BR112012021146A2 - cristal estabilizado de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi) fenoxi) quinolina-4-ilmetil carbonato, processo para produção do cristal, e composição química agrícola constituída pelo cristal. - Google Patents

cristal estabilizado de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi) fenoxi) quinolina-4-ilmetil carbonato, processo para produção do cristal, e composição química agrícola constituída pelo cristal.

Info

Publication number
BR112012021146A2
BR112012021146A2 BR112012021146A BR112012021146A BR112012021146A2 BR 112012021146 A2 BR112012021146 A2 BR 112012021146A2 BR 112012021146 A BR112012021146 A BR 112012021146A BR 112012021146 A BR112012021146 A BR 112012021146A BR 112012021146 A2 BR112012021146 A2 BR 112012021146A2
Authority
BR
Brazil
Prior art keywords
crystal
trifluoromethoxy
quinoline
dimethyl
ethyl
Prior art date
Application number
BR112012021146A
Other languages
English (en)
Other versions
BR112012021146A8 (pt
Inventor
Akinori Morikawa
Hiroki Hotta
Kazumi Yamamoto
Kouki Tanigakiuchi
Mikio Sekiguchi
Nobuto Minowa
Nozomu Nakanishi
Shizuo Shimano
Takashi Watanabe
Original Assignee
Meiji Seika Pharma Co Ltd
Nippon Kayaku Kk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Meiji Seika Pharma Co Ltd, Nippon Kayaku Kk filed Critical Meiji Seika Pharma Co Ltd
Publication of BR112012021146A2 publication Critical patent/BR112012021146A2/pt
Publication of BR112012021146A8 publication Critical patent/BR112012021146A8/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D215/00—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems
    • C07D215/02—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom
    • C07D215/16—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D215/20—Oxygen atoms
    • C07D215/22—Oxygen atoms attached in position 2 or 4
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D215/00—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems
    • C07D215/02—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom
    • C07D215/16—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D215/20—Oxygen atoms
    • C07D215/22—Oxygen atoms attached in position 2 or 4
    • C07D215/233—Oxygen atoms attached in position 2 or 4 only one oxygen atom which is attached in position 4
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
    • A01N43/42—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings condensed with carbocyclic rings
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
    • A01N47/06—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom containing —O—CO—O— groups; Thio analogues thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D215/00—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems
    • C07D215/02—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom
    • C07D215/16—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D215/20—Oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Quinoline Compounds (AREA)

Abstract

cristal estabilizado de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi) quinolina-4-ilmetil carbonato, processo para produção do cristal, e composição química agrícola constituída pelo cristal. um objetivo da invenção atual é produzir um cristal de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi)fenoxi)quinolina-4-ilmetil carbonato tendo propriedades físico-químicas estáveis. o objetivo é alcançado em um cristal de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi)fenoxi)quinolina-4-ilmetil carbonato que apresenta um padrão de pico de difração mostrada na figura 1 conforme determinado por difratometria de raios x em pó.
BR112012021146A 2010-02-23 2011-02-22 cristal estabilizado de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi) fenoxi) quinolina-4-il metil carbonato, processo para produção do cristal, e composição química agrícola constituída pelo cristal. BR112012021146A8 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2010037475 2010-02-23
PCT/JP2011/053781 WO2011105349A1 (ja) 2010-02-23 2011-02-22 ２－エチル－３，７－ジメチル－６－（４－（トリフルオロメトキシ）フェノキシ）キノリン－４－イルメチルカーボネートの安定型結晶およびその製造方法並びにその結晶を含有する農薬組成物

Publications (2)

Publication Number Publication Date
BR112012021146A2 true BR112012021146A2 (pt) 2015-09-22
BR112012021146A8 BR112012021146A8 (pt) 2017-02-07

Family

ID=44506757

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112012021146A BR112012021146A8 (pt) 2010-02-23 2011-02-22 cristal estabilizado de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi) fenoxi) quinolina-4-il metil carbonato, processo para produção do cristal, e composição química agrícola constituída pelo cristal.

Country Status (13)

Country Link
US (1) US8648195B2 (pt)
EP (1) EP2540709B1 (pt)
JP (1) JP5697655B2 (pt)
KR (1) KR101814836B1 (pt)
CN (1) CN102884050B (pt)
AU (1) AU2011218939B2 (pt)
BR (1) BR112012021146A8 (pt)
CA (1) CA2790921A1 (pt)
ES (1) ES2523758T3 (pt)
RU (1) RU2545094C2 (pt)
SG (1) SG183453A1 (pt)
TW (1) TWI491356B (pt)
WO (1) WO2011105349A1 (pt)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB201202393D0 (en) * 2012-02-09 2012-03-28 Syngenta Ltd Polymorphs
JP2013166724A (ja) * 2012-02-16 2013-08-29 Sumitomo Chemical Co Ltd フルミオキサジンの結晶形
CN105050394B (zh) * 2013-01-30 2017-05-24 明治制果药业株式会社 呈含水悬浮液形式的农药组合物
CN103814939A (zh) * 2014-02-21 2014-05-28 深圳诺普信农化股份有限公司 一种杀虫组合物
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
WO2019117179A1 (ja) 2017-12-12 2019-06-20 日本化薬株式会社 キノリン‐４（１ｈ）－オン誘導体の製造方法
WO2019235602A1 (ja) * 2018-06-08 2019-12-12 日本化薬株式会社 水和性農薬組成物
CN113875766B (zh) * 2020-07-02 2023-09-15 江苏龙灯化学有限公司 一种杀虫组合物
CN111808020B (zh) * 2020-09-07 2020-12-01 湖南速博生物技术有限公司 一种flometoquin中间体的合成方法
CN115500354B (zh) * 2022-10-26 2024-03-01 海利尔药业集团股份有限公司 一种杀虫组合物及其用途

Family Cites Families (14)

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Publication number Priority date Publication date Assignee Title
DE3925253A1 (de) 1989-07-29 1991-01-31 Basf Ag Monoklines metazachlor und verfahren zu seiner herstellung
US6486195B1 (en) 1993-08-19 2002-11-26 Merck & Co., Inc. Thermodynamically stable crystal form of 4″-deoxy-4″-epi-methylamino avermectin B1a/B1b benzoic acid salt and processes for its preparation
AU684828B2 (en) * 1993-08-19 1998-01-08 Merck Sharp & Dohme Corp. Thermodynamically stable crystal form of 4"-deoxy-4"-(epi)-methylamino avermectin B1a/B1b benzoic acid salt and processes for its preparation
EP0722430B1 (en) * 1994-08-04 1998-10-21 Sumitomo Chemical Company Limited Dihalopropene compounds, insecticidal/acaricidal agents containing same, and intermediates for their production
JPH09227538A (ja) 1996-02-28 1997-09-02 Nissan Chem Ind Ltd 効力が安定化したチフルザミド
JPH101476A (ja) 1996-02-28 1998-01-06 Nissan Chem Ind Ltd 効力が向上したチフルザミド
JP2001114707A (ja) 1999-10-14 2001-04-24 Nissan Chem Ind Ltd 安定型結晶を製造する方法
JP4557131B2 (ja) * 2003-10-03 2010-10-06 日産化学工業株式会社 結晶多形インド−ル化合物およびその製造方法
BRPI0514051B1 (pt) * 2004-08-04 2014-07-22 Nippon Kayaku Kk Composto derivado de quinolina que compreende o mesmo como ingrediente ativo, inseticida, método e uso destes no controle de pragas de insetos na agricultura e horticultura
WO2007088978A1 (ja) * 2006-02-03 2007-08-09 Meiji Seika Kaisha, Ltd. 新規キノリン誘導体およびこれを有効成分として含有する農園芸用殺菌剤
JP4989153B2 (ja) * 2006-08-15 2012-08-01 コスモ石油株式会社 ５−アミノレブリン酸リン酸塩の新規結晶及びその製造方法
IL181125A0 (en) * 2007-02-01 2007-07-04 Maktheshim Chemical Works Ltd Polymorphs of 3-(e)-2-{2-[6-(2-
UA97267C2 (ru) * 2007-03-16 2012-01-25 Сингента Партисипейшнс Аг Кристаллические модификации с, i и моногидрат в форме а (9-изопропил-1,2,3,4-тетрагидро-1,4-метанонафталин-5-ил)-амида 3-дифторметил-1-метил-1н-пиразол-4-карбоновой кислоты, бактерицидная композиция, композиция для борьбы с болезнями полезных растений, способ борьбы с болезнями полезных растений и способ получения композиции
CN102149684B (zh) * 2008-07-15 2015-04-29 日本化药株式会社 制备6-芳氧基喹啉衍生物的方法及其中间体

Also Published As

Publication number Publication date
BR112012021146A8 (pt) 2017-02-07
EP2540709A4 (en) 2013-07-31
CN102884050B (zh) 2014-05-28
EP2540709A1 (en) 2013-01-02
KR101814836B1 (ko) 2018-01-04
RU2012140431A (ru) 2014-03-27
TWI491356B (zh) 2015-07-11
AU2011218939B2 (en) 2015-08-13
KR20130056213A (ko) 2013-05-29
SG183453A1 (en) 2012-09-27
TW201204255A (en) 2012-02-01
CA2790921A1 (en) 2011-09-01
WO2011105349A1 (ja) 2011-09-01
JP5697655B2 (ja) 2015-04-08
JPWO2011105349A1 (ja) 2013-06-20
US8648195B2 (en) 2014-02-11
US20130045989A1 (en) 2013-02-21
AU2011218939A1 (en) 2012-10-04
RU2545094C2 (ru) 2015-03-27
CN102884050A (zh) 2013-01-16
ES2523758T3 (es) 2014-12-01
EP2540709B1 (en) 2014-08-20

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Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]