CH186169A - Process for the production of a new azo dye. - Google Patents
Process for the production of a new azo dye.Info
- Publication number
- CH186169A CH186169A CH186169DA CH186169A CH 186169 A CH186169 A CH 186169A CH 186169D A CH186169D A CH 186169DA CH 186169 A CH186169 A CH 186169A
- Authority
- CH
- Switzerland
- Prior art keywords
- azo dye
- production
- new azo
- dye
- scarlet
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title claims description 4
- 239000000975 dye Substances 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 150000003931 anilides Chemical class 0.000 claims description 2
- 229920002678 cellulose Polymers 0.000 claims description 2
- 239000001913 cellulose Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- RCTGMCJBQGBLKT-PAMTUDGESA-N scarlet red Chemical compound CC1=CC=CC=C1\N=N\C(C=C1C)=CC=C1\N=N\C1=C(O)C=CC2=CC=CC=C12 RCTGMCJBQGBLKT-PAMTUDGESA-N 0.000 claims description 2
- 229960005369 scarlet red Drugs 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- -1 3-oxynaphthoic acid anilide Chemical class 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical compound ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 description 1
- 229940073608 benzyl chloride Drugs 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 150000003457 sulfones Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/10—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
- C09B29/18—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides
- C09B29/20—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides of the naphthalene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. <B>183685.</B> Verfahren zur Herstellung eines neuen Azofarbstoffes. Es wurde gefunden, dass man einen neuen Azofarbstoff erhält, wenn man diazotiertes 1-Amit)o-4-methylphenyl-3-benzylsulfon mit 2,3-Oxynaphthoesäui#eanilid vereinigt. Der so erhaltene Farbstoff bildet ein scharlachrotes, in Wasser unlösliches Pulver. Auf geeigne ten Substraten, wie zum Beispiel Zellulose, hergestellt, färbt er diese in leuchtend schar lachroten Tönen.
<I>Beispiel:</I> <B>26,1</B> Teile 1-Amino-4-methylphenyl-ä- benzylsulfon (das erhalten wird durch Konden sieren der 1-Nitro-4-methylber)zol-3-sulfinsäui-e mit Benzylchlorid und Reduktion des ent standenen Sulfons) werden wie üblich diazo- tiert und in eine Lösung von<B>26,3</B> Teilen 2,3- Oxynaphthoesäureanilid, <B>50</B> Teilen 30'/oigei- Natronlauge,<B>15</B> Teilen Soda und 2<B>000</B> Teilen Wasser eingetragen. Der gebildete Farbstoff fällt sofort aus. Der scharlachrote Nieder schlag wird filtriert und getrocknet.
Additional patent to main patent no. <B> 183685. </B> Process for the production of a new azo dye. It has been found that a new azo dye is obtained when diazotized 1-amite) o-4-methylphenyl-3-benzylsulfone is combined with 2,3-oxynaphthoic acid anilide. The dye obtained in this way forms a scarlet red powder which is insoluble in water. Produced on suitable substrates such as cellulose, he colors them in bright, sharp, laugh-red tones.
<I> Example: </I> <B> 26.1 </B> parts of 1-amino-4-methylphenyl-benzylsulfone (which is obtained by condensing the 1-nitro-4-methylber) zol-3 -sulfinsäui-e with benzyl chloride and reduction of the resulting sulfone) are diazotized as usual and converted into a solution of <B> 26.3 </B> parts of 2,3-oxynaphthoic anilide, <B> 50 </B> parts 30% sodium hydroxide solution, 15 parts soda and 2 000 parts water are added. The dye formed precipitates immediately. The scarlet precipitate is filtered and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH186169T | 1935-05-09 | ||
| CH183685T | 1935-05-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH186169A true CH186169A (en) | 1936-08-31 |
Family
ID=25720898
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH186169D CH186169A (en) | 1935-05-09 | 1935-05-09 | Process for the production of a new azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH186169A (en) |
-
1935
- 1935-05-09 CH CH186169D patent/CH186169A/en unknown
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