CA1081256A - Purification de la dinotroaniline - Google Patents

Purification de la dinotroaniline

Info

Publication number
CA1081256A
CA1081256A CA307,403A CA307403A CA1081256A CA 1081256 A CA1081256 A CA 1081256A CA 307403 A CA307403 A CA 307403A CA 1081256 A CA1081256 A CA 1081256A
Authority
CA
Canada
Prior art keywords
nitrosamine
trifluralin
hcl
ppm
dinitroaniline
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA307,403A
Other languages
English (en)
Inventor
Richard F. Eizember
Kathleen R. Vogler
William N. Cannon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eli Lilly and Co
Original Assignee
Eli Lilly and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eli Lilly and Co filed Critical Eli Lilly and Co
Application granted granted Critical
Publication of CA1081256A publication Critical patent/CA1081256A/fr
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/84Purification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/44Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
    • C07C211/52Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring the carbon skeleton being further substituted by halogen atoms or by nitro or nitroso groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
CA307,403A 1977-07-18 1978-07-14 Purification de la dinotroaniline Expired CA1081256A (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US81655877A 1977-07-18 1977-07-18
US87883478A 1978-02-17 1978-02-17

Publications (1)

Publication Number Publication Date
CA1081256A true CA1081256A (fr) 1980-07-08

Family

ID=27124088

Family Applications (1)

Application Number Title Priority Date Filing Date
CA307,403A Expired CA1081256A (fr) 1977-07-18 1978-07-14 Purification de la dinotroaniline

Country Status (21)

Country Link
JP (1) JPS5822102B2 (fr)
AR (1) AR221846A1 (fr)
AU (1) AU516698B2 (fr)
BG (1) BG34182A3 (fr)
BR (1) BR7804599A (fr)
CA (1) CA1081256A (fr)
CS (1) CS203196B2 (fr)
DD (1) DD137222A5 (fr)
DE (1) DE2831119C2 (fr)
DK (1) DK152113C (fr)
ES (1) ES471821A1 (fr)
FR (1) FR2398044A1 (fr)
GB (1) GB1599930A (fr)
HU (1) HU182483B (fr)
IE (1) IE47127B1 (fr)
IL (1) IL55142A (fr)
IT (1) IT1097822B (fr)
MX (1) MX5203E (fr)
NL (1) NL189911C (fr)
PL (1) PL119759B1 (fr)
RO (1) RO75656A (fr)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3061492D1 (en) * 1979-05-21 1983-02-03 Hoechst Ag Process for the removal of nitrozation agents from nitrated aromatic compounds
DE2926947C2 (de) * 1979-07-04 1982-03-18 Hoechst Ag, 6000 Frankfurt Verfahren zur Entfernung von Nitrosierungsmittel (n) aus nitrierten aromatischen Verbindungen
DE3345157A1 (de) * 1983-12-14 1985-06-27 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von nitrosaminfreien n,n-disubstituierten nitroaromatischen aminen und deren stabilisierung gegen nitrosaminbildung
IT1195822B (it) * 1986-08-12 1988-10-27 I Pi Ci Spa Procedimento per la purificazione della trifluralina
IT1293450B1 (it) * 1997-07-14 1999-03-01 Finchimica Srl Procedimento per la purificazione di dinitroaniline.
CA2973331C (fr) * 2015-01-07 2019-10-22 Mitsubishi Hitachi Power Systems, Ltd. Procede et dispositif pour traiter un compose nitrose
CN109320424B (zh) * 2017-07-31 2021-12-21 江苏永安化工有限公司 一种二甲戊灵的纯化方法
CN116735760B (zh) * 2023-08-16 2024-02-09 山东道可化学有限公司 一种氟乐灵中n,n-二丙基亚硝胺的检测方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4134917A (en) * 1977-04-25 1979-01-16 American Cyanamid Company Method for the denitrosation of organic nitrosamines

Also Published As

Publication number Publication date
DE2831119A1 (de) 1979-02-08
PL119759B1 (en) 1982-01-30
CS203196B2 (en) 1981-02-27
BG34182A3 (en) 1983-07-15
PL208500A1 (pl) 1979-07-02
RO75656A (fr) 1981-04-20
HU182483B (en) 1984-01-30
NL189911C (nl) 1993-09-01
JPS5822102B2 (ja) 1983-05-06
DD137222A5 (de) 1979-08-22
MX5203E (es) 1983-04-25
AR221846A1 (es) 1981-03-31
DK152113B (da) 1988-02-01
IT1097822B (it) 1985-08-31
IL55142A0 (en) 1978-09-29
BR7804599A (pt) 1979-03-20
GB1599930A (en) 1981-10-07
AU516698B2 (en) 1981-06-18
ES471821A1 (es) 1979-10-01
IT7825724A0 (it) 1978-07-14
NL189911B (nl) 1993-04-01
JPS5422329A (en) 1979-02-20
DK319378A (da) 1979-01-19
DK152113C (da) 1988-06-20
IE47127B1 (en) 1983-12-28
FR2398044B1 (fr) 1980-10-31
FR2398044A1 (fr) 1979-02-16
IL55142A (en) 1981-06-29
NL7807576A (nl) 1979-01-22
DE2831119C2 (de) 1983-05-26
IE781430L (en) 1979-01-18
AU3805878A (en) 1980-01-17

Similar Documents

Publication Publication Date Title
US4185035A (en) Dinitroaniline purification with inorganic acid halides
CA1081256A (fr) Purification de la dinotroaniline
US4226789A (en) Removal of nitrosamines from denitroanilines by treatment with HCl
RU2127246C1 (ru) Способ получения дифторметана (варианты)
Ginsburg Concerning amines: their properties, preparation and reactions
US4127610A (en) Dinitroaniline purification with bromine and chlorine
US4123466A (en) Process for nitrating aromatic hydrocarbons
CA1057774A (fr) Purification de la dinitroaniline a l'aide de brome et de chlore
JPS5840940B2 (ja) ニトロソ化剤の除去方法
KR820000427B1 (ko) 디니트로아닐린 정제법
KR102176381B1 (ko) 니트로벤젠 제조로부터의 폐수의 후처리 방법
US9771291B2 (en) Process for working up waste water from nitrobenzene preparation
CA1144943A (fr) Methode pour debarrasser les composes aromatiques nitres, des agents de nitrosation
WO1999058489A1 (fr) Procede permettant d'eliminer des composes n-nitroso de compositions organo-amines, notamment d'herbicides a la dinitroaniline
KR820000056B1 (ko) 브롬과 염소로서 디니트로 아닐린을 정제하는 방법
KR820000052B1 (ko) 무기산 할라이드로 디니트로 아닐린을 정제하는 방법
CA2110329C (fr) Methode de preparation d'ethalfluraline
US4469890A (en) Preparation of ortho-aminobenzotrifluoride
EP0254009B1 (fr) Procédé de purification d'herbicides de dinitroaniline
CN110498461A (zh) 降解卤代对羟基苯胺或邻羟基苯胺的方法
Nonomura et al. Cyanide formation in oxime blocked isocyanates of cation electro‐deposited paints
US3835178A (en) Process for the production of mixtures consisting of benzyl cyanide and {62 -phenylethylamine
Jackson et al. Formation of by-products in the nitration of pentachlorobenzene
Chaykovskiy et al. Interaction of substituted aril iodide with protonic acid
McCullough et al. The Reactivity of Atoms and Groups in Organic Compounds: Second Contribution on the Carbon-chlorine Bond: the Rates of the Reactions of Certain Derivatives of Diphenylchloromethane with Ethyl Alcohol and with Isopropyl Alcohol. IV

Legal Events

Date Code Title Description
MKEX Expiry