BRPI0919647B1 - processo para preparação de acroleína, de ácido acrílico e de um polímero - Google Patents

processo para preparação de acroleína, de ácido acrílico e de um polímero Download PDF

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Publication number
BRPI0919647B1
BRPI0919647B1 BRPI0919647-1A BRPI0919647A BRPI0919647B1 BR PI0919647 B1 BRPI0919647 B1 BR PI0919647B1 BR PI0919647 A BRPI0919647 A BR PI0919647A BR PI0919647 B1 BRPI0919647 B1 BR PI0919647B1
Authority
BR
Brazil
Prior art keywords
glycerol
acrolein
phase
reaction
acrylic acid
Prior art date
Application number
BRPI0919647-1A
Other languages
English (en)
Portuguese (pt)
Inventor
Guido Stochniol
Franz-Felix Kuppinger
Götz Baumgarten
Original Assignee
Evonik Degussa Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Degussa Gmbh filed Critical Evonik Degussa Gmbh
Publication of BRPI0919647A2 publication Critical patent/BRPI0919647A2/pt
Publication of BRPI0919647B1 publication Critical patent/BRPI0919647B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/79—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/52—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition by dehydration and rearrangement involving two hydroxy groups in the same molecule
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/786—Separation; Purification; Stabilisation; Use of additives by membrane separation process, e.g. pervaporation, perstraction, reverse osmosis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
BRPI0919647-1A 2008-12-09 2009-11-03 processo para preparação de acroleína, de ácido acrílico e de um polímero BRPI0919647B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102008060888A DE102008060888A1 (de) 2008-12-09 2008-12-09 Verfahren zur Herstellung von Acrolein umfassend die Aufarbeitung einer Rohglycerin-Phase
DE102008060888.2 2008-12-09
PCT/EP2009/064500 WO2010066513A1 (de) 2008-12-09 2009-11-03 Verfahren zur herstellung von acrolein umfassend die aufarbeitung einer rohglycerin-phase

Publications (2)

Publication Number Publication Date
BRPI0919647A2 BRPI0919647A2 (pt) 2015-12-08
BRPI0919647B1 true BRPI0919647B1 (pt) 2018-11-06

Family

ID=41668419

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0919647-1A BRPI0919647B1 (pt) 2008-12-09 2009-11-03 processo para preparação de acroleína, de ácido acrílico e de um polímero

Country Status (8)

Country Link
US (1) US8524945B2 (https=)
EP (1) EP2356088B1 (https=)
JP (1) JP2012511505A (https=)
CN (1) CN102245551A (https=)
BR (1) BRPI0919647B1 (https=)
DE (1) DE102008060888A1 (https=)
WO (1) WO2010066513A1 (https=)
ZA (1) ZA201102268B (https=)

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DE102006039203B4 (de) 2006-08-22 2014-06-18 Evonik Degussa Gmbh Verfahren zur Herstellung von durch Kristallisation gereinigter Acrylsäure aus Hydroxypropionsäure sowie Vorrichtung dazu
FR2953829B1 (fr) 2009-12-14 2011-12-09 Arkema France Procede de fabrication d'acroleine et/ou d'acide acrylique a partir de glycerol
US10676664B2 (en) * 2012-03-29 2020-06-09 Axel R. Johnson Increased availability and reduced costs for viscoelastic surfactants used in hydrofracturing fluids
US9725641B2 (en) * 2012-03-29 2017-08-08 Axel R. Johnson Methods fluids by producing and employing oil and gas well drilling and completion fluids as well as hydraulic fracturing fluids employing triglyceride processing by products and propylene glycol recovered from aircraft deicing operations
DE102013000602A1 (de) 2013-01-16 2014-07-17 Evonik Industries Ag Verfahren zur Herstellung von Acrylsäure
DE102013217386A1 (de) 2013-09-02 2015-03-05 Evonik Industries Ag Verfahren zur Herstellung von Acrylsäure
JP6228246B2 (ja) 2015-03-03 2017-11-08 エボニック デグサ ゲーエムベーハーＥｖｏｎｉｋ Ｄｅｇｕｓｓａ ＧｍｂＨ エテンのオリゴマー化に使用される不均一系触媒の再生
PL3255029T3 (pl) 2016-06-10 2019-04-30 Evonik Degussa Gmbh Oligomeryzacja etenu w warunkach nadkrytycznych
EP3266757B1 (de) 2016-07-08 2019-12-25 Evonik Operations GmbH Herstellung von zumindest 1-hexen und octen aus ethen
US10227279B2 (en) 2016-09-12 2019-03-12 Evonik Degussa Gmbh Dehydrogenation of LPG or NGL and flexible utilization of the olefins thus obtained
US10850261B2 (en) 2018-03-14 2020-12-01 Evonik Operations Gmbh Oligomerization catalyst and process for the production thereof
US11253844B2 (en) 2018-03-14 2022-02-22 Evonik Operations Gmbh Oligomerization catalyst and process for the production thereof
US10882028B2 (en) 2018-03-14 2021-01-05 Evonik Operations Gmbh Ni-containing catalyst for the oligomerization of olefins
US10882027B2 (en) 2018-03-14 2021-01-05 Evonik Operations Gmbh Process for producing an oligomerization catalyst
US10633302B2 (en) 2018-07-25 2020-04-28 Evonik Operations Gmbh Process for oligomerization of butene with determination of the proportion of acidic catalysis
EP3680224B1 (de) 2019-01-08 2023-05-24 Evonik Operations GmbH Verfahren zur entfernung mehrfach ungesättigter kohlenwasserstoffe aus c4-kohlenwasserstoffströmen in anwesenheit von mercaptanen, disulfiden und c5-kohlenwasserstoffen
US11186782B2 (en) 2019-01-08 2021-11-30 Evonik Operations Gmbh Catalyst and process for removing mercaptans from hydrocarbon streams
CN110642674B (zh) * 2019-10-15 2022-04-26 宁波环洋新材料股份有限公司 一种在生物柴油副产粗甘油的精制过程中联产丙烯醛的方法

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CA1329782C (en) * 1988-08-09 1994-05-24 Thomas Buenemann Process for purifying crude glycerol
US5250182A (en) 1992-07-13 1993-10-05 Zenon Environmental Inc. Membrane-based process for the recovery of lactic acid and glycerol from a "corn thin stillage" stream
DE4238493C1 (de) * 1992-11-14 1994-04-21 Degussa Verfahren zur Herstellung von Acrolein und dessen Verwendung
DE4328407C1 (de) 1993-08-24 1994-09-01 Sartorius Gmbh Durch Einwirkung von Hitze sterilisierbarer Wickelmodul
DE19636767A1 (de) * 1996-09-10 1998-03-12 Basf Ag Verfahren zur Herstellung von aliphatischen alpha, omega-Aminonitrilen
SG81982A1 (en) 1998-05-18 2001-07-24 Nippon Catalytic Chem Ind Method for production of acrolein and acrylic acid
DE19829747A1 (de) 1998-07-03 2000-01-05 Huels Infracor Gmbh Entaluminierter Katalysatorträger, Verfahren zur Herstellung des Katalysatorträgers und Verfahren zur Hydratisierung von C2- oder C3-Olefinen mit Wasser in Gegenwart eines Katalysators, der aus diesem mit Säure getränkten Katalysatorträger besteht
DE19838425A1 (de) * 1998-08-24 2000-03-02 Degussa Verfahren zur Abtrennung mehrfunktioneller Alkohole von wasserlöslichen Salzen aus wäßrigen Systemen
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DE10138150A1 (de) * 2001-08-03 2003-02-13 Basf Ag Verfahren zur Herstellung wasserabsorbierender Harze
DE10142620A1 (de) 2001-08-31 2003-03-20 Degussa Ammoximation von Ketonen und Aufarbeitung durch Pervaporation/Dampfpermeation
DE10153546A1 (de) 2001-10-30 2003-05-22 Degussa Direktsynthese von Wasserstoffperoxid und deren Integration in Oxidationsprozesse
ATE391116T1 (de) 2001-12-14 2008-04-15 Stockhausen Chem Fab Gmbh Verfahren zur herstellung von acrylsäure
US7141683B2 (en) 2002-05-02 2006-11-28 Degussa Ag Process for the epoxidation of olefins
DE10241762A1 (de) 2002-09-10 2004-03-18 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von wasserfreiem tert.-Butanol
US6838572B2 (en) 2002-09-30 2005-01-04 Degussa Ag Process for the epoxidation of olefins
US7722847B2 (en) 2002-09-30 2010-05-25 Evonik Degussa Gmbh Aqueous hydrogen peroxide solutions and method of making same
US7169945B2 (en) 2002-11-26 2007-01-30 Degussa Ag Process for the epoxidation of olefins
US6878836B2 (en) 2003-06-18 2005-04-12 Degussa Ag Process for the epoxidation of propene
DE10335510A1 (de) 2003-07-31 2005-03-10 Stockhausen Chem Fab Gmbh Beschichteter Katalysator-Trägerkörper
DE102004030943B4 (de) 2004-06-26 2013-10-02 Evonik Oxeno Gmbh Verfahren zur Herstellung von tert.-Butanol aus Isobuten-haltigen Kohlenwasserstoffgemischen
US7501064B2 (en) 2005-01-06 2009-03-10 Eet Integrated electro-pressure membrane deionization system
BRPI0606520A2 (pt) 2005-01-06 2009-06-30 Telik Inc tripeptìdeo e tetrapeptìdeo tioéteres
FR2882052B1 (fr) * 2005-02-15 2007-03-23 Arkema Sa Procede de deshydratation du glycerol en acroleine
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TWI522092B (zh) * 2005-02-28 2016-02-21 贏創德固賽有限責任公司 丙烯酸和基於可再生原料之吸水聚合物結構及二者之製備方法
US20090068440A1 (en) * 2005-06-20 2009-03-12 Gunther Bub Production of acrolein, acrylic acid and water-absorbent polymer structures made from glycerine
DE102005046250B4 (de) 2005-09-27 2020-10-08 Evonik Operations Gmbh Anlage zur Abtrennung von organischen Übergangsmetallkomplexkatalysatoren
DE102006003618A1 (de) 2006-01-26 2007-08-02 Oxeno Olefinchemie Gmbh Verfahren zur Abtrennung von Metall-Komplexkatalysatoren aus Telomerisationsgemischen
GB2437516A (en) * 2006-04-26 2007-10-31 Bai Leng Method and apparatus for purifying glycerine using filter membranes and a deionisation means
DE102006039205A1 (de) * 2006-08-22 2008-03-20 Stockhausen Gmbh Auf nachwachsenden Rohstoffen basierende Acrylsäure und wasserabsorbierende Polymergebilde sowie Verfahren zu deren Herstellung mittels Dehydratisierung
DE102006054519A1 (de) * 2006-11-20 2008-05-21 Evonik Degussa Gmbh Verfahren zur Herstellung von Fettsäurealkylestern und Acrolein aus Triglyceriden
DE102007004350A1 (de) 2007-01-29 2008-07-31 Evonik Degussa Gmbh Verfahren zur Regenerierung eines Katalysators
DE102007004351A1 (de) * 2007-01-29 2008-07-31 Evonik Degussa Gmbh Neue Katalysatoren und Verfahren zur Dehydratisierung von Glycerin
DE102007019379A1 (de) 2007-04-23 2008-10-30 Bayer Technology Services Gmbh Verfahren zur Aufreinigung von Produktgemischen aus Umesterungsreaktionen

Also Published As

Publication number Publication date
CN102245551A (zh) 2011-11-16
ZA201102268B (en) 2011-12-28
EP2356088B1 (de) 2018-09-26
EP2356088A1 (de) 2011-08-17
BRPI0919647A2 (pt) 2015-12-08
JP2012511505A (ja) 2012-05-24
US20110275777A1 (en) 2011-11-10
WO2010066513A1 (de) 2010-06-17
US8524945B2 (en) 2013-09-03
DE102008060888A1 (de) 2010-06-10

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Legal Events

Date Code Title Description
B25A Requested transfer of rights approved

Owner name: EVONIK DEGUSSA GMBH (DE)

B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 03/11/2009, OBSERVADAS AS CONDICOES LEGAIS.

B25D Requested change of name of applicant approved

Owner name: EVONIK OPERATIONS GMBH (DE)

B25A Requested transfer of rights approved

Owner name: EVONIK SUPERABSORBER GMBH (DE)

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: EXTINTA A PATENTE, NOS TERMOS DO ARTIGO 86, DA LPI, E ARTIGO 14 DA PORTARIA 52/2023, REFERENTE AO NAO RECOLHIMENTO DA 16A RETRIBUICAO ANUAL. PARA FINS DE RESTAURACAO CONFORME ARTIGO 87, DA LPI 9.279, E ARTIGO 15, DA PORTARIA 52/2023, VIDE PARECER.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2853 DE 09-09-2025 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.