CA2988553C - Bipyramid-templated synthesis of monodisperse noble metal nanocrystals - Google Patents

Bipyramid-templated synthesis of monodisperse noble metal nanocrystals Download PDF

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Publication number
CA2988553C
CA2988553C CA2988553A CA2988553A CA2988553C CA 2988553 C CA2988553 C CA 2988553C CA 2988553 A CA2988553 A CA 2988553A CA 2988553 A CA2988553 A CA 2988553A CA 2988553 C CA2988553 C CA 2988553C
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nanocrystals
twinned
bipyramid
reaction mixture
penta
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English (en)
French (fr)
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CA2988553A1 (en
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Yossi Weizmann
Kyle GIBSON
Jung-Hoon Lee
Zoya Cheglakov
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University of Chicago
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University of Chicago
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B22F1/0553—Complex form nanoparticles, e.g. prism, pyramid, octahedron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02—Elements
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/34—Silicates
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/52—Alloys
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/60—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
    • C30B29/66—Crystals of complex geometrical shape, e.g. tubes, cylinders
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/005—Epitaxial layer growth
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/14—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions the crystallising materials being formed by chemical reactions in the solution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/052—Metallic powder characterised by the size or surface area of the particles characterised by a mixture of particles of different sizes or by the particle size distribution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y20/00—Nanooptics, e.g. quantum optics or photonic crystals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Nanotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Geometry (AREA)
  • Manufacturing & Machinery (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Measuring Or Testing Involving Enzymes Or Micro-Organisms (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)
  • Silicon Compounds (AREA)
CA2988553A 2015-06-08 2016-05-09 Bipyramid-templated synthesis of monodisperse noble metal nanocrystals Active CA2988553C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562172481P 2015-06-08 2015-06-08
US62/172,481 2015-06-08
PCT/US2016/031522 WO2016200525A1 (en) 2015-06-08 2016-05-09 Bipyramid-templated synthesis of monodisperse noble metal nanocrystals

Publications (2)

Publication Number Publication Date
CA2988553A1 CA2988553A1 (en) 2016-12-15
CA2988553C true CA2988553C (en) 2022-02-15

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CA2988553A Active CA2988553C (en) 2015-06-08 2016-05-09 Bipyramid-templated synthesis of monodisperse noble metal nanocrystals

Country Status (8)

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US (2) US11045874B2 (https=)
EP (1) EP3303662B1 (https=)
JP (2) JP2018525305A (https=)
CN (1) CN107849726B (https=)
AU (1) AU2016274238B2 (https=)
CA (1) CA2988553C (https=)
HK (1) HK1253414A1 (https=)
WO (1) WO2016200525A1 (https=)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3303662B1 (en) 2015-06-08 2022-03-09 The University of Chicago Bipyramid-templated synthesis of monodisperse noble metal nanocrystals
KR20190091185A (ko) * 2018-01-26 2019-08-05 서울대학교산학협력단 모서리 첨예도 지수가 조절된 금속 나노큐브의 제조방법
CN108356278A (zh) * 2018-03-01 2018-08-03 东南大学 一种表面等离激元纳米钉结构的规模化可控制备方法
CN109128210A (zh) * 2018-08-02 2019-01-04 黄河科技学院 一种哑铃状金纳米双锥/银纳米复合材料及其制备方法
WO2020237017A1 (en) * 2019-05-22 2020-11-26 Promega Corporation Methods using photothermal nanoparticles in rapid nucleic acid amplification and photothermal nanoparticles
CN110193608B (zh) * 2019-06-06 2022-03-11 中国科学院合肥物质科学研究院 一种基于微刻蚀的从金纳米哑铃到金纳米颗粒的调控方法
CN113275555B (zh) * 2021-04-13 2022-04-19 南京航空航天大学 一种阵列结构的金属纳米框及其制备方法与应用
CN113369492B (zh) * 2021-06-09 2022-09-13 合肥工业大学 一种五重孪晶铂纳米棒及其制备方法
CN113984685B (zh) * 2021-09-30 2023-03-10 南京航空航天大学 一种银纳米结构生长机理的分析方法
WO2023123134A1 (zh) 2021-12-29 2023-07-06 长庚大学 核酸扩增方法及其装置暨核酸检测方法与其装置
CN114309592B (zh) * 2021-12-30 2025-01-10 杭州电子科技大学 一种在金纳米棒两端包覆二氧化硅的方法
CN115901630B (zh) * 2023-01-05 2023-06-06 武汉理工大学 一种氢敏反射膜片、制备方法及氢气浓度检测装置
CN116559120A (zh) * 2023-04-19 2023-08-08 大连海事大学 一种基于金双锥体纳米粒子的高灵敏度近红外lspr光纤生化传感器
CN117300118B (zh) * 2023-09-27 2026-03-31 浙江理工大学嵊州创新研究院有限公司 一种多组分复合异构纳米材料及其制备方法及应用

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JP4540754B2 (ja) * 1996-06-04 2010-09-08 ユニバーシティ オブ ユタ リサーチ ファウンデーション Ｐｃｒ中のハイブリダイゼーションのモニタリング
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WO2009045579A2 (en) * 2007-06-14 2009-04-09 The Regents Of The University Of California Multimodal imaging probes for in vivo targeted and non-targeted imaging and therapeutics
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CN101618461B (zh) * 2009-08-12 2011-02-16 吉林大学 葫芦状、哑铃状或棒状金纳米粒子的制备方法
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EP3303662B1 (en) 2015-06-08 2022-03-09 The University of Chicago Bipyramid-templated synthesis of monodisperse noble metal nanocrystals

Also Published As

Publication number Publication date
JP2018525305A (ja) 2018-09-06
AU2016274238B2 (en) 2020-04-30
JP2021052786A (ja) 2021-04-08
JP7142958B2 (ja) 2022-09-28
US11872635B2 (en) 2024-01-16
WO2016200525A1 (en) 2016-12-15
EP3303662A4 (en) 2018-12-05
EP3303662B1 (en) 2022-03-09
HK1253414A1 (zh) 2019-06-14
AU2016274238A1 (en) 2018-02-01
CN107849726A (zh) 2018-03-27
EP3303662A1 (en) 2018-04-11
CA2988553A1 (en) 2016-12-15
US20180297120A1 (en) 2018-10-18
CN107849726B (zh) 2021-07-13
US11045874B2 (en) 2021-06-29
US20210276095A1 (en) 2021-09-09

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