CH155024A - Process for the production of a new azo dye. - Google Patents
Process for the production of a new azo dye.Info
- Publication number
- CH155024A CH155024A CH155024DA CH155024A CH 155024 A CH155024 A CH 155024A CH 155024D A CH155024D A CH 155024DA CH 155024 A CH155024 A CH 155024A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- azo dye
- new azo
- dye
- anisidide
- Prior art date
Links
- 239000000987 azo dye Substances 0.000 title claims description 4
- 239000000975 dye Substances 0.000 claims description 5
- OCISOSJGBCQHHN-UHFFFAOYSA-N 3-hydroxynaphthalene-1-carboxylic acid Chemical compound C1=CC=C2C(C(=O)O)=CC(O)=CC2=C1 OCISOSJGBCQHHN-UHFFFAOYSA-N 0.000 claims description 2
- 229920000742 Cotton Polymers 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/10—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group
- C09B29/18—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides
- C09B29/20—Monoazo dyes prepared by diazotising and coupling from coupling components containing hydroxy as the only directing group ortho-Hydroxy carbonamides of the naphthalene series
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. <B>162883-</B> Verfahren zur Herstellung eines neuen Azofarbstoffes. Es wurde gefunden, dass man einen neuen Azofarbstoff der Formel-.
EMI0001.0005
erhält, wenn man den 4-Ohlor-4'-methoxy- 2-diazo-1 <B>.</B> l'-diphenyläther mit dem o-Anisidid der 2. S-Oxynaphthoesäure kuppelt.
Der so erhaltene Farbstoff bildet ein hell rotes Pulver. Auf geeigneten Substraten, wie zum Beispiel Baumwolle, hergestellt, färbt er diese in leuchtenden, ausserordentlich echten Tönen.
<I>Beispiel:</I> 24,9 Teile 4-Cblor-4'-methoxy-2-amino- 1 <B>.</B> l'-diphenyläther werden wie üblich diazo- tiert und in eine Lösung von<B>29,3</B> Teilen des o-Anisidids der 2. 3-Oxynaphthoesäure, <B>60</B> Teilen<B>30</B> '/oiger Natronlauge,<B>15</B> Teilen Soda und 2000 Teilen Wasser eingetragen. Der gebildete Farbstoff fällt sofort aus. Er wird filtriert, gewaschen und getrocknet.
Additional patent to main patent no. <B> 162883- </B> Process for the production of a new azo dye. It has been found that a new azo dye of the formula.
EMI0001.0005
obtained when the 4-chloro-4'-methoxy-2-diazo-1 <B>. </B> l'-diphenyl ether is coupled with the o-anisidide of the 2nd S-oxynaphthoic acid.
The dye thus obtained forms a light red powder. Produced on suitable substrates, such as cotton, for example, he dyes them in bright, extraordinarily real tones.
<I> Example: </I> 24.9 parts of 4-chloro-4'-methoxy-2-amino-1 <B>. </B> l'-diphenyl ether are diazo- tated as usual and converted into a solution of <B> 29.3 </B> parts of the o-anisidide of the 2nd 3-oxynaphthoic acid, <B> 60 </B> parts <B> 30 </B> '/ oiger sodium hydroxide, <B> 15 </ B> parts of soda and 2000 parts of water entered. The dye formed precipitates immediately. It is filtered, washed and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH152883T | 1930-11-15 | ||
| CH155024T | 1930-11-15 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH155024A true CH155024A (en) | 1932-05-31 |
Family
ID=25716076
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH155024D CH155024A (en) | 1930-11-15 | 1930-11-15 | Process for the production of a new azo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH155024A (en) |
-
1930
- 1930-11-15 CH CH155024D patent/CH155024A/en unknown
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