CH186169A - Process for the production of a new azo dye. - Google Patents

Process for the production of a new azo dye.

Info

Publication number
CH186169A
CH186169A CH186169DA CH186169A CH 186169 A CH186169 A CH 186169A CH 186169D A CH186169D A CH 186169DA CH 186169 A CH186169 A CH 186169A
Authority
CH
Switzerland
Prior art keywords
azo dye
production
new azo
dye
scarlet
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH186169A publication Critical patent/CH186169A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/10Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
    • C09B29/18Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides
    • C09B29/20Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides of the naphthalene series

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  Zusatzpatent zum Hauptpatent     Nr.   <B>183685.</B>    Verfahren zur Herstellung eines neuen     Azofarbstoffes.       Es wurde gefunden,     dass    man einen neuen       Azofarbstoff    erhält, wenn man     diazotiertes          1-Amit)o-4-methylphenyl-3-benzylsulfon    mit       2,3-Oxynaphthoesäui#eanilid    vereinigt. Der so  erhaltene Farbstoff bildet ein scharlachrotes,  in Wasser unlösliches Pulver. Auf geeigne  ten Substraten, wie zum Beispiel Zellulose,  hergestellt, färbt er diese in leuchtend schar  lachroten Tönen.

      <I>Beispiel:</I>    <B>26,1</B> Teile     1-Amino-4-methylphenyl-ä-          benzylsulfon    (das erhalten wird durch Konden  sieren der     1-Nitro-4-methylber)zol-3-sulfinsäui-e     mit     Benzylchlorid    und Reduktion des ent  standenen     Sulfons)    werden wie üblich     diazo-          tiert    und in eine Lösung von<B>26,3</B> Teilen     2,3-          Oxynaphthoesäureanilid,   <B>50</B> Teilen 30'/oigei-    Natronlauge,<B>15</B> Teilen Soda und 2<B>000</B> Teilen  Wasser eingetragen. Der gebildete Farbstoff  fällt sofort aus. Der scharlachrote Nieder  schlag wird filtriert und getrocknet.



  Additional patent to main patent no. <B> 183685. </B> Process for the production of a new azo dye. It has been found that a new azo dye is obtained when diazotized 1-amite) o-4-methylphenyl-3-benzylsulfone is combined with 2,3-oxynaphthoic acid anilide. The dye obtained in this way forms a scarlet red powder which is insoluble in water. Produced on suitable substrates such as cellulose, he colors them in bright, sharp, laugh-red tones.

      <I> Example: </I> <B> 26.1 </B> parts of 1-amino-4-methylphenyl-benzylsulfone (which is obtained by condensing the 1-nitro-4-methylber) zol-3 -sulfinsäui-e with benzyl chloride and reduction of the resulting sulfone) are diazotized as usual and converted into a solution of <B> 26.3 </B> parts of 2,3-oxynaphthoic anilide, <B> 50 </B> parts 30% sodium hydroxide solution, 15 parts soda and 2 000 parts water are added. The dye formed precipitates immediately. The scarlet precipitate is filtered and dried.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Azofarbstoffes, dadurch gekennzeichnet, dass man diazotiertes 1-Amino-4-methylpberiyl-3- benzylsulfon mit 2,3-Oxynaphthoesäureanilid vereinigt. Der so erhaltene Farbstoff bildet ein scharlachrotes, in Wasser unlösliches Pulver. Auf gäeigneten Substraten, wie zum Beispiel Zellulose hergestellt, färbt er diese in leuchtend scharlachroten Tönen. Claim: Process for the preparation of a new azo dye, characterized in that diazotized 1-amino-4-methylpberiyl-3-benzylsulfone is combined with 2,3-oxynaphthoic anilide. The dye obtained in this way forms a scarlet red powder which is insoluble in water. Produced on suitable substrates, such as cellulose, for example, he dyes them in bright scarlet shades.
CH186169D 1935-05-09 1935-05-09 Process for the production of a new azo dye. CH186169A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH186169T 1935-05-09
CH183685T 1935-05-09

Publications (1)

Publication Number Publication Date
CH186169A true CH186169A (en) 1936-08-31

Family

ID=25720898

Family Applications (1)

Application Number Title Priority Date Filing Date
CH186169D CH186169A (en) 1935-05-09 1935-05-09 Process for the production of a new azo dye.

Country Status (1)

Country Link
CH (1) CH186169A (en)

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