wheat, 30 kilograms of campanulaceae；Institute
Stating raw material Chinese herbal medicine is to handle by removal of impurities, and individually crushed, and partial size is -200 mesh of 100 mesh；
The number according to viable bacteria amount of each strain component is as follows: 40 parts of lactobacillus plantarum, 40 parts of lactobacillus acidophilus, long pair
40 parts of discrimination bacillus, 30 parts of bacillus licheniformis, 30 parts of bacillus coagulans, 10 parts of candida utili, 10 parts of saccharomyces cerevisiae, institute
The final viable bacteria amount for stating strain is 10 × 108cfu/g；
S2, inoculation: the sugar of adding raw materials Chinese herbal medicine quality 10% obtains raw material base in herbal medicine in the feed, and the sugar is Portugal
Grape sugar, raw material base is uniformly mixed, and the strain (volume) that 15% is then put into raw material base obtains fermentation base, and fermentation base is mixed
It closes uniformly, 35 DEG C of warm water is added in fermentation base after mixing, adjust the moisture content mass fraction of fermentation base to 50%；
S3, fermentation: carrying out ferment at constant temperature, and the fermentation temperature is 35 DEG C, and fermentation time is for 24 hours, to obtain tunning；
S4, dries pulverizing: by the weight content that tunning is dried to moisture being 10% at being 80 DEG C in drying temperature, so
After be crushed to -80 mesh of 50 mesh, obtain filling product；
S5, composite filter preparation: glyceride will be sprayed after the abundant shredding of the tow of acetate fiber, is then filled out what S4 was obtained
It fills product to be sprayed on tow, is then wrapped up with forming paper and composite filter, in composite filter, the filling product and silk is made
The mass ratio of beam is 40:60, and gained composite filter is No. 2 filter sticks.
Prepare embodiment 3:
The preparation of S1, raw material Chinese herbal medicine and strain:
The quality of the component of the raw material Chinese herbal medicine is as follows: 15 kilograms of rhizoma polygonati, 15 kilograms of American Ginseng, 15 kilograms of tendril-leaved fritillary bulb, sand
15 kilograms, 20 kilograms of lily of ginseng；The raw material Chinese herbal medicine is to handle by removal of impurities, and individually crushed, and partial size is 50 mesh -300
Mesh；
The number according to viable bacteria amount of each strain component is as follows: 20 parts of lactobacillus plantarum, 20 parts of lactobacillus acidophilus,
20 parts of bifidobacterium longum, 15 parts of bacillus licheniformis, the final viable bacteria amount of the strain are 5 × 108cfu/g；
S2, inoculation: the sugar of adding raw materials Chinese herbal medicine quality 1%-10% obtains raw material base, the sugar in herbal medicine in the feed
50% is respectively accounted for for maltose, lactose, raw material base is uniformly mixed, 12% strain (volume) is then put into raw material base and is obtained
Ferment base, and fermentation base is uniformly mixed, and fermentation base after mixing is added to 32 DEG C of warm water, adjusts the moisture content matter of fermentation base
Score is measured to 40%；
S3, fermentation: carrying out ferment at constant temperature, and the fermentation temperature is 30 DEG C, and fermentation time 72h obtains tunning；
S4, dries pulverizing: by the weight content that tunning is dried to moisture being 12% at being 55 DEG C in drying temperature, so
After be crushed to -80 mesh of 10 mesh, obtain filling product；
S5, composite filter preparation: glyceride will be sprayed after the abundant shredding of the tow of acetate fiber, is then filled out what S4 was obtained
It fills product to be sprayed on tow, is then wrapped up with forming paper and composite filter, in composite filter, the filling product and silk is made
The mass ratio of beam is 1:99, and gained composite filter is No. 3 filter sticks.
Prepare embodiment 4:
The preparation of S1, raw material Chinese herbal medicine and strain:
The quality of the component of each raw material Chinese herbal medicine is as follows: 10 kilograms of dendrobium nobile, 10 kilograms of radix polygonati officinalis, 15 kilograms of Radix Glycyrrhizae,
15 kilograms of winter wheat, 15 kilograms of campanulaceae；The raw material Chinese herbal medicine is to handle by removal of impurities, and individually crushed, and partial size is 50 mesh -80
Mesh；
The number according to viable bacteria amount of each strain component is as follows: 15 parts of bacillus licheniformis, bacillus coagulans
15 parts, 5 parts of candida utili, 5 parts of saccharomyces cerevisiae, the final viable bacteria amount of the strain are 5 × 108cfu/g；
S2, inoculation: the sugar of adding raw materials Chinese herbal medicine quality 5% obtains raw material base in herbal medicine in the feed, and the sugar is cream
Sugar and sucrose and fructose respectively account for 1/3, and raw material base is uniformly mixed, and the strain (volume) that 10% is then put into raw material base must
To fermentation base, fermentation base is uniformly mixed, fermentation base after mixing is added to 33 DEG C of warm water, adjusts the moisture content of fermentation base
Mass fraction is to 40%；
S3, fermentation: carrying out ferment at constant temperature, and the fermentation temperature is 32 DEG C, and fermentation time 60h obtains tunning；
S4, dries pulverizing: by the weight content that tunning is dried to moisture being 13% at being 55 DEG C in drying temperature, so
After be crushed to -80 mesh of 10 mesh, obtain filling product；
S5, composite filter preparation: glyceride will be sprayed after the abundant shredding of the tow of acetate fiber, is then filled out what S4 was obtained
It fills product to be sprayed on tow, is then wrapped up with forming paper and composite filter, in composite filter, the filling product and silk is made
The mass ratio of beam is 20:80, and gained composite filter is No. 4 filter sticks.
Comparative test: influence of the fermentation of Chinese herbal medicine filtering material to Chemical Components in Cigarette Smoke is verified by comparative test.
Test is divided into control group and test group 1, test group 2, test group 3,4 five groups of test group, control group use with examination
It tests group 1 and removes " filling product " after S2 and S3 step, 1-4 filter stick is respectively adopted in correspondence in test group 1-4.According to YC/
The industry standard methods smoking cigarette of T29-1997 " flavouring essence for tobacco volatile component total amount universal test method " collects cigarette cigarette
Gas is detected, and testing result is as shown in the table:
| Smoke components | Control group | Test group 1 | Test group 2 | Test group 3 | Test group 4 |
| Furfural | 0.946 | 2.582 | 2.456 | 1.591 | 2.597 |
| 2 methyl indole | 0.087 | 0.206 | 0.202 | 0.112 | 0.208 |
| Limonene | 0.412 | 0.996 | 0.962 | 0.576 | 0.967 |
| Methyl palmitate | 0.015 | 0.026 | 0.025 | 0.017 | 0.025 |
| 2,3- xylenol | 0.780 | 0.356 | 0.361 | 0.581 | 0.370 |
| 2,4- xylenol | 0.288 | 0.071 | 0.074 | 0.200 | 0.089 |
| 2,5- lutidines | 0.026 | 0.008 | 0.007 | 0.022 | 0.011 |
| Phytol | 0.389 | 0.143 | 0.147 | 0.257 | 0.163 |
It can be seen that the test group 3 in addition to using No. 3 filter sticks by data in table, due to the filling product contained in it
Very few, aroma component furfural, 2 methyl indole, limonene, the methyl palmitate of other filter sticks have increased separately 100% or so,
Harmful components 2,3- xylenol, 2,4- xylenol, 2,5- lutidines reduce 50% or more respectively, can produce
The phytol content of raw miscellaneous gas reduces 50 or more %.Therefore it can be shown that the product that the present invention obtains can make mainly to cause in cigarette
Fragrant ingredient dramatically increases, and harmful components are substantially reduced.
Flue gas point is carried out to above-mentioned filter stick with conventional analysis with smoking machine measuring method according to GB/T 19609-2004 cigarette
Analysis show control group and test group 1, test group 2, test group 3, test group 4 tar content be respectively 12.39mg/ branch,
9.93mg/ branch, 10.12mg/ branch, 11.12mg/ branch, 9.75mg/ branch, in addition to No. 3 filter sticks reduce about 10%, remaining group is all reduced
20% or more.
Then the said goods are met at 10 professional members of smoking to smoke panel test, test group 1, test group 2,4 cigarette of test group
It gives off a strong fragrance plentiful, has Chinese herbal medicine fragrance, nonirritant without miscellaneous gas, pleasant impression is pure comfortable when suction；3 cigarette of test group is fragrant
Gas is strong, more plentiful, has slight Chinese herbal medicine fragrance, slightly miscellaneous gas, to throat's slightly irritation, pleasant impression is purer and comfortable；It is right
Strong according to group cigarette flavor, slightly miscellaneous gas slightly has irritation to throat, and pleasant impression is neter, still comfortably.The result shows that fermentation medium-height grass
Medicine acts on more obvious than non-fermentation of Chinese herbal medicine in enhancing filter effect and in terms of increasing fragrance, and sensory experience is more preferable when suction.
To sum up, advantage of the present invention is as follows: 1, by the fermentation of microorganism, promoting releasing for active constituent in Chinese herbal medicine
It puts, reduces toxic side effect, to enhance the medicinal efficacy of Chinese herbal medicine, reduce the miscellaneous gas in flue gas, mouthfeel is sucked in promotion.
2, by the double action of Chinese herbal medicine particle and microbial cell structure, enhance absorption of the filter stick to harmful components
Performance is filtered, while reducing the usage amount of Chinese herbal medicine, is reduced costs.
3, the metabolism such as the organic acid that the fragrance and microorganism generated after Chinese herbal medicine is fermented generates during growth metabolism
The drawbacks of product plays the role of flavouring, compensates for insufficient fragrance improves the suction mouthfeel of cigarette.
4, the active constituent of Chinese herbal medicine and the beneficial metabolic product of microorganism can alleviate flue gas pair with air-flow progress lung
The irritation of throat and lung has moist and repair to lung organ, facilitates human health.
Above-mentioned specific embodiment cannot function as limiting the scope of the invention, for the technology people of the art
For member, any alternate modification or transformation made to embodiment of the present invention are fallen within the scope of protection of the present invention.
Place is not described in detail by the present invention, is the well-known technique of those skilled in the art of the present technique.
Claims (6)
1. a kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle, characterized by the following steps:
The preparation of S1, raw material Chinese herbal medicine and strain:
The raw material Chinese herbal medicine include rhizoma polygonati, American Ginseng, tendril-leaved fritillary bulb, the root of straight ladybell, lily, dendrobium nobile, radix polygonati officinalis, Radix Glycyrrhizae, winter wheat, in campanulaceae
The parts by weight of at least one, above-mentioned each raw material Chinese herbal medicine component are as follows: 0-15 parts of rhizoma polygonati, 0-15 parts of American Ginseng, tendril-leaved fritillary bulb 0-
15 parts, 0-15 parts of the root of straight ladybell, 0-20 parts of lily, 0-20 parts of dendrobium nobile, 0-20 parts of radix polygonati officinalis, 0-30 parts of Radix Glycyrrhizae, 0-30 parts of winter wheat, campanulaceae 0-
30 parts；
The strain includes lactobacillus plantarum, lactobacillus acidophilus, bifidobacterium longum, bacillus licheniformis, bacillus coagulans, production
At least one of protein Candida, saccharomyces cerevisiae, above-mentioned each strain component are as follows according to the number of viable bacteria amount: lactobacillus plantarum
0-40 parts, 0-40 parts of lactobacillus acidophilus, 0-40 parts of bifidobacterium longum, 0-30 parts of bacillus licheniformis, bacillus coagulans 0-30
Part, 0-10 parts of candida utili, 0-10 parts of saccharomyces cerevisiae；
S2, inoculation: the sugar of adding raw materials Chinese herbal medicine quality 3%-10% obtains raw material base in herbal medicine in the feed, and raw material base is mixed
Uniformly, the strain that 5%vol-15%vol is then put into raw material base obtains fermentation base for conjunction, and fermentation base is uniformly mixed；
S3, fermentation: carrying out ferment at constant temperature, and the fermentation temperature is 30 DEG C -35 DEG C, and fermentation time is -72h for 24 hours, obtains fermentation and produces
Object；
S4, dries pulverizing: by the weight content that tunning is dried to moisture being 8%- at being 30 DEG C -80 DEG C in drying temperature
10%, it is then crushed to -80 mesh of 10 mesh, obtains filling product；
S5, composite filter preparation: glyceride will be sprayed after the abundant shredding of the tow of acetate fiber, the filling for then obtaining S4 produces
Object is sprayed on tow, is then wrapped up with forming paper and composite filter is made.
2. a kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle according to claim 1, it is characterised in that: in S1
In, the final viable bacteria amount of the strain is 0.1-10 × 108cfu/g。
3. a kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle according to claim 1, it is characterised in that: in S2
In, the sugar is glucose and/or maltose and/or lactose and/or sucrose and/or fructose.
4. a kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle according to claim 1, it is characterised in that: in S2
In, 30 DEG C -35 DEG C of warm water is added in fermentation base after mixing, adjusts the moisture content mass fraction of fermentation base to 30%-
50%.
5. a kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle according to claim 1, it is characterised in that: in S1
In, the raw material Chinese herbal medicine is to handle by removal of impurities, and individually crushed, and partial size is -200 mesh of 50 mesh.
6. a kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle according to claim 1, it is characterised in that: in S5
In, in the composite filter, the mass fraction of the filling product is 1-40 parts；The mass fraction of tow are as follows: 60-99 parts.
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Application publication date: 20181214 |
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