BR9812895A - Processo para a preparação de derivados de triazolintiona - Google Patents
Processo para a preparação de derivados de triazolintionaInfo
- Publication number
- BR9812895A BR9812895A BR9812895-7A BR9812895A BR9812895A BR 9812895 A BR9812895 A BR 9812895A BR 9812895 A BR9812895 A BR 9812895A BR 9812895 A BR9812895 A BR 9812895A
- Authority
- BR
- Brazil
- Prior art keywords
- derivatives
- formula
- preparation
- triazolinthion
- diluent
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- 239000003085 diluting agent Substances 0.000 abstract 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 abstract 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000001728 carbonyl compounds Chemical class 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 235000019253 formic acid Nutrition 0.000 abstract 1
- 150000002429 hydrazines Chemical class 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- ZNNZYHKDIALBAK-UHFFFAOYSA-M potassium thiocyanate Chemical compound [K+].[S-]C#N ZNNZYHKDIALBAK-UHFFFAOYSA-M 0.000 abstract 1
- 229940116357 potassium thiocyanate Drugs 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
- C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
- C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
- C07D249/10—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D249/12—Oxygen or sulfur atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Thiazole And Isothizaole Compounds (AREA)
Abstract
Patente de Invenção: <B>"PROCESSO PARA A PREPARAçãO DE DERIVADOS DE TRIAZOLINTIONA"<D>. A invenção refere-se a um novo processo para a produção de derivados de triazolintionas da fórmula (I), em que R^ 1^ e R^ 2^ têm os significados dados na descrição. O processo consiste em a) reação dos derivados de hidrazina da fórmula (II) com compostos de carbonila da fórmula (III), em que R^ 3^ e R^ 4^ têm os significados dados no relatório descritivo, com tiocianato de potássio, de sódio ou de amónio, opcionalmente na presença de um diluente e/ou de um ácido; e b) reação dos derivados de triazolidintiona da fórmula (V) assim produzidos com ácido fórmico, opcionalmente na presença de um catalisador e/ou de um diluente. Esses derivados de triazolidintiona da fórmula (V) são compostos novos.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19744401A DE19744401A1 (de) | 1997-10-08 | 1997-10-08 | Verfahren zur Herstellung von Triazolinthion-Derivaten |
| PCT/EP1998/006111 WO1999018086A1 (de) | 1997-10-08 | 1998-09-25 | Verfahren zur herstellung von triazolinthion-derivaten |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR9812895A true BR9812895A (pt) | 2000-08-08 |
| BR9812895B1 BR9812895B1 (pt) | 2009-05-05 |
Family
ID=7844918
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI9812895-7A BR9812895B1 (pt) | 1997-10-08 | 1998-09-25 | derivados de triazolintiona, bem como processo para sua preparação. |
Country Status (15)
| Country | Link |
|---|---|
| US (2) | US6271389B1 (pt) |
| EP (1) | EP1021420B1 (pt) |
| JP (1) | JP4028172B2 (pt) |
| KR (1) | KR100555367B1 (pt) |
| CN (2) | CN1286818C (pt) |
| AT (1) | ATE235473T1 (pt) |
| AU (1) | AU1484799A (pt) |
| BR (1) | BR9812895B1 (pt) |
| DE (2) | DE19744401A1 (pt) |
| DK (1) | DK1021420T3 (pt) |
| ES (1) | ES2191357T3 (pt) |
| HU (1) | HU228840B1 (pt) |
| IL (1) | IL134875A (pt) |
| MX (1) | MX212965B (pt) |
| WO (1) | WO1999018086A1 (pt) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19917617A1 (de) * | 1999-04-19 | 2000-10-26 | Bayer Ag | -(-)Enantiomeres des 2-[2-(1-Chlor-cyclopropyl)-3-(2-chlorphenyl) 2-hydroxy-propyl]-2,4-dihydro-[1,2,4]-triazol-3-thions |
| US7247408B2 (en) | 1999-11-23 | 2007-07-24 | Sion Power Corporation | Lithium anodes for electrochemical cells |
| US20070221265A1 (en) | 2006-03-22 | 2007-09-27 | Sion Power Corporation | Rechargeable lithium/water, lithium/air batteries |
| DE19961603A1 (de) * | 1999-12-21 | 2001-06-28 | Bayer Ag | Verfahren zur Herstellung eines Triazolinthion-Derivates |
| DE10233171A1 (de) * | 2002-07-22 | 2004-02-12 | Bayer Cropscience Ag | Kristallmodifikation II des 2-[2-(Chlor-cyclopropyl)-3-(2-chlorphenyl)-2-hydroxy-propyl]-2,4dihydro-3H-1,2,4-triazol-3-thions |
| JP2010513458A (ja) | 2006-12-19 | 2010-04-30 | ファイザー・プロダクツ・インク | Ｈ−ｐｇｄｓの阻害剤としてのニコチンアミド誘導体、およびプロスタグランジンｄ２の仲介による疾患を治療するためのその使用 |
| EP2234488A2 (de) * | 2007-12-19 | 2010-10-06 | Basf Se | Azolylmethyloxirane, ihre verwendung sowie sie enthaltende mittel |
| WO2009077497A2 (de) * | 2007-12-19 | 2009-06-25 | Basf Se | Azolylmethyloxirane, ihre verwendung sowie sie enthaltende mittel |
| WO2009077471A2 (de) * | 2007-12-19 | 2009-06-25 | Basf Se | Azolylmethyloxirane, ihre verwendung sowie sie enthaltende mittel |
| CN101952279A (zh) * | 2007-12-19 | 2011-01-19 | 巴斯夫欧洲公司 | 唑基甲基环氧乙烷、其应用和包含它们的组合物 |
| WO2010142779A1 (en) | 2009-06-12 | 2010-12-16 | Basf Se | Antifungal 1,2,4-triazolyl derivatives having a 5- sulfur substituent |
| WO2010146113A1 (en) | 2009-06-18 | 2010-12-23 | Basf Se | Antifungal 1, 2, 4-triazolyl derivatives having a 5- sulfur substituent |
| US20120108422A1 (en) | 2009-06-18 | 2012-05-03 | Basf Se | Antifungal 1,2,4-triazolyl Derivatives |
| US20120088660A1 (en) | 2009-06-18 | 2012-04-12 | Basf Se | Antifungal 1,2,4-triazolyl Derivatives |
| WO2010149758A1 (en) | 2009-06-25 | 2010-12-29 | Basf Se | Antifungal 1, 2, 4-triazolyl derivatives |
| CN102753536A (zh) | 2009-12-18 | 2012-10-24 | 巴斯夫欧洲公司 | 制备三唑啉硫酮衍生物及其中间体的方法 |
| WO2012146535A1 (en) | 2011-04-28 | 2012-11-01 | Basf Se | Process for the preparation of 2-substituted 2,4-dihydro-[1,2,4]triazole-3-thiones |
| WO2012146598A1 (en) | 2011-04-28 | 2012-11-01 | Basf Se | Process for the preparation of 2-substituted 4-amino-2,4-dihydro-[1,2,4]triazole-3-thiones |
| CN105949137B (zh) | 2016-07-15 | 2019-01-29 | 泸州东方农化有限公司 | 一种丙硫菌唑及其光学活性体的合成方法和中间体 |
| CA3092748C (en) * | 2018-03-06 | 2024-02-13 | Upl Ltd | A process for preparation of fungicidally active triazole compounds |
| CN110218197B (zh) * | 2019-06-25 | 2022-10-21 | 芮城县斯普伦迪生物工程有限公司 | 利用微通道反应器连续化生产丙硫菌唑的方法及微通道系统 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS52113972A (en) * | 1976-03-17 | 1977-09-24 | Mitsubishi Chem Ind Ltd | Triazolidine derivatives, their preparation, and herbicidal compositio n containing the same |
| DE3812967A1 (de) | 1987-06-24 | 1989-01-05 | Bayer Ag | Azolylmethyl-cyclopropyl-derivate |
| DE4030039A1 (de) | 1990-09-22 | 1992-03-26 | Bayer Ag | Verfahren zur herstellung von 2-(1-chlor-cyclopropyl)-1- (2-chlor-phenyl)-3-(1,2,4-triazol-1-yl- propan-2-ol |
| DE19528046A1 (de) * | 1994-11-21 | 1996-05-23 | Bayer Ag | Triazolyl-Derivate |
| DE19601189A1 (de) | 1996-01-15 | 1997-07-17 | Degussa | Verfahren zur Herstellung von 1,2,4-Triazolin-3(2H)-onen |
| EP0784053A1 (de) * | 1996-01-15 | 1997-07-16 | Degussa Aktiengesellschaft | Verfahren zur Herstellung von Triazolinonherbiziden |
-
1997
- 1997-10-08 DE DE19744401A patent/DE19744401A1/de not_active Withdrawn
-
1998
- 1998-09-25 CN CNB031368727A patent/CN1286818C/zh not_active Expired - Lifetime
- 1998-09-25 HU HU0100103A patent/HU228840B1/hu not_active IP Right Cessation
- 1998-09-25 CN CN98809959A patent/CN1121397C/zh not_active Expired - Lifetime
- 1998-09-25 JP JP2000514897A patent/JP4028172B2/ja not_active Expired - Lifetime
- 1998-09-25 ES ES98958843T patent/ES2191357T3/es not_active Expired - Lifetime
- 1998-09-25 DK DK98958843T patent/DK1021420T3/da active
- 1998-09-25 KR KR20007003071A patent/KR100555367B1/ko not_active IP Right Cessation
- 1998-09-25 AT AT98958843T patent/ATE235473T1/de active
- 1998-09-25 US US09/509,889 patent/US6271389B1/en not_active Expired - Lifetime
- 1998-09-25 AU AU14847/99A patent/AU1484799A/en not_active Abandoned
- 1998-09-25 DE DE59807672T patent/DE59807672D1/de not_active Expired - Lifetime
- 1998-09-25 EP EP98958843A patent/EP1021420B1/de not_active Expired - Lifetime
- 1998-09-25 BR BRPI9812895-7A patent/BR9812895B1/pt active IP Right Grant
- 1998-09-25 WO PCT/EP1998/006111 patent/WO1999018086A1/de active IP Right Grant
- 1998-09-25 IL IL13487598A patent/IL134875A/xx not_active IP Right Cessation
-
2000
- 2000-04-07 MX MXPA00003448 patent/MX212965B/es unknown
- 2000-12-28 US US09/750,589 patent/US6372916B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE19744401A1 (de) | 1999-04-15 |
| EP1021420A1 (de) | 2000-07-26 |
| CN1286818C (zh) | 2006-11-29 |
| IL134875A (en) | 2003-10-31 |
| KR100555367B1 (ko) | 2006-03-03 |
| BR9812895B1 (pt) | 2009-05-05 |
| ATE235473T1 (de) | 2003-04-15 |
| HUP0100103A3 (en) | 2002-08-28 |
| CN1515558A (zh) | 2004-07-28 |
| IL134875A0 (en) | 2001-05-20 |
| DE59807672D1 (de) | 2003-04-30 |
| MXPA00003448A (es) | 2000-11-01 |
| AU1484799A (en) | 1999-04-27 |
| JP4028172B2 (ja) | 2007-12-26 |
| DK1021420T3 (da) | 2003-07-21 |
| EP1021420B1 (de) | 2003-03-26 |
| HU228840B1 (en) | 2013-06-28 |
| US6372916B2 (en) | 2002-04-16 |
| US20010056187A1 (en) | 2001-12-27 |
| ES2191357T3 (es) | 2003-09-01 |
| MX212965B (es) | 2003-02-13 |
| CN1274348A (zh) | 2000-11-22 |
| CN1121397C (zh) | 2003-09-17 |
| KR20010024242A (ko) | 2001-03-26 |
| US6271389B1 (en) | 2001-08-07 |
| HUP0100103A2 (hu) | 2001-06-28 |
| JP2001519336A (ja) | 2001-10-23 |
| WO1999018086A1 (de) | 1999-04-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 28/07/2009, OBSERVADAS AS CONDICOES LEGAIS. |
|
| B25A | Requested transfer of rights approved |
Owner name: BAYER INTELLECTUAL PROPERTY GMBH (DE) |