CH183685A - Process for the production of a new azo dye. - Google Patents
Process for the production of a new azo dye.Info
- Publication number
- CH183685A CH183685A CH183685DA CH183685A CH 183685 A CH183685 A CH 183685A CH 183685D A CH183685D A CH 183685DA CH 183685 A CH183685 A CH 183685A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- azo dye
- new azo
- dye
- diazotized
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title claims description 4
- 239000000975 dye Substances 0.000 claims description 4
- -1 3-oxynaphthoic acid anilide Chemical class 0.000 claims description 3
- 229920002678 cellulose Polymers 0.000 claims description 2
- 239000001913 cellulose Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- 239000003086 colorant Substances 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 2
- AVHXRJBDMUSUCQ-UHFFFAOYSA-N 3-nitrobenzenesulfinic acid Chemical compound OS(=O)C1=CC=CC([N+]([O-])=O)=C1 AVHXRJBDMUSUCQ-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 150000003457 sulfones Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/10—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
- C09B29/18—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides
- C09B29/20—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides of the naphthalene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
Verfahren zur Herstellung eines neuen Azofarbstoffes. Es wurde gefunden, dass man einen neuen Azofarbstoff erhält, wenn man diazotiertes 1-Aminophenyl-3-beiizyl8ulfoii mit 2,3-Oxy- naphthoesäure-anilid vereinigt. Der so erhal tene Farbstoff bildet ein orange gefärbtes, in Wasser unlöslichesPulver. Auf geeigneten Substraten, wie zum Beispiel Zellulose, her gestellt, färbt er diese in leuchtend orangen Tönen.
<I>Beispiel:</I> 24,7 Teile 1-Aminophenyl-3-benzylsulfon (das erhalten wird durch Kondensieren der 1-Nitrobenzol-3-sulfinsäure mit BenzirIch16rid und Reduktion des entstandenen 'Sulfons) werden wie üblich diazotiert und in eine Lösung von<B>26,3</B> Teilen 2,3-Oxynaphthoe- säure-anilid, <B>50</B> Teilen<B>80</B> % iger Natronlauge, <B>15</B> Teilen Soda und 2000 Teilen Wasser ein getragen. Der gebildete Farbstoff fällt sofort aus. Der orange Niederschlag wird filtriert und getrocknet.
Process for the production of a new azo dye. It has been found that a new azo dye is obtained if diazotized 1-aminophenyl-3-beiicyl8ulfoii is combined with 2,3-oxynaphthoic acid anilide. The dye thus obtained forms an orange colored, water-insoluble powder. Produced on suitable substrates such as cellulose, he dyes them in bright orange tones.
<I> Example: </I> 24.7 parts of 1-aminophenyl-3-benzylsulfone (which is obtained by condensing the 1-nitrobenzene-3-sulfinic acid with benziric chloride and reducing the sulfone formed) are diazotized as usual and converted into a Solution of <B> 26.3 </B> parts of 2,3-oxynaphthoic acid anilide, <B> 50 </B> parts of <B> 80 </B>% sodium hydroxide, <B> 15 </ B> parts of soda and 2000 parts of water. The dye formed precipitates immediately. The orange precipitate is filtered and dried.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH183685T | 1935-05-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH183685A true CH183685A (en) | 1936-04-30 |
Family
ID=4432497
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH183685D CH183685A (en) | 1935-05-09 | 1935-05-09 | Process for the production of a new azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH183685A (en) |
-
1935
- 1935-05-09 CH CH183685D patent/CH183685A/en unknown
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