CA2710768A1 - Method for making colloidal metal oxide particles - Google Patents
Method for making colloidal metal oxide particles Download PDFInfo
- Publication number
- CA2710768A1 CA2710768A1 CA2710768A CA2710768A CA2710768A1 CA 2710768 A1 CA2710768 A1 CA 2710768A1 CA 2710768 A CA2710768 A CA 2710768A CA 2710768 A CA2710768 A CA 2710768A CA 2710768 A1 CA2710768 A1 CA 2710768A1
- Authority
- CA
- Canada
- Prior art keywords
- metal oxide
- silica
- reaction vessel
- particles
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 239000002245 particle Substances 0.000 title claims abstract description 256
- 150000004706 metal oxides Chemical class 0.000 title claims abstract description 252
- 229910044991 metal oxide Inorganic materials 0.000 title claims abstract description 251
- 238000000034 method Methods 0.000 title claims abstract description 104
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 131
- 239000000377 silicon dioxide Substances 0.000 claims description 44
- 239000000376 reactant Substances 0.000 claims description 27
- 239000008119 colloidal silica Substances 0.000 claims description 23
- 238000004519 manufacturing process Methods 0.000 claims description 21
- 230000006911 nucleation Effects 0.000 claims description 16
- 238000010899 nucleation Methods 0.000 claims description 16
- 230000008021 deposition Effects 0.000 claims description 15
- 238000013178 mathematical model Methods 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 10
- 239000003729 cation exchange resin Substances 0.000 claims description 10
- 230000035484 reaction time Effects 0.000 claims description 10
- 150000004760 silicates Chemical class 0.000 claims description 7
- 229910052910 alkali metal silicate Inorganic materials 0.000 claims description 5
- 239000003456 ion exchange resin Substances 0.000 claims description 5
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 5
- 230000009467 reduction Effects 0.000 claims description 5
- 238000010791 quenching Methods 0.000 claims description 4
- 230000000171 quenching effect Effects 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims 4
- 239000007795 chemical reaction product Substances 0.000 claims 2
- 239000000203 mixture Substances 0.000 abstract description 14
- 238000007792 addition Methods 0.000 description 30
- 230000008569 process Effects 0.000 description 13
- 238000007796 conventional method Methods 0.000 description 9
- 239000002994 raw material Substances 0.000 description 9
- 229910052681 coesite Inorganic materials 0.000 description 7
- 229910052906 cristobalite Inorganic materials 0.000 description 7
- 229910052682 stishovite Inorganic materials 0.000 description 7
- 229910052905 tridymite Inorganic materials 0.000 description 7
- 229940023913 cation exchange resins Drugs 0.000 description 6
- 235000012239 silicon dioxide Nutrition 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- 238000012986 modification Methods 0.000 description 5
- 230000004048 modification Effects 0.000 description 5
- 239000011347 resin Substances 0.000 description 5
- 229920005989 resin Polymers 0.000 description 5
- 239000000758 substrate Substances 0.000 description 5
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 238000013386 optimize process Methods 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 150000001768 cations Chemical class 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 239000004115 Sodium Silicate Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 238000011065 in-situ storage Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 229910052752 metalloid Inorganic materials 0.000 description 2
- 150000002738 metalloids Chemical class 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 235000019353 potassium silicate Nutrition 0.000 description 2
- 238000012552 review Methods 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 229910052911 sodium silicate Inorganic materials 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000004111 Potassium silicate Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 239000000378 calcium silicate Substances 0.000 description 1
- 229910052918 calcium silicate Inorganic materials 0.000 description 1
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- PAZHGORSDKKUPI-UHFFFAOYSA-N lithium metasilicate Chemical compound [Li+].[Li+].[O-][Si]([O-])=O PAZHGORSDKKUPI-UHFFFAOYSA-N 0.000 description 1
- 229910052912 lithium silicate Inorganic materials 0.000 description 1
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000019792 magnesium silicate Nutrition 0.000 description 1
- 238000004377 microelectronic Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000013387 non optimize process Methods 0.000 description 1
- 150000002927 oxygen compounds Chemical class 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 229910052699 polonium Inorganic materials 0.000 description 1
- HZEBHPIOVYHPMT-UHFFFAOYSA-N polonium atom Chemical compound [Po] HZEBHPIOVYHPMT-UHFFFAOYSA-N 0.000 description 1
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 1
- 229910052913 potassium silicate Inorganic materials 0.000 description 1
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 235000019351 sodium silicates Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000004627 transmission electron microscopy Methods 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/0004—Preparation of sols
- B01J13/0047—Preparation of sols containing a metal oxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Colloid Chemistry (AREA)
- Silicon Compounds (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US924507P | 2007-12-27 | 2007-12-27 | |
| US61/009,245 | 2007-12-27 | ||
| PCT/US2008/013358 WO2009085091A2 (en) | 2007-12-27 | 2008-12-04 | Method for making colloidal metal oxide particles |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2710768A1 true CA2710768A1 (en) | 2009-07-09 |
Family
ID=40723278
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2710768A Abandoned CA2710768A1 (en) | 2007-12-27 | 2008-12-04 | Method for making colloidal metal oxide particles |
Country Status (13)
| Country | Link |
|---|---|
| EP (1) | EP2231323A2 (ko) |
| JP (1) | JP5637863B2 (ko) |
| KR (1) | KR101629035B1 (ko) |
| CN (1) | CN101959590B (ko) |
| AR (1) | AR069976A1 (ko) |
| AU (1) | AU2008344012A1 (ko) |
| BR (1) | BRPI0821516A2 (ko) |
| CA (1) | CA2710768A1 (ko) |
| CL (1) | CL2008003914A1 (ko) |
| MX (1) | MX2010007105A (ko) |
| RU (1) | RU2557238C2 (ko) |
| TW (1) | TWI466714B (ko) |
| WO (1) | WO2009085091A2 (ko) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5602190B2 (ja) * | 2012-06-08 | 2014-10-08 | 住友ゴム工業株式会社 | 高分子材料のシミュレーション方法 |
| CN110217799B (zh) * | 2018-03-02 | 2020-12-18 | 中国石油化工股份有限公司 | 硅溶胶及其制备方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3538015A (en) * | 1967-12-07 | 1970-11-03 | Nalco Chemical Co | Large particle silica sols and method of production |
| US3969266A (en) * | 1971-06-23 | 1976-07-13 | E. I. Du Pont De Nemours And Company | Microporous membrane process for making concentrated silica sols |
| US3789009A (en) * | 1971-07-15 | 1974-01-29 | Du Pont | Process for the preparation of large particle silica sols |
| SU1452789A1 (ru) * | 1987-03-13 | 1989-01-23 | Армянский филиал Всесоюзного научно-исследовательского института химических реактивов и особо чистых химических веществ | Способ получени гидрозолей кремнезема |
| US5352277A (en) * | 1988-12-12 | 1994-10-04 | E. I. Du Pont De Nemours & Company | Final polishing composition |
| SU1712307A1 (ru) * | 1989-11-01 | 1992-02-15 | Всесоюзный Научно-Исследовательский И Проектный Институт "Теплопроект" | Способ получени кремнезол |
| US5100581A (en) * | 1990-02-22 | 1992-03-31 | Nissan Chemical Industries Ltd. | Method of preparing high-purity aqueous silica sol |
| DE4216119C2 (de) * | 1992-05-15 | 1995-08-10 | Bayer Ag | Verfahren zur Herstellung und Konzentrierung von Kieselsolen |
| US6906109B2 (en) * | 2000-09-01 | 2005-06-14 | Chemical Products Corp. | Method for controling uniformity of colloidal silica particle size |
| FR2819245B1 (fr) * | 2001-01-09 | 2004-11-26 | Clariant | Nouvelles suspensions aqueuses de silice colloidale anionique de ph neutre et leur procede de preparation, et leurs applications |
| CN100337914C (zh) * | 2002-10-14 | 2007-09-19 | 阿克佐诺贝尔公司 | 含水二氧化硅分散液 |
| US20070034116A1 (en) * | 2005-08-10 | 2007-02-15 | Mac Donald Dennis L | Silica sols with controlled minimum particle size and preparation thereof |
-
2008
- 2008-12-04 EP EP08866152A patent/EP2231323A2/en not_active Withdrawn
- 2008-12-04 WO PCT/US2008/013358 patent/WO2009085091A2/en active Application Filing
- 2008-12-04 RU RU2010131001/04A patent/RU2557238C2/ru not_active IP Right Cessation
- 2008-12-04 BR BRPI0821516A patent/BRPI0821516A2/pt not_active IP Right Cessation
- 2008-12-04 JP JP2010540633A patent/JP5637863B2/ja not_active Expired - Fee Related
- 2008-12-04 CN CN200880127591.1A patent/CN101959590B/zh not_active Expired - Fee Related
- 2008-12-04 MX MX2010007105A patent/MX2010007105A/es unknown
- 2008-12-04 CA CA2710768A patent/CA2710768A1/en not_active Abandoned
- 2008-12-04 AU AU2008344012A patent/AU2008344012A1/en not_active Abandoned
- 2008-12-04 KR KR1020107016727A patent/KR101629035B1/ko not_active IP Right Cessation
- 2008-12-23 AR ARP080105717A patent/AR069976A1/es unknown
- 2008-12-24 TW TW97150396A patent/TWI466714B/zh not_active IP Right Cessation
- 2008-12-26 CL CL2008003914A patent/CL2008003914A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| MX2010007105A (es) | 2010-08-26 |
| AR069976A1 (es) | 2010-03-03 |
| WO2009085091A3 (en) | 2009-11-12 |
| CN101959590A (zh) | 2011-01-26 |
| RU2557238C2 (ru) | 2015-07-20 |
| EP2231323A2 (en) | 2010-09-29 |
| TW200938294A (en) | 2009-09-16 |
| RU2010131001A (ru) | 2012-02-10 |
| TWI466714B (zh) | 2015-01-01 |
| CN101959590B (zh) | 2014-12-10 |
| KR101629035B1 (ko) | 2016-06-09 |
| CL2008003914A1 (es) | 2010-10-01 |
| AU2008344012A1 (en) | 2009-07-09 |
| BRPI0821516A2 (pt) | 2017-06-06 |
| KR20100105863A (ko) | 2010-09-30 |
| WO2009085091A2 (en) | 2009-07-09 |
| JP5637863B2 (ja) | 2014-12-10 |
| JP2011508719A (ja) | 2011-03-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Dead |