BR112013008249A2 - método para fabricar xaropes de sorbitol de alta pureza a partir de sacarose e seus usos - Google Patents

método para fabricar xaropes de sorbitol de alta pureza a partir de sacarose e seus usos

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Publication number
BR112013008249A2
BR112013008249A2 BR112013008249A BR112013008249A BR112013008249A2 BR 112013008249 A2 BR112013008249 A2 BR 112013008249A2 BR 112013008249 A BR112013008249 A BR 112013008249A BR 112013008249 A BR112013008249 A BR 112013008249A BR 112013008249 A2 BR112013008249 A2 BR 112013008249A2
Authority
BR
Brazil
Prior art keywords
content
sucrose
syrup
high purity
making high
Prior art date
Application number
BR112013008249A
Other languages
English (en)
Other versions
BR112013008249B1 (pt
Inventor
Duflot Pierrick
Original Assignee
Roquette Freres
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Roquette Freres filed Critical Roquette Freres
Publication of BR112013008249A2 publication Critical patent/BR112013008249A2/pt
Publication of BR112013008249B1 publication Critical patent/BR112013008249B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A23L27/34—Sugar alcohols
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
    • A23L29/37—Sugar alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/56—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by isomerisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Molecular Biology (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Saccharide Compounds (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

método para fabricar xaropes de sorbitol de alta pureza a partir de sacarose e seus usos. a invenção refere-se a um método para fabricar um xarope de sorbitol que tem um teor de açúcares redutores totais de no máximo 0,2% e um teor de manitol inferior a 1%, com 70% em peso de matéria seca. esse método de fabricação é caracterizado pelo fato de que inclui as etapas de: (a) hidrolisar uma solução de sacarose em uma solução de açúcares invertidos, (b) separar a solução de açúcar inverto por cromatografia de leito móvel simulado ("simulated movig bed chromatography") em, por um lado, um xarope de dextrose que tem pelo menos 99,3% de preferência 99,4% de maior preferência pelo menos 99,5%, e de ainda maior preferência 99,7% de teor de dextrose e, por outro lado, um xarope de frutose que tem pelo menos 90% de preferência 92%, de teor de frutose, e (c) hidrogenação do dito xarope de dextrose em um xarope de sorbitol que tem um teor de açúcares redutores de no máximo 0,2% e um teor de manitol inferior a 1% com 70% em peso de matéria seca.
BR112013008249-6A 2010-10-08 2011-10-07 Método para fabricar xaropes de sorbitol de alta pureza a partir de sacarose e seus usos BR112013008249B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1058189A FR2965819B1 (fr) 2010-10-08 2010-10-08 Procede de fabrication de sirops de sorbitol de haute purete a partir de saccharose et utilisations
FR1058189 2010-10-08
PCT/FR2011/052345 WO2012045985A1 (fr) 2010-10-08 2011-10-07 Procédé de fabrication de sirops de sorbitol de haute pureté à partir de saccharose et utilisations

Publications (2)

Publication Number Publication Date
BR112013008249A2 true BR112013008249A2 (pt) 2017-10-31
BR112013008249B1 BR112013008249B1 (pt) 2019-04-02

Family

ID=43920126

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112013008249-6A BR112013008249B1 (pt) 2010-10-08 2011-10-07 Método para fabricar xaropes de sorbitol de alta pureza a partir de sacarose e seus usos

Country Status (8)

Country Link
US (1) US8865948B2 (pt)
EP (1) EP2624709B1 (pt)
CN (1) CN103179866A (pt)
BR (1) BR112013008249B1 (pt)
ES (1) ES2524893T3 (pt)
FR (1) FR2965819B1 (pt)
MX (1) MX339466B (pt)
WO (1) WO2012045985A1 (pt)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE1021455B1 (nl) 2012-11-22 2015-11-26 Syral Belgium Nv Werkwijze voor het verwerken van substraten die een uitgangsstof voor mannitol omvatten.
BE1022099B1 (nl) 2014-01-17 2016-02-16 Syral Belgium Nv Werkwijze voor het bereiden van een sorbitolrijke stroop met hoge zuiverheid
BE1021954B1 (nl) * 2014-06-05 2016-01-28 Syral Belgium Nv Samenstelling van sorbitol met lage friabiliteit
FR3023128B1 (fr) * 2014-07-01 2017-11-10 Roquette Freres Nouvelle composition edulcorante
MX2020001277A (es) * 2017-08-02 2020-08-20 Evonik Operations Gmbh Un edulcorante a base de isomaltulosa.
CN108503506A (zh) * 2018-06-25 2018-09-07 山东兆光色谱分离技术有限公司 一种利用色谱分离技术生产高纯山梨醇的新工艺
CN109053823A (zh) * 2018-08-10 2018-12-21 太仓沪试试剂有限公司 一种从葡萄糖浆中分离纯化葡萄糖的方法
EP3886818A1 (en) 2018-11-30 2021-10-06 Amerilab Technologies, Inc. Effervescent tablets that include crystalline sugar binder and methods of making the same

Family Cites Families (24)

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US2985589A (en) 1957-05-22 1961-05-23 Universal Oil Prod Co Continuous sorption process employing fixed bed of sorbent and moving inlets and outlets
US3044904A (en) 1960-02-15 1962-07-17 Central Aguirre Sugar Company Separation of dextrose and levulose
US3416961A (en) 1964-01-07 1968-12-17 Colonial Sugar Refining Co Process for the separation of fructose and glucose
US3785864A (en) 1970-07-23 1974-01-15 Boehringer Mannheim Gmbh Process for the chromatographic separation of multi-component mixtures containing glucose
DE2036525B2 (de) 1970-07-23 1974-06-20 Boehringer Mannheim Gmbh Verfahren und Vorrichtung zur chromatographischen Auftrennung von Mehrstoffgemischen
US3692582A (en) 1970-07-31 1972-09-19 Suomen Sokeri Oy Procedure for the separation of fructose from the glucose of invert sugar
US4226977A (en) 1976-05-27 1980-10-07 Uop Inc. Process for separating a ketose from an aldose by selective adsorption
JPS5326336A (en) 1976-08-24 1978-03-11 Toray Industries Method of fractional absorption for saccharides
FI69248C (fi) 1976-12-21 1986-01-10 Mitsubishi Chem Ind Foerfarande foer reglering av operationsprocessen av en simulerad roerlig baedd
JPS6055162B2 (ja) 1977-05-26 1985-12-04 参松工業株式会社 カラムクロマト分離法
FR2454830A1 (fr) 1979-04-25 1980-11-21 Roquette Freres Installation et procede pour la separation continue par adsorption selective de melanges de sucres et/ou de polyols
US4293346A (en) 1979-11-05 1981-10-06 Uop Inc. Simulated countercurrent sorption process employing ion exchange resins with backflushing
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FR2838452B1 (fr) 2002-04-10 2004-07-09 Eurodia Ind Procede de production en continu de galacto oligosaccharides
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Also Published As

Publication number Publication date
FR2965819B1 (fr) 2013-02-22
US8865948B2 (en) 2014-10-21
BR112013008249B1 (pt) 2019-04-02
EP2624709A1 (fr) 2013-08-14
MX339466B (es) 2016-05-27
CN103179866A (zh) 2013-06-26
WO2012045985A1 (fr) 2012-04-12
EP2624709B1 (fr) 2014-08-27
ES2524893T3 (es) 2014-12-15
FR2965819A1 (fr) 2012-04-13
MX2013003870A (es) 2013-10-30
US20130225874A1 (en) 2013-08-29

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 07/10/2011, OBSERVADAS AS CONDICOES LEGAIS. (CO) 20 (VINTE) ANOS CONTADOS A PARTIR DE 07/10/2011, OBSERVADAS AS CONDICOES LEGAIS