CA1211433A - Precipitation of xanthan gum - Google Patents
Precipitation of xanthan gumInfo
- Publication number
- CA1211433A CA1211433A CA000405227A CA405227A CA1211433A CA 1211433 A CA1211433 A CA 1211433A CA 000405227 A CA000405227 A CA 000405227A CA 405227 A CA405227 A CA 405227A CA 1211433 A CA1211433 A CA 1211433A
- Authority
- CA
- Canada
- Prior art keywords
- solution
- xanthan gum
- solvent
- amount
- ipa
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920001285 xanthan gum Polymers 0.000 title claims abstract description 26
- 239000000230 xanthan gum Substances 0.000 title claims abstract description 21
- 229940082509 xanthan gum Drugs 0.000 title claims abstract description 21
- 235000010493 xanthan gum Nutrition 0.000 title claims abstract description 21
- 238000001556 precipitation Methods 0.000 title claims abstract description 10
- 150000001768 cations Chemical class 0.000 claims abstract description 16
- 239000000243 solution Substances 0.000 claims abstract description 12
- 239000003960 organic solvent Substances 0.000 claims abstract description 8
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 6
- 239000007864 aqueous solution Substances 0.000 claims abstract description 4
- 230000001376 precipitating effect Effects 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 21
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical group CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 17
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 12
- 239000002904 solvent Substances 0.000 claims description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 10
- 239000011575 calcium Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 8
- 235000013405 beer Nutrition 0.000 claims description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 3
- 229910052791 calcium Inorganic materials 0.000 claims description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 2
- 229910052749 magnesium Inorganic materials 0.000 claims description 2
- 239000011777 magnesium Substances 0.000 claims description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 2
- 150000001342 alkaline earth metals Chemical class 0.000 claims 2
- 229910052725 zinc Inorganic materials 0.000 claims 2
- 239000011701 zinc Substances 0.000 claims 2
- -1 alka-line earth metal cations Chemical class 0.000 claims 1
- 150000002576 ketones Chemical class 0.000 claims 1
- GJCOSYZMQJWQCA-UHFFFAOYSA-N 9H-xanthene Chemical compound C1=CC=C2CC3=CC=CC=C3OC2=C1 GJCOSYZMQJWQCA-UHFFFAOYSA-N 0.000 abstract description 5
- 235000010633 broth Nutrition 0.000 description 31
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Inorganic materials [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 11
- 150000003839 salts Chemical class 0.000 description 9
- 238000011084 recovery Methods 0.000 description 6
- 239000011734 sodium Substances 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 229920000447 polyanionic polymer Polymers 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 description 3
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 3
- 210000000056 organ Anatomy 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 159000000007 calcium salts Chemical class 0.000 description 2
- MCWXGJITAZMZEV-UHFFFAOYSA-N dimethoate Chemical compound CNC(=O)CSP(=S)(OC)OC MCWXGJITAZMZEV-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 102000007469 Actins Human genes 0.000 description 1
- 108010085238 Actins Proteins 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
- 241000518994 Conta Species 0.000 description 1
- 241000282326 Felis catus Species 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 101100120538 Rattus norvegicus Fos gene Proteins 0.000 description 1
- HFCYZXMHUIHAQI-UHFFFAOYSA-N Thidiazuron Chemical compound C=1C=CC=CC=1NC(=O)NC1=CN=NS1 HFCYZXMHUIHAQI-UHFFFAOYSA-N 0.000 description 1
- 241000589634 Xanthomonas Species 0.000 description 1
- 241000589636 Xanthomonas campestris Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- JLDSOYXADOWAKB-UHFFFAOYSA-N aluminium nitrate Inorganic materials [Al+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O JLDSOYXADOWAKB-UHFFFAOYSA-N 0.000 description 1
- 159000000013 aluminium salts Chemical class 0.000 description 1
- 229910000329 aluminium sulfate Inorganic materials 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- UDGHXQPQKQPSBB-BOXHHOBZSA-N bepotastine besylate Chemical compound OS(=O)(=O)C1=CC=CC=C1.C1CN(CCCC(=O)O)CCC1O[C@H](C=1N=CC=CC=1)C1=CC=C(Cl)C=C1 UDGHXQPQKQPSBB-BOXHHOBZSA-N 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M potassium chloride Inorganic materials [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- XTUSEBKMEQERQV-UHFFFAOYSA-N propan-2-ol;hydrate Chemical compound O.CC(C)O XTUSEBKMEQERQV-UHFFFAOYSA-N 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- CMXPERZAMAQXSF-UHFFFAOYSA-M sodium;1,4-bis(2-ethylhexoxy)-1,4-dioxobutane-2-sulfonate;1,8-dihydroxyanthracene-9,10-dione Chemical compound [Na+].O=C1C2=CC=CC(O)=C2C(=O)C2=C1C=CC=C2O.CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC CMXPERZAMAQXSF-UHFFFAOYSA-M 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
- C12P19/06—Xanthan, i.e. Xanthomonas-type heteropolysaccharides
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB8119707 | 1981-06-25 | ||
| GB8119707 | 1981-06-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1211433A true CA1211433A (en) | 1986-09-16 |
Family
ID=10522822
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000405227A Expired CA1211433A (en) | 1981-06-25 | 1982-06-15 | Precipitation of xanthan gum |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP0068706B1 (enEXAMPLES) |
| JP (1) | JPS585301A (enEXAMPLES) |
| AU (1) | AU8498382A (enEXAMPLES) |
| CA (1) | CA1211433A (enEXAMPLES) |
| DE (1) | DE3261454D1 (enEXAMPLES) |
| DK (1) | DK283782A (enEXAMPLES) |
| ES (1) | ES8403523A1 (enEXAMPLES) |
| FI (1) | FI71169C (enEXAMPLES) |
| GR (1) | GR75953B (enEXAMPLES) |
| PT (1) | PT75059B (enEXAMPLES) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1308097C (en) * | 1986-10-28 | 1992-09-29 | John J. Cannon | Polysaccharide isolation process |
| JP3741734B2 (ja) | 1994-06-30 | 2006-02-01 | 信越化学工業株式会社 | キサンタンガムの回収精製方法 |
| JP3228315B2 (ja) * | 1993-04-23 | 2001-11-12 | 信越化学工業株式会社 | キサンタンガムの汚染生菌数を減少させる方法 |
| CA2369294A1 (en) * | 1999-04-09 | 2000-10-19 | Monsanto Company | Xanthan viscosified compositions and preparation thereof |
| US6881838B2 (en) | 2002-05-21 | 2005-04-19 | A.E. Staley Manufacturing Company | Polysaccharide gum and process for its manufacture |
| WO2007007562A1 (ja) | 2005-07-08 | 2007-01-18 | Morishita Jintan Co., Ltd. | ビフィドバクテリウム属の微生物が産生する多糖 |
| CN101662946B (zh) | 2007-04-24 | 2013-06-12 | Fmc有限公司 | 共沉淀角叉菜胶/黄原胶组合物及其制备方法 |
| US9050357B2 (en) | 2010-03-08 | 2015-06-09 | Cp Kelco U.S., Inc. | Compositions and methods for producing consumables for patients with dysphagia |
| JP5737646B2 (ja) | 2010-03-24 | 2015-06-17 | 森下仁丹株式会社 | 抗アレルギー剤 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3232929A (en) * | 1960-05-25 | 1966-02-01 | William H Mcneely | Process for producing xanthomonas hydrophilic colloid |
| US3382229A (en) * | 1963-04-11 | 1968-05-07 | Exxon Production Research Co | Polysaccharide recovery process |
| US3338792A (en) * | 1963-07-30 | 1967-08-29 | Exxon Production Research Co | Fermentation process utilizing pathogenic organisms |
| US3355447A (en) * | 1964-04-28 | 1967-11-28 | Kelco Co | Treatment of xanthomonas hydrophilic colloid and resulting product |
| FR1526105A (fr) * | 1967-04-03 | 1968-05-24 | Melle Usines Sa | Procédé de production de polysaccharides par fermentation |
| IE50263B1 (en) * | 1979-10-29 | 1986-03-19 | Tate & Lyle Patent Holdings | Recovery of xanthan gum |
-
1982
- 1982-06-15 FI FI822149A patent/FI71169C/fi not_active IP Right Cessation
- 1982-06-15 EP EP19820303089 patent/EP0068706B1/en not_active Expired
- 1982-06-15 CA CA000405227A patent/CA1211433A/en not_active Expired
- 1982-06-15 DE DE8282303089T patent/DE3261454D1/de not_active Expired
- 1982-06-16 PT PT7505982A patent/PT75059B/pt unknown
- 1982-06-18 AU AU84983/82A patent/AU8498382A/en not_active Abandoned
- 1982-06-22 ES ES513363A patent/ES8403523A1/es not_active Expired
- 1982-06-23 GR GR68534A patent/GR75953B/el unknown
- 1982-06-23 JP JP10698382A patent/JPS585301A/ja active Granted
- 1982-06-24 DK DK283782A patent/DK283782A/da not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| ES513363A0 (es) | 1983-08-01 |
| JPH0452281B2 (enEXAMPLES) | 1992-08-21 |
| GR75953B (enEXAMPLES) | 1984-08-02 |
| EP0068706B1 (en) | 1984-12-05 |
| ES8403523A1 (es) | 1983-08-01 |
| FI71169C (fi) | 1986-11-24 |
| DE3261454D1 (en) | 1985-01-17 |
| EP0068706A1 (en) | 1983-01-05 |
| PT75059B (en) | 1985-05-31 |
| FI822149L (fi) | 1982-12-26 |
| FI71169B (fi) | 1986-08-14 |
| FI822149A0 (fi) | 1982-06-15 |
| JPS585301A (ja) | 1983-01-12 |
| PT75059A (en) | 1982-07-01 |
| DK283782A (da) | 1982-12-26 |
| AU8498382A (en) | 1983-01-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |