CA2878248C - Reactor system for the production of carbon allotropes - Google Patents

Reactor system for the production of carbon allotropes Download PDF

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Publication number
CA2878248C
CA2878248C CA2878248A CA2878248A CA2878248C CA 2878248 C CA2878248 C CA 2878248C CA 2878248 A CA2878248 A CA 2878248A CA 2878248 A CA2878248 A CA 2878248A CA 2878248 C CA2878248 C CA 2878248C
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CA
Canada
Prior art keywords
reactor
catalyst
stream
carbon allotropes
separation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA2878248A
Other languages
English (en)
French (fr)
Other versions
CA2878248A1 (en
Inventor
Russell J. Koveal
Terry A. Ring
Original Assignee
SOLID CARBON PRODUCTS LLC
ExxonMobil Upstream Research Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SOLID CARBON PRODUCTS LLC, ExxonMobil Upstream Research Co filed Critical SOLID CARBON PRODUCTS LLC
Publication of CA2878248A1 publication Critical patent/CA2878248A1/en
Application granted granted Critical
Publication of CA2878248C publication Critical patent/CA2878248C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836—Heating and cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/16—Preparation
    • C01B32/162—Preparation characterised by catalysts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/16—Preparation
    • C01B32/164—Preparation involving continuous processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00752—Feeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00761—Discharging
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00893—Feeding means for the reactants
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Combustion & Propulsion (AREA)
  • Manufacturing & Machinery (AREA)
  • Composite Materials (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Fibers (AREA)
CA2878248A 2012-09-18 2013-09-13 Reactor system for the production of carbon allotropes Expired - Fee Related CA2878248C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201261702620P 2012-09-18 2012-09-18
US61/702,620 2012-09-18
PCT/US2013/059613 WO2014046972A1 (en) 2012-09-18 2013-09-13 Reactor system for the production of carbon allotropes

Publications (2)

Publication Number Publication Date
CA2878248A1 CA2878248A1 (en) 2014-03-27
CA2878248C true CA2878248C (en) 2019-11-12

Family

ID=50341872

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2878248A Expired - Fee Related CA2878248C (en) 2012-09-18 2013-09-13 Reactor system for the production of carbon allotropes

Country Status (13)

Country Link
US (1) US9663367B2 (OSRAM)
EP (1) EP2897900A4 (OSRAM)
JP (1) JP6252915B2 (OSRAM)
KR (1) KR102116696B1 (OSRAM)
CN (1) CN104603051B (OSRAM)
AR (1) AR092596A1 (OSRAM)
AU (1) AU2013318327B2 (OSRAM)
CA (1) CA2878248C (OSRAM)
MX (1) MX369935B (OSRAM)
MY (1) MY169176A (OSRAM)
SG (1) SG11201408692VA (OSRAM)
TW (1) TWI638770B (OSRAM)
WO (1) WO2014046972A1 (OSRAM)

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KR102669941B1 (ko) * 2016-02-27 2024-05-27 니폰 제온 가부시키가이샤 섬유상 탄소 나노 구조체의 제조 방법
CN108778493B (zh) * 2016-02-27 2022-02-11 学校法人早稻田大学 粒子处理装置以及催化剂担载体和/或纤维状碳纳米结构体的制造方法
US12281013B2 (en) 2016-10-06 2025-04-22 Lyten, Inc. Microwave reactor system enclosing a self-igniting plasma
WO2018067814A1 (en) * 2016-10-06 2018-04-12 Lyten, Inc. Microwave reactor system with gas-solids separation
US9812295B1 (en) 2016-11-15 2017-11-07 Lyten, Inc. Microwave chemical processing
US9767992B1 (en) 2017-02-09 2017-09-19 Lyten, Inc. Microwave chemical processing reactor
US9997334B1 (en) 2017-02-09 2018-06-12 Lyten, Inc. Seedless particles with carbon allotropes
US10920035B2 (en) 2017-03-16 2021-02-16 Lyten, Inc. Tuning deformation hysteresis in tires using graphene
EP3596163A4 (en) 2017-03-16 2021-01-13 Lyten, Inc. CARBON AND ELASTOMER INTEGRATION
CN108726507B (zh) * 2017-04-21 2020-11-13 山东大展纳米材料有限公司 一种单级连续化制备碳纳米管的装置及方法
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CN112105922B (zh) * 2018-01-04 2024-09-03 利腾股份有限公司 谐振气体传感器
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CN113135562B (zh) * 2020-01-20 2024-02-23 山东大展纳米材料有限公司 一种制备碳纳米管和氢气的方法和装置
CN111348642B (zh) * 2020-04-23 2022-03-08 无锡东恒新能源科技有限公司 一种浮动催化法制备单壁碳纳米管的装置及方法
WO2022049427A1 (en) * 2020-09-04 2022-03-10 Hindustan Petroleum Corporation Limited Co-production of hydrogen-enriched compressed natural gas and carbon nanotubes
CN116600884A (zh) * 2020-12-11 2023-08-15 株式会社Lg化学 碳纳米管制造装置和碳纳米管制造方法
WO2022124867A1 (ko) * 2020-12-11 2022-06-16 주식회사 엘지화학 탄소나노튜브 제조장치 및 제조방법
EP4408796A4 (en) * 2021-10-01 2025-09-03 Chasm Advanced Mat Inc SYSTEM AND METHOD FOR THE SYNTHESIS OF CARBON NANOTUBES AND HYBRID MATERIALS BY CATALYTIC CHEMICAL DEPOSITION

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Also Published As

Publication number Publication date
MY169176A (en) 2019-02-25
JP2015533762A (ja) 2015-11-26
CA2878248A1 (en) 2014-03-27
KR102116696B1 (ko) 2020-06-01
EP2897900A4 (en) 2016-08-31
AR092596A1 (es) 2015-04-29
TW201422522A (zh) 2014-06-16
MX2014015920A (es) 2015-04-10
AU2013318327A1 (en) 2015-04-16
JP6252915B2 (ja) 2017-12-27
KR20150056535A (ko) 2015-05-26
WO2014046972A1 (en) 2014-03-27
CN104603051B (zh) 2017-06-09
US9663367B2 (en) 2017-05-30
TWI638770B (zh) 2018-10-21
EP2897900A1 (en) 2015-07-29
AU2013318327B2 (en) 2015-11-26
SG11201408692VA (en) 2015-02-27
CN104603051A (zh) 2015-05-06
US20150246813A1 (en) 2015-09-03
MX369935B (es) 2019-11-26

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