CN100355805C - 使用dmc催化生产聚醚醇的方法 - Google Patents

使用dmc催化生产聚醚醇的方法 Download PDF

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Publication number
CN100355805C
CN100355805C CNB2004800184122A CN200480018412A CN100355805C CN 100355805 C CN100355805 C CN 100355805C CN B2004800184122 A CNB2004800184122 A CN B2004800184122A CN 200480018412 A CN200480018412 A CN 200480018412A CN 100355805 C CN100355805 C CN 100355805C
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CN
China
Prior art keywords
acid
steam
product
aethoxy sklerol
butyl
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CNB2004800184122A
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English (en)
Chinese (zh)
Other versions
CN1813019A (zh
Inventor
T·奥斯特洛夫斯基
R·鲁佩尔
E·鲍姆
K·阿尔
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BASF SE
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BASF SE
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Application filed by BASF SE filed Critical BASF SE
Publication of CN1813019A publication Critical patent/CN1813019A/zh
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/50—Polyethers having heteroatoms other than oxygen
    • C08G18/5021—Polyethers having heteroatoms other than oxygen having nitrogen
    • C08G18/5054—Polyethers having heteroatoms other than oxygen having nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring
    • C08G18/5063—Polyethers having heteroatoms other than oxygen having nitrogen containing heterocyclic rings having at least one nitrogen atom in the ring containing three nitrogen atoms in the ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C08G65/10—Saturated oxiranes characterised by the catalysts used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/22—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the initiator used in polymerisation
    • C08G2650/24—Polymeric initiators

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Polyethers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyurethanes Or Polyureas (AREA)
CNB2004800184122A 2003-06-03 2004-06-03 使用dmc催化生产聚醚醇的方法 Expired - Fee Related CN100355805C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10324998.2 2003-06-03
DE10324998A DE10324998A1 (de) 2003-06-03 2003-06-03 Herstellung von Polyetheralkoholen unter Verwendung der DMC-Katalyse

Publications (2)

Publication Number Publication Date
CN1813019A CN1813019A (zh) 2006-08-02
CN100355805C true CN100355805C (zh) 2007-12-19

Family

ID=33482419

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2004800184122A Expired - Fee Related CN100355805C (zh) 2003-06-03 2004-06-03 使用dmc催化生产聚醚醇的方法

Country Status (10)

Country Link
US (1) US20060167209A1 (enExample)
EP (1) EP1633799B1 (enExample)
JP (2) JP2006526677A (enExample)
KR (1) KR101089004B1 (enExample)
CN (1) CN100355805C (enExample)
AT (1) ATE411351T1 (enExample)
DE (2) DE10324998A1 (enExample)
ES (1) ES2313011T3 (enExample)
PT (1) PT1633799E (enExample)
WO (1) WO2004106408A1 (enExample)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102004013408A1 (de) * 2004-03-18 2005-10-06 Basf Ag Polyetheralkohole und Verfahren zur Herstellung von Polyetheralkoholen zur Polyurethansynthese
US20080033214A1 (en) * 2004-06-09 2008-02-07 Duijghuisen Henricus Petrus B Process of Preparing Odour-Lean Polyether Polyol
EP2173803A1 (en) * 2007-08-01 2010-04-14 Basf Se Liquid antioxidant mixtures
DE102007057146A1 (de) * 2007-11-28 2009-06-04 Evonik Goldschmidt Gmbh Verfahren zur Herstellung von Polyetheralkoholen mit DMC-Katalysatoren unter Verwendung von speziellen Additiven mit aromatischer Hydroxy-Funktionalisierung
MX2010005449A (es) * 2007-12-19 2010-06-01 Basf Se Metodo para producir alcoholes de polieter.
RU2560724C2 (ru) 2009-07-29 2015-08-20 Басф Се Способ получения простых полиэфироспиртов из алкиленоксидов
EP2471831A4 (en) 2009-09-30 2013-08-21 Asahi Glass Co Ltd PROCESS FOR PREPARING AN ISOCYANATE-TERMINATED PREPOLYMER, PREPOLYMER AND POLYURETHANE RESIN GAINED IN THIS METHOD
BR112012007190A2 (pt) 2009-09-30 2016-03-29 Basf Se processo para a preparação de polímeros alcoxilados, polímero alcoxilado, processo para preparar poliuretanos, poliuretanos, reagente tensoativo, e, formulação detergente
US11332387B2 (en) * 2018-06-29 2022-05-17 Fuel Tech, Inc. Removing arsenic from water with acid-activated clay
CN111494976B (zh) * 2020-04-27 2022-07-15 上海化工研究院有限公司 一种淤浆法聚乙烯工艺中稀释剂的脱除装置
EP4273185A1 (en) 2022-05-04 2023-11-08 PCC Rokita SA Method for the manufacture of a polyether diol product
WO2024180261A2 (en) 2023-03-02 2024-09-06 Basf Se Environmenal friendly ethylene oxide, propylene oxide and downstream products
CN120936657A (zh) 2023-04-12 2025-11-11 巴斯夫欧洲公司 具有低氘含量的乙酸乙烯酯

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1084523A (zh) * 1993-07-18 1994-03-30 中国科学院广州化学研究所 一种聚醚醇脂肪酸酯及其制法和用途
CN1378571A (zh) * 1999-10-12 2002-11-06 巴斯福股份公司 聚醚醇化合物的制备方法
CN1379792A (zh) * 1999-10-12 2002-11-13 巴斯福股份公司 聚酯、聚醚嵌段共聚物
CN1409736A (zh) * 1999-12-14 2003-04-09 巴斯福股份公司 聚醚醇的制备方法

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US3829505A (en) * 1970-02-24 1974-08-13 Gen Tire & Rubber Co Polyethers and method for making the same
JPS5260899A (en) * 1975-11-14 1977-05-19 Nippon Oil & Fats Co Ltd Purification method of polyalkylene
JPS56104936A (en) * 1980-01-24 1981-08-21 Dai Ichi Kogyo Seiyaku Co Ltd Purification of polyether polyol
US5391722A (en) * 1990-03-30 1995-02-21 Olin Corporation Acid-catalyzed fabrication of precursors for use in making polyols using double metal cyanide catalysts
US5149862A (en) * 1991-02-26 1992-09-22 E. I. Du Pont De Nemours And Company Preparation of polytetramethylene ether glycol using an acidic zirconia catalyst
US5158922A (en) * 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
US5571935A (en) * 1994-01-14 1996-11-05 Cpc International Inc. Process for producing esterified alkoxylated polyols with improved stability
US5563221A (en) * 1995-06-21 1996-10-08 Arco Chemical Technology, L.P. Process for making ethylene oxide-capped polyols from double metal cyanide-catalyzed polyols
US5811829A (en) * 1995-08-10 1998-09-22 Arco Chemical Technology, L.P. Viscosity stable isocyanate-terminated prepolymers and polyoxyalkylene polyether polyols having improved storage stability
DE19745580B4 (de) * 1997-10-15 2012-08-16 Basf Se Verfahren zur Dampfeinleitung in Polymerdispersionen
IS4687A (is) * 1998-03-13 1998-04-06 Shell Internationale Research Maatschappij B.V. Aðferð við framleiðslu á lyktarlitlum pólýeter pólýólum
DE19928156A1 (de) * 1999-06-19 2000-12-28 Bayer Ag Aus Polyetherpolyolen hergestellte Polyurethan-Weichschäume
EP1295902A1 (en) * 2001-09-20 2003-03-26 Shell Internationale Researchmaatschappij B.V. Process for preparing polyoxyalkylene polyether products.

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1084523A (zh) * 1993-07-18 1994-03-30 中国科学院广州化学研究所 一种聚醚醇脂肪酸酯及其制法和用途
CN1378571A (zh) * 1999-10-12 2002-11-06 巴斯福股份公司 聚醚醇化合物的制备方法
CN1379792A (zh) * 1999-10-12 2002-11-13 巴斯福股份公司 聚酯、聚醚嵌段共聚物
CN1409736A (zh) * 1999-12-14 2003-04-09 巴斯福股份公司 聚醚醇的制备方法

Also Published As

Publication number Publication date
ATE411351T1 (de) 2008-10-15
EP1633799A1 (de) 2006-03-15
JP2006526677A (ja) 2006-11-24
CN1813019A (zh) 2006-08-02
KR101089004B1 (ko) 2011-12-01
KR20060026414A (ko) 2006-03-23
PT1633799E (pt) 2008-11-03
WO2004106408A1 (de) 2004-12-09
JP2010111875A (ja) 2010-05-20
US20060167209A1 (en) 2006-07-27
EP1633799B1 (de) 2008-10-15
ES2313011T3 (es) 2009-03-01
DE10324998A1 (de) 2004-12-23
DE502004008277D1 (de) 2008-11-27
JP5170576B2 (ja) 2013-03-27

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C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
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GR01 Patent grant
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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20071219

Termination date: 20140603