BR112015017949A2 - processo - Google Patents

processo

Info

Publication number
BR112015017949A2
BR112015017949A2 BR112015017949A BR112015017949A BR112015017949A2 BR 112015017949 A2 BR112015017949 A2 BR 112015017949A2 BR 112015017949 A BR112015017949 A BR 112015017949A BR 112015017949 A BR112015017949 A BR 112015017949A BR 112015017949 A2 BR112015017949 A2 BR 112015017949A2
Authority
BR
Brazil
Prior art keywords
hydrogenation
nitrogen
trialkylamine catalyst
reduces
containing salts
Prior art date
Application number
BR112015017949A
Other languages
English (en)
Inventor
K Paris Amy
H Brown Eugene
Wayne Hampton Kenneth Jr
S Howe Kevin
Allen Puckette Thomas
K Brown Thomas
Original Assignee
Eastman Chem Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eastman Chem Co filed Critical Eastman Chem Co
Publication of BR112015017949A2 publication Critical patent/BR112015017949A2/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/72Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups
    • C07C45/75Reactions with formaldehyde

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

1 / 1 resumo “ pro ce sso ” ㉠descrito um processo para produzir poliois (tais como neopentil glicol) que compreende reagir formaldeã­do e um outro aldeã­do na presenã§a de um catalisador de trialquilamina e um promotor de base para formar um produto da reaã§ã£o de condensaã§ã£o aldã³lica. o promotor de base melhora a remoã§ã£o de sais contendo nitrogãªnio antes da hidrogenaã§ã£o do hidroxi aldeã­do para produzir o poliol. o processo melhorado tambã©m reduz a utilizaã§ã£o de catalisador de trialquilamina, melhora a recuperaã§ã£o do catalisador de trialquilamina, e reduz os sais contendo nitrogãªnio antes da hidrogenaã§ã£o.
BR112015017949A 2013-01-31 2014-01-17 processo BR112015017949A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US13/755,910 US8710278B1 (en) 2013-01-31 2013-01-31 Process for producing polyols
PCT/US2014/012032 WO2014120481A1 (en) 2013-01-31 2014-01-17 Process for producing polyols

Publications (1)

Publication Number Publication Date
BR112015017949A2 true BR112015017949A2 (pt) 2017-07-11

Family

ID=50514200

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112015017949A BR112015017949A2 (pt) 2013-01-31 2014-01-17 processo

Country Status (10)

Country Link
US (2) US8710278B1 (pt)
EP (1) EP2951141B1 (pt)
JP (1) JP2016508997A (pt)
KR (1) KR20150113121A (pt)
CN (2) CN110002982A (pt)
AU (1) AU2014212774B2 (pt)
BR (1) BR112015017949A2 (pt)
SG (1) SG11201505972SA (pt)
TW (1) TWI610908B (pt)
WO (1) WO2014120481A1 (pt)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101952690B1 (ko) 2015-09-07 2019-02-27 주식회사 엘지화학 글리콜의 제조장치 및 제조방법
EP3315484B1 (de) * 2016-10-25 2019-02-27 OXEA GmbH Verfahren zur koppelproduktion von polyolen in gegenwart einer anorganischen base
CN108821943A (zh) * 2018-05-22 2018-11-16 吉林市道特化工科技有限责任公司 一种去除多羟基醇类物质中的叔胺盐的方法及精制工艺
CN109180428B (zh) * 2018-08-06 2020-06-05 吉林市道特化工科技有限责任公司 一种2,2-二甲基-1,3-丙二醇的生产工艺
KR102245931B1 (ko) 2018-10-22 2021-04-28 주식회사 엘지화학 디메틸올부탄알의 제조방법 및 이를 이용한 트리메틸올프로판의 제조방법
KR102119729B1 (ko) * 2018-10-31 2020-06-08 에스케이피아이씨글로벌(주) 프로필렌 글리콜 조성물 및 이의 제조 방법
CN109320397A (zh) * 2018-11-22 2019-02-12 湖南湘硕化工有限公司 一种新戊二醇的制备方法
EP3747855B1 (de) * 2019-06-04 2024-01-10 OQ Chemicals GmbH Verfahren zur kontinuierlichen herstellung von diolen aus aldehyden mittels raney-cobalt katalyse
CN110759821A (zh) * 2019-11-23 2020-02-07 张家港市华昌新材料科技有限公司 一种新戊二醇生产原料回收系统及其回收方法
CN112028758B (zh) * 2020-05-25 2024-09-10 广安摩珈生物科技有限公司 羟基醛的制备方法以及使用电渗析技术拆分光学异构体的方法
CN113200834A (zh) * 2021-05-15 2021-08-03 公主岭市恒昌科技有限公司 一种制备羟基新戊醛的方法
EP4410766A1 (en) 2023-01-31 2024-08-07 Arkema France Process for producing 2-methyl-1, 3-propanediol and system

Family Cites Families (67)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3886219A (en) 1969-01-14 1975-05-27 Huels Chemische Werke Ag Process for preparing saturated alcohols
BE758910A (fr) 1969-11-15 1971-05-13 Basf Ag Preparation de dimethyl-2, 2-propanediol-1, 3
DE2105922C3 (de) 1971-02-09 1974-08-08 Institut Organitscheskoj Chimii Akademii Nauk Kirgisskoj Ssr, Frunse (Sowjetunion) Verfahren zur Herstellung von Aldehydalkoholen und Ketonalkoholen
US3939216A (en) 1974-06-26 1976-02-17 Eastman Kodak Company Process for the preparation of neopentyl glycol
US3975450A (en) 1974-09-03 1976-08-17 Eastman Kodak Company Process for the preparation of polyhydric alcohols
FR2289478A1 (fr) 1974-10-30 1976-05-28 Charbonnages Ste Chimique Procede de preparation d'hydroxypivaldehyde
DE2702582C3 (de) * 1977-01-22 1980-12-04 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von Trimethylolalkanen
DE2813201A1 (de) * 1978-03-25 1979-10-04 Bayer Ag Verfahren zur herstellung von 2,2-dimethylolalkanalen
DE2827795A1 (de) 1978-06-24 1980-01-10 Huels Chemische Werke Ag Verfahren zur gewinnung von reinem neopentylglykol
DE3027890A1 (de) 1980-07-23 1982-03-04 Basf Ag, 6700 Ludwigshafen Hydrierkatalysatoren fuer die herstellung von propandiolen und verfahren zur herstellung von propandiolen mit solchen katalysatoren
US4393251A (en) 1981-06-17 1983-07-12 Basf Aktiengesellschaft Preparation of propanediols using a copper-and zinc containing hydrogenation catalyst
DE3432577A1 (de) 1984-09-05 1986-03-13 Basf Ag, 6700 Ludwigshafen Verfahren zur gewinnung von hydroxypivalinsaeureneopentylglykolester
DE3644675A1 (de) 1986-12-30 1988-07-14 Ruhrchemie Ag Verfahren zur herstellung von 2,2-dimethylpropandiol-(1,3)
US4855515A (en) 1987-08-12 1989-08-08 Eastman Kodak Company Process for the production of neopentyl glycol
US4851592A (en) 1987-10-27 1989-07-25 Eastman Kodak Company Triethylamine catalyzed neopentyl glycol production utilizing a gas sparged reactor
JPH01299239A (ja) 1988-05-25 1989-12-04 Mitsubishi Gas Chem Co Inc ネオペンチルグリコールの製造方法
DE3942792A1 (de) 1989-12-23 1991-06-27 Hoechst Ag Verfahren zur herstellung von 2,2-dimethylpropandiol-(1,3)
JPH0474143A (ja) 1990-07-13 1992-03-09 Mitsubishi Gas Chem Co Inc ネオペンチルグリコールの製造方法
US5395989A (en) 1990-11-06 1995-03-07 Mitsubishi Gas Chemical Company, Inc. Process for producing neopentyl glycol
US5166370A (en) 1991-04-12 1992-11-24 Arco Chemical Technology, L.P. Preparation of tetrahydrofuran using a supported transition metal
US5146012A (en) 1991-04-26 1992-09-08 Aristech Chemical Corporation Manufacture of neopentyl glycol (III)
US5144088A (en) * 1991-04-26 1992-09-01 Aristech Chemical Corporation Manufacture of neopentyl glycol (I)
US5532417A (en) 1991-04-26 1996-07-02 Aristech Chemical Corporation Manufacture of neopentyl glycol (IV)
US5185478A (en) 1991-06-17 1993-02-09 Aristech Chemical Corporation Manufacture of neopentyl glycol (IIA)
US5093537A (en) 1991-07-24 1992-03-03 Hoechst Celanese Corporation Method for the manufacture of 1,3-propanediol
DE4208571A1 (de) 1992-03-18 1993-09-23 Basf Ag Verfahren zur herstellung von hydroxypivalinsaeureneopentylglykolester
DE4218282A1 (de) 1992-06-03 1993-12-09 Degussa Verfahren zur Herstellung von 1,3-Propandiol
JPH0782192A (ja) * 1993-09-10 1995-03-28 Mitsubishi Gas Chem Co Inc ネオペンチルグリコールの製造法
US5608121A (en) 1994-10-20 1997-03-04 Mitsubishi Gas Chemical Company, Inc. Process for producing polyhydric alcohol
GB9519975D0 (en) 1995-09-28 1995-11-29 Davy Process Techn Ltd Process
DE19542036A1 (de) * 1995-11-10 1997-05-15 Basf Ag Verfahren zur Herstellung von Polyalkoholen
US5888923A (en) 1996-04-15 1999-03-30 Dairen Chemical Corporation Modified Raney nickel catalyst and a process for preparing diols by using the same
EP0935594B1 (en) * 1996-10-22 2002-01-23 Lg Chemical Limited Process for the continuous production of neopentyl glycol
DE19653093A1 (de) 1996-12-20 1998-06-25 Basf Ag Verfahren zur Herstellung von Polyalkoholen
FI102474B1 (fi) 1996-12-30 1998-12-15 Neste Oy Menetelmä moniarvoisten alkoholien valmistamiseksi
US6080896A (en) 1997-08-07 2000-06-27 Mitsubishi Gas Chemical Company, Inc. Process for producing polyhydric alcohol
JP4003018B2 (ja) 1997-08-07 2007-11-07 三菱瓦斯化学株式会社 多価アルコールの製造法
DE19754848C2 (de) 1997-12-10 2003-06-18 Celanese Chem Europe Gmbh Verfahren zur Herstellung von Alkoholen
FI108029B (fi) * 1997-12-30 2001-11-15 Neste Oy Menetelmä neopentyyliglykolin valmistamiseksi
SE520963C2 (sv) 1999-03-31 2003-09-16 Perstorp Ab Formaldehyd- och formiatreducerad polyolprocess
FI109993B (fi) * 1999-07-02 2002-11-15 Neste Chemicals Oy Menetelmä polyolien valmistamiseksi
US6268539B1 (en) 1999-10-07 2001-07-31 Nan Ya Plastics Corporation Manufacturing method of neopentyl glycol
EP1094051B1 (en) 1999-10-20 2003-06-11 Saudi Basic Industries Corporation A liquid phase catalytic hydrogenation process to convert aldehydes to the corresponding alcohols
DE19957522A1 (de) 1999-11-30 2001-05-31 Oxeno Olefinchemie Gmbh Verfahren zur katalytischen Durchführung von Aldolkondensationen mittels Mehrphasenreaktion
DE19963437A1 (de) 1999-12-28 2001-07-05 Basf Ag Verfahren zur Zersetzung von bei der Synthese mehrwertiger Alkohole gebildeter hochsiedender Nebenprodukte
DE10001257A1 (de) 2000-01-14 2001-07-19 Bayer Ag Verfahren zur Herstellung von Trimethylolalkanen
US7087800B2 (en) 2000-06-27 2006-08-08 Mitsubishi Gas Chemical Company, Inc Process for producing a polyol
DE10055180A1 (de) 2000-11-08 2002-05-29 Basf Ag Verfahren zur Hydrierung von Poly- oder Monomethylolalkanalen
US6552232B2 (en) 2001-06-26 2003-04-22 Exxonmobil Research And Engineering Company Process for conducting aldol condensation reactions in ionic liquid media
DE10152525A1 (de) 2001-10-24 2003-05-08 Basf Ag Verfahren zur Zersetzung von Ammoniumformiaten in polyolhaltigen Reaktionsgemischen
DE10234016A1 (de) 2002-07-26 2004-02-05 Basf Ag Verfahren zur Ausbeuteerhöhung bei der Herstellung von mehrwertigen Alkoholen durch Spaltung acetalhaltiger Nebenprodukte
DE10317543A1 (de) 2003-04-16 2004-11-04 Basf Ag Verfahren zur Hydrierung von Methylolalkanalen
DE10317545A1 (de) 2003-04-16 2004-11-04 Basf Ag Verfahren zur Herstellung von Neopentylglykol und Hydroxypivalinsäureneopentylglykolester
SG130108A1 (en) 2005-08-08 2007-03-20 Mitsubishi Gas Chemical Co Method of producing high-purity hydroxypivalaldehyde and/or dimer thereof
DE102006009838A1 (de) 2006-03-01 2007-09-06 Basf Ag Verfahren zur Hydrierung von Methylolalkanalen
US7388116B2 (en) 2006-06-06 2008-06-17 Basf Aktiengesellschaft Hydrogenation of methylolalkanals
US20080004475A1 (en) 2006-06-28 2008-01-03 Basf Aktiengesellschaft Process for the production of neopentylglycol using formaldehyde with a low methanol content
AU2007329489A1 (en) 2006-12-05 2008-06-12 Shell Internationale Research Maatschappij B.V. Process for preparing 1,3-propanediol
US7462747B2 (en) 2007-01-05 2008-12-09 Basf Aktiengesellschaft Process for preparing polyalcohols from formaldehyde having a low formic acid content
BRPI0808032B1 (pt) 2007-03-02 2017-01-24 Basf Se processos para preparar hidroxipivalinaldeído e para preparar neopentil glicol.
DE102008031338B4 (de) 2008-07-02 2012-09-13 Oxea Gmbh Verfahren zur Herstellung von Neopentylglykol
DE102008033163B4 (de) 2008-07-15 2012-06-14 Oxea Gmbh Verfahren zur Gewinnung von Neopentylglykol durch Spaltung von im Herstellverfahren anfallenden Hochsiedern
EP2376413B2 (de) 2008-12-09 2018-10-31 Basf Se Verfahren zur destillation eines wässrigen neopentylglykolgemisches
EP2376414A2 (de) 2008-12-09 2011-10-19 Basf Se Verfahren zur reinigung von roh-polymethylolen
FR2939790B1 (fr) 2008-12-16 2013-07-12 Rhodia Poliamida E Especialidades Ltda Procede catalytique de fabrication de composes de type diol
ES2494418T3 (es) 2009-01-12 2014-09-15 Basf Se Procedimiento para la preparación de polimetiloles
US8853465B2 (en) 2010-05-12 2014-10-07 Basf Se Process for preparing neopentyl glycol

Also Published As

Publication number Publication date
EP2951141B1 (en) 2019-06-19
US8710278B1 (en) 2014-04-29
AU2014212774B2 (en) 2018-01-04
WO2014120481A1 (en) 2014-08-07
EP2951141A1 (en) 2015-12-09
TWI610908B (zh) 2018-01-11
SG11201505972SA (en) 2015-08-28
KR20150113121A (ko) 2015-10-07
AU2014212774A1 (en) 2015-09-10
CN105008317A (zh) 2015-10-28
CN110002982A (zh) 2019-07-12
EP2951141A4 (en) 2016-09-14
JP2016508997A (ja) 2016-03-24
US20150368171A1 (en) 2015-12-24
TW201443007A (zh) 2014-11-16

Similar Documents

Publication Publication Date Title
BR112015017949A2 (pt) processo
BR112015000892A2 (pt) processo de preparar ácido acrílico
BR112015019704A2 (pt) método e sistema de destilação reativa, e, método de separar uma corrente de fase orgânica e aquosa mista
BR112016011849A2 (pt) Sistemas de gerenciamento de pátio ferroviário
CL2012001052A1 (es) Proceso para producir etanol por hidrogenación de ácido acético en presencia de un catalizador que comprende un primer metal, un segundo metal, un soporte y un modificador de soporte seleccionado de oxidos y metasilicatos de metal alcalino, alcalino térreo, del grupo iib y iiib, y sus mezclas.
CL2008001869A1 (es) Proceso para producir dialquil éter que comprende : alimentar corriente de alquil alcohol a sistema de reactor de columna de destilacion; contactarlo con una estructura de destilación catalítica y formar dialquil éter y agua; y recuperar dialquil éter como farcción de cabeza y el agua como fraccion de cola.
BR112012007592A2 (pt) produção de módulos solares
BR112015024535A2 (pt) método para preparar hidróxido de 1 -adamantiltrimetilamônio
BR112015027931A8 (pt) processo para recuperar e aperfeiçoar a produção de meso-lactida a partir de um fluxo que contém lactida bruta
BR112015018018A2 (pt) Processo para a preparação de hidróxi aldeído
BR112018010230A2 (pt) sistema catalisador e processo para a produção de glicóis
BRPI1011992A2 (pt) solução catalítica, e, processo para preparar aldeídos
BR112018000959A2 (pt) processo para a recuperação de sulfato de sódio
BR112012007162A2 (pt) poliol de reticulação multifuncional, e, método para produzir um poliol de reticulação multifuncional
BR112017024762A2 (pt) ?processo para preparar um policarbonato poliol hiper-ramificado e policarbonato poliol hiper- ramificado?
CY1121351T1 (el) Μεθοδος για την παρασκευη οξυκωδονης
BR112014020236A8 (pt) Catalisador de platina/paládio sobre zeólito, seu processo de produção e uso
PE20171664A1 (es) Proceso de sintesis de hidrocarburos
BR112012014997A2 (pt) sistemas de desidratação de compostos multi-hídricos, composições catalisadoras e processos.
BR112013018345A2 (pt) hidrogenação de ligação dupla carbono-carbono catalítica
AR098779A1 (es) Un proceso catalítico para la producción de propilenglicol a partir de glicerol, un catalizador de cobre y cerio, y un proceso para elaborar dicho catalizador
BR112016010239A2 (pt) Utilização de um catalisador, processo de síntese de um éster a partir de um álcool, e, composto
BR112015001785A2 (pt) concentração de uma solução de ureia em um processo para síntese de ureia.
BRPI1005287A2 (pt) processo para produzir resinas epóxi
BR112017012865A2 (pt) Processo para a produção de n-butanol e 1,4- butanodiol a partir de furano

Legal Events

Date Code Title Description
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]

Free format text: REFERENTE A 6A ANUIDADE.

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: EM VIRTUDE DO ARQUIVAMENTO PUBLICADO NA RPI 2549 DE 12-11-2019 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDO O ARQUIVAMENTO DO PEDIDO DE PATENTE, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.