CA1253867A - Process for the preparation of monocarbonyl or biscarbonyl compounds - Google Patents

Process for the preparation of monocarbonyl or biscarbonyl compounds

Info

Publication number
CA1253867A
CA1253867A CA000469941A CA469941A CA1253867A CA 1253867 A CA1253867 A CA 1253867A CA 000469941 A CA000469941 A CA 000469941A CA 469941 A CA469941 A CA 469941A CA 1253867 A CA1253867 A CA 1253867A
Authority
CA
Canada
Prior art keywords
atoms
formula
process according
hydrogenation
alkylene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA000469941A
Other languages
English (en)
French (fr)
Inventor
Alexander Sajtos
Manfred Wechsberg
Erich Roithner
Stefan Pollhammer
Andreas Mahringer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Patheon Austria GmbH and Co KG
Original Assignee
Chemie Linz AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chemie Linz AG filed Critical Chemie Linz AG
Application granted granted Critical
Publication of CA1253867A publication Critical patent/CA1253867A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/40—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with ozone; by ozonolysis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C315/00—Preparation of sulfones; Preparation of sulfoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • C07C45/57—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom
    • C07C45/59—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom in five-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
    • C07C47/12—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen containing more than one —CHO group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
    • C07C47/198—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen containing ether groups, groups, groups, or groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/52—Compounds having —CHO groups bound to carbon atoms of six—membered aromatic rings
    • C07C47/542—Alkylated benzaldehydes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/52—Compounds having —CHO groups bound to carbon atoms of six—membered aromatic rings
    • C07C47/544—Diformyl benzenes; Alkylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/04—Saturated compounds containing keto groups bound to acyclic carbon atoms
    • C07C49/12—Ketones containing more than one keto group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/313—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by introduction of doubly bound oxygen containing functional groups, e.g. carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/44—Radicals substituted by doubly-bound oxygen, sulfur, or nitrogen atoms, or by two such atoms singly-bound to the same carbon atom
    • C07D213/46—Oxygen atoms
    • C07D213/48—Aldehydo radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CA000469941A 1983-12-23 1984-12-12 Process for the preparation of monocarbonyl or biscarbonyl compounds Expired CA1253867A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AT0450083A AT380008B (de) 1983-12-23 1983-12-23 Verfahren zur herstellung von mono- oder biscarbonylverbindungen
ATA4500/83 1983-12-23

Publications (1)

Publication Number Publication Date
CA1253867A true CA1253867A (en) 1989-05-09

Family

ID=3564834

Family Applications (1)

Application Number Title Priority Date Filing Date
CA000469941A Expired CA1253867A (en) 1983-12-23 1984-12-12 Process for the preparation of monocarbonyl or biscarbonyl compounds

Country Status (15)

Country Link
US (1) US4769464A (US06373033-20020416-M00071.png)
EP (1) EP0147593B1 (US06373033-20020416-M00071.png)
JP (1) JPS60156635A (US06373033-20020416-M00071.png)
KR (1) KR920000444B1 (US06373033-20020416-M00071.png)
AT (2) AT380008B (US06373033-20020416-M00071.png)
AU (1) AU572246B2 (US06373033-20020416-M00071.png)
CA (1) CA1253867A (US06373033-20020416-M00071.png)
DE (2) DE3401672A1 (US06373033-20020416-M00071.png)
ES (1) ES8606234A1 (US06373033-20020416-M00071.png)
GR (1) GR81086B (US06373033-20020416-M00071.png)
HU (1) HU198437B (US06373033-20020416-M00071.png)
IE (1) IE57650B1 (US06373033-20020416-M00071.png)
IL (1) IL73933A (US06373033-20020416-M00071.png)
NZ (1) NZ210517A (US06373033-20020416-M00071.png)
ZA (1) ZA849894B (US06373033-20020416-M00071.png)

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DE3346266A1 (de) * 1983-12-21 1985-07-11 Lentia Gmbh Verfahren zur herstelung von glyoxal, alkylglyoxalen und von deren acetalen
DE3544046A1 (de) * 1985-12-13 1987-06-19 Degussa Verfahren zur herstellung von 2,5-dimethoxy- und 2,5-diethoxytetrahydrofuran
ATE127775T1 (de) * 1989-12-14 1995-09-15 Chemie Linz Gmbh Verfahren zur herstellung von alpha-omega- alkandicarbonsäuren.
AT398759B (de) * 1993-03-12 1995-01-25 Chemie Linz Gmbh Hydrogenolytische reduktion peroxidischer ozonolyseprodukte und vorrichtung zu ihrer durchführung
TW299317B (US06373033-20020416-M00071.png) * 1993-03-12 1997-03-01 Chemie Linz Gmbh
AT402293B (de) * 1994-09-06 1997-03-25 Chemie Linz Gmbh Verfahren zur herstellung von mono- oder dicarbonsäuren aus aldehyden, deren vollacetalen oder halbacetalen, sowie aus gemischen davon
AT404938B (de) * 1996-10-30 1999-03-25 Chemie Linz Gmbh Verfahren zur reinigung von o-phthaldialdehyd
DE19811517A1 (de) * 1998-03-17 1999-09-23 Studiengesellschaft Kohle Mbh Verfahren zur Oxidation von Cyclohexan mit Ozon
AT408099B (de) * 1999-11-26 2001-08-27 Dsm Fine Chem Austria Gmbh Verfahren zur herstellung von hydroxymethylpyridinen
WO2001062696A1 (en) * 2000-02-25 2001-08-30 Akzo Nobel N.V. Process for the preparation of glyceraldehyde and derivatives thereof
CA2413970A1 (en) * 2000-06-22 2001-12-27 James D. Burrington Acylating agents and dispersants for lubricating oil and fuels
AT500421A1 (de) 2000-12-14 2005-12-15 Dsm Fine Chem Austria Gmbh Verbessertes verfahren zur reinigung von ketonen, erhalten aus den korrespondierenden terpenen durch ozonolyse und reduktion
AT500489A1 (de) * 2001-03-09 2006-01-15 Dsm Fine Chem Austria Gmbh Verfahren zur herstellung von mono- oder biscarbonyl- oder hydroxylverbindungen
AT413537B (de) 2001-05-15 2006-03-15 Dsm Fine Chem Austria Gmbh Verbessertes verfahren zur reinigung und formulierung von o-phthalaldehyd
AT412087B (de) * 2002-12-13 2004-09-27 Dsm Fine Chem Austria Gmbh In-situ zersetzung von peroxiden während der ozonolyse von alkenen
HU227638B1 (en) * 2005-12-23 2011-10-28 Thales Rt Flowing laboratorial ozonizating apparatus and method for ozonization reaction
CN101460450B (zh) * 2006-05-23 2013-03-20 帝斯曼知识产权资产管理有限公司 在一系列微反应器中经由危险中间体制备化合物的方法
US7754913B2 (en) * 2006-07-11 2010-07-13 Cambridge Isotope Laboratories, Inc. Synthesis of isotopically labeled alpha-keto acids and esters
WO2008077769A1 (en) * 2006-12-20 2008-07-03 Dsm Fine Chemicals Austria Nfg Gmbh & Co Kg Process for the safe ozonolysis of organic compounds in flammable solvents
US9828324B2 (en) 2010-10-20 2017-11-28 Sirrus, Inc. Methylene beta-diketone monomers, methods for making methylene beta-diketone monomers, polymerizable compositions and products formed therefrom
US9279022B1 (en) 2014-09-08 2016-03-08 Sirrus, Inc. Solution polymers including one or more 1,1-disubstituted alkene compounds, solution polymerization methods, and polymer compositions
US10414839B2 (en) 2010-10-20 2019-09-17 Sirrus, Inc. Polymers including a methylene beta-ketoester and products formed therefrom
AU2011317067A1 (en) * 2010-10-20 2013-05-23 Bioformix, Inc. Synthesis of methylene malonates using rapid recovery in the presence of a heat transfer agent
US9249265B1 (en) 2014-09-08 2016-02-02 Sirrus, Inc. Emulsion polymers including one or more 1,1-disubstituted alkene compounds, emulsion methods, and polymer compositions
JP2014532625A (ja) 2011-10-19 2014-12-08 シラス・インコーポレイテッド メチレンβ−ジケトンモノマー、メチレンβ−ジケトンモノマーを製造するための方法、これらから作られる重合可能な組成物および製品
JP6188252B2 (ja) 2012-03-30 2017-08-30 シラス・インコーポレイテッド 重合性組成物の活性化方法、重合系およびこれにより形成される製品
US10913875B2 (en) 2012-03-30 2021-02-09 Sirrus, Inc. Composite and laminate articles and polymerizable systems for producing the same
US9234107B2 (en) 2012-03-30 2016-01-12 Sirrus, Inc. Ink coating formulations and polymerizable systems for producing the same
US10047192B2 (en) 2012-06-01 2018-08-14 Sirrus, Inc. Optical material and articles formed therefrom
CN105008438B (zh) 2012-11-16 2019-10-22 拜奥福米克斯公司 塑料粘结体系及方法
CN105164797B (zh) 2012-11-30 2019-04-19 瑟拉斯公司 用于电子应用的复合组合物
WO2014110388A1 (en) 2013-01-11 2014-07-17 Bioformix Inc. Method to obtain methylene malonate via bis(hydroxymethyl) malonate pathway
US9315597B2 (en) 2014-09-08 2016-04-19 Sirrus, Inc. Compositions containing 1,1-disubstituted alkene compounds for preparing polymers having enhanced glass transition temperatures
US9416091B1 (en) 2015-02-04 2016-08-16 Sirrus, Inc. Catalytic transesterification of ester compounds with groups reactive under transesterification conditions
US10501400B2 (en) 2015-02-04 2019-12-10 Sirrus, Inc. Heterogeneous catalytic transesterification of ester compounds with groups reactive under transesterification conditions
US9334430B1 (en) 2015-05-29 2016-05-10 Sirrus, Inc. Encapsulated polymerization initiators, polymerization systems and methods using the same
US9217098B1 (en) 2015-06-01 2015-12-22 Sirrus, Inc. Electroinitiated polymerization of compositions having a 1,1-disubstituted alkene compound
US9518001B1 (en) 2016-05-13 2016-12-13 Sirrus, Inc. High purity 1,1-dicarbonyl substituted-1-alkenes and methods for their preparation
US10196481B2 (en) 2016-06-03 2019-02-05 Sirrus, Inc. Polymer and other compounds functionalized with terminal 1,1-disubstituted alkene monomer(s) and methods thereof
US10428177B2 (en) 2016-06-03 2019-10-01 Sirrus, Inc. Water absorbing or water soluble polymers, intermediate compounds, and methods thereof
US9617377B1 (en) 2016-06-03 2017-04-11 Sirrus, Inc. Polyester macromers containing 1,1-dicarbonyl-substituted 1 alkenes
US9567475B1 (en) 2016-06-03 2017-02-14 Sirrus, Inc. Coatings containing polyester macromers containing 1,1-dicarbonyl-substituted 1 alkenes
CN111056955B (zh) * 2019-12-16 2021-05-25 中国科学院大连化学物理研究所 一种环己烯制备己二胺的方法
CN111138255B (zh) * 2019-12-16 2021-06-22 中国科学院大连化学物理研究所 一种环己烯制备己二醛的工艺

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US2733270A (en) * 1956-01-31 Preparation of aldehydes
GB709450A (en) * 1950-10-09 1954-05-26 Du Pont Preparation of adipaldehyde
US3145232A (en) * 1959-11-03 1964-08-18 Monsanto Co Ozonization and reduction of unsaturated organic compounds
US3637721A (en) * 1970-06-25 1972-01-25 Inmont Corp Process for producing aldehydes by ozonizing and reducing certain aromatic and heterocyclic compounds containing carbon-to-carbon unsaturation
US3705922A (en) * 1970-08-11 1972-12-12 United States Steel Corp Process for the preparation of glyoxylic acid methyl hemiacetal
NL171808C (nl) * 1971-02-19 1983-05-16 Snia Viscosa Werkwijze voor het ozoniseren van alkenen.
DE2514001A1 (de) * 1975-03-29 1976-10-07 Basf Ag Verfahren zur herstellung von glyoxalmonoacetalen
SU590314A1 (ru) * 1975-12-11 1978-01-30 Институт Химии Башкирского Филиала Ан Ссср Способ получени олигомерных (цис-1,4-полидиен-1,3)-гликолей
DE3346266A1 (de) * 1983-12-21 1985-07-11 Lentia Gmbh Verfahren zur herstelung von glyoxal, alkylglyoxalen und von deren acetalen

Also Published As

Publication number Publication date
IE57650B1 (en) 1993-02-10
EP0147593A2 (de) 1985-07-10
ZA849894B (en) 1985-08-28
IL73933A0 (en) 1985-03-31
AT380008B (de) 1986-03-25
ES538965A0 (es) 1986-04-16
HUT36444A (en) 1985-09-30
HU198437B (en) 1989-10-30
DE3401672A1 (de) 1985-09-26
JPS6361296B2 (US06373033-20020416-M00071.png) 1988-11-28
NZ210517A (en) 1988-01-08
KR850004564A (ko) 1985-07-25
ATA450083A (de) 1985-08-15
IE843164L (en) 1985-06-23
ES8606234A1 (es) 1986-04-16
IL73933A (en) 1989-02-28
DE3481414D1 (de) 1990-04-05
EP0147593B1 (de) 1990-02-28
JPS60156635A (ja) 1985-08-16
KR920000444B1 (ko) 1992-01-14
AU3703684A (en) 1985-07-04
ATE50555T1 (de) 1990-03-15
GR81086B (en) 1985-01-09
AU572246B2 (en) 1988-05-05
EP0147593A3 (en) 1986-06-04
US4769464A (en) 1988-09-06

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