BR112012021146A2 - 2-Ethyl-3,7-dimethyl-6- (4- (trifluoromethoxy) phenoxy) quinoline-4-ylmethyl carbonate stabilized crystal, crystal production process and crystal agricultural chemical composition. - Google Patents

2-Ethyl-3,7-dimethyl-6- (4- (trifluoromethoxy) phenoxy) quinoline-4-ylmethyl carbonate stabilized crystal, crystal production process and crystal agricultural chemical composition.

Info

Publication number
BR112012021146A2
BR112012021146A2 BR112012021146A BR112012021146A BR112012021146A2 BR 112012021146 A2 BR112012021146 A2 BR 112012021146A2 BR 112012021146 A BR112012021146 A BR 112012021146A BR 112012021146 A BR112012021146 A BR 112012021146A BR 112012021146 A2 BR112012021146 A2 BR 112012021146A2
Authority
BR
Brazil
Prior art keywords
crystal
trifluoromethoxy
quinoline
dimethyl
ethyl
Prior art date
Application number
BR112012021146A
Other languages
Portuguese (pt)
Other versions
BR112012021146A8 (en
Inventor
Akinori Morikawa
Hiroki Hotta
Kazumi Yamamoto
Kouki Tanigakiuchi
Mikio Sekiguchi
Nobuto Minowa
Nozomu Nakanishi
Shizuo Shimano
Takashi Watanabe
Original Assignee
Meiji Seika Pharma Co Ltd
Nippon Kayaku Kk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Meiji Seika Pharma Co Ltd, Nippon Kayaku Kk filed Critical Meiji Seika Pharma Co Ltd
Publication of BR112012021146A2 publication Critical patent/BR112012021146A2/en
Publication of BR112012021146A8 publication Critical patent/BR112012021146A8/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D215/00—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems
    • C07D215/02—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom
    • C07D215/16—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D215/20—Oxygen atoms
    • C07D215/22—Oxygen atoms attached in position 2 or 4
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D215/00—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems
    • C07D215/02—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom
    • C07D215/16—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D215/20—Oxygen atoms
    • C07D215/22—Oxygen atoms attached in position 2 or 4
    • C07D215/233—Oxygen atoms attached in position 2 or 4 only one oxygen atom which is attached in position 4
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
    • A01N43/42—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings condensed with carbocyclic rings
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
    • A01N47/06—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom containing —O—CO—O— groups; Thio analogues thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D215/00—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems
    • C07D215/02—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom
    • C07D215/16—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D215/20—Oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

Abstract

cristal estabilizado de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi) quinolina-4-ilmetil carbonato, processo para produção do cristal, e composição química agrícola constituída pelo cristal. um objetivo da invenção atual é produzir um cristal de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi)fenoxi)quinolina-4-ilmetil carbonato tendo propriedades físico-químicas estáveis. o objetivo é alcançado em um cristal de 2-etil-3,7-dimetil-6-(4-(trifluormetoxi)fenoxi)quinolina-4-ilmetil carbonato que apresenta um padrão de pico de difração mostrada na figura 1 conforme determinado por difratometria de raios x em pó.2-Ethyl-3,7-dimethyl-6- (4- (trifluoromethoxy) quinoline-4-ylmethyl carbonate) stabilized crystal, crystal production process, and crystal-based agricultural chemical composition An object of the present invention is to produce a 2-ethyl-3,7-dimethyl-6- (4- (trifluoromethoxy) phenoxy) quinoline-4-ylmethyl carbonate crystal having stable physicochemical properties The objective is achieved in a 2-ethyl-3.7 crystal -dimethyl-6- (4- (trifluoromethoxy) phenoxy) quinoline-4-ylmethyl carbonate exhibiting a peak diffraction pattern shown in Figure 1 as determined by powder x-ray diffractometry.

BR112012021146A 2010-02-23 2011-02-22 2-Ethyl-3,7-dimethyl-6- (4- (trifluoromethoxy) phenoxy) quinoline-4-yl methyl carbonate stabilized crystal, crystal production process, and agricultural chemical composition consisting of the crystal. BR112012021146A8 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2010037475 2010-02-23
PCT/JP2011/053781 WO2011105349A1 (en) 2010-02-23 2011-02-22 Stable crystal form of 2-ethyl-3, 7-dimethyl-6-(4-(trifluoromethoxy) phenoxy)quinoline-4-ylmethyl carbonate, method of manufacturing same and agricultural chemical composition containing crystals of same

Publications (2)

Publication Number Publication Date
BR112012021146A2 true BR112012021146A2 (en) 2015-09-22
BR112012021146A8 BR112012021146A8 (en) 2017-02-07

Family

ID=44506757

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112012021146A BR112012021146A8 (en) 2010-02-23 2011-02-22 2-Ethyl-3,7-dimethyl-6- (4- (trifluoromethoxy) phenoxy) quinoline-4-yl methyl carbonate stabilized crystal, crystal production process, and agricultural chemical composition consisting of the crystal.

Country Status (13)

Country Link
US (1) US8648195B2 (en)
EP (1) EP2540709B1 (en)
JP (1) JP5697655B2 (en)
KR (1) KR101814836B1 (en)
CN (1) CN102884050B (en)
AU (1) AU2011218939B2 (en)
BR (1) BR112012021146A8 (en)
CA (1) CA2790921A1 (en)
ES (1) ES2523758T3 (en)
RU (1) RU2545094C2 (en)
SG (1) SG183453A1 (en)
TW (1) TWI491356B (en)
WO (1) WO2011105349A1 (en)

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GB201202393D0 (en) * 2012-02-09 2012-03-28 Syngenta Ltd Polymorphs
JP2013166724A (en) * 2012-02-16 2013-08-29 Sumitomo Chemical Co Ltd Crystalline form of flumioxazin
KR102055969B1 (en) * 2013-01-30 2019-12-13 메이지 세이카 파루마 가부시키가이샤 Agrochemical composition in form of aqueous suspension
CN103814939A (en) * 2014-02-21 2014-05-28 深圳诺普信农化股份有限公司 Insecticidal composition
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
US11267787B2 (en) 2017-12-12 2022-03-08 Nippon Kayaku Co., Ltd Method for producing quinolin-4(1H)-one derivative
AU2019281147A1 (en) * 2018-06-08 2021-01-07 Meiji Seika Pharma Co., Ltd. Water-dispersible agrochemical composition
CN113875766B (en) * 2020-07-02 2023-09-15 江苏龙灯化学有限公司 Insecticidal composition
CN111808020B (en) * 2020-09-07 2020-12-01 湖南速博生物技术有限公司 Synthetic method of flometoquin intermediate
CN115500354B (en) * 2022-10-26 2024-03-01 海利尔药业集团股份有限公司 Insecticidal composition and application thereof

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US6486195B1 (en) 1993-08-19 2002-11-26 Merck & Co., Inc. Thermodynamically stable crystal form of 4″-deoxy-4″-epi-methylamino avermectin B1a/B1b benzoic acid salt and processes for its preparation
SK281684B6 (en) * 1993-08-19 2001-06-11 Merck & Co., Inc. Hemihydrate of the crystalline form of the benzoic acid salt of 4''-deoxy-4''-epimethylamino avermectin b1a/b1b, method for production and means containing it
CZ129696A3 (en) * 1994-08-04 1996-09-11 Sumitomo Chemical Co Dihalogenpropene compounds, insecticidal-acaricidal agents in which said compounds are comprised and intermediates for their preparation
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JP4557131B2 (en) * 2003-10-03 2010-10-06 日産化学工業株式会社 Crystalline polymorphic indole compound and process for producing the same
RU2424232C2 (en) * 2004-08-04 2011-07-20 Мейдзи Сейка Кайся, Лтд. Quinoline derivatives and insecticides containing said derivatives as active ingredient
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Also Published As

Publication number Publication date
BR112012021146A8 (en) 2017-02-07
CA2790921A1 (en) 2011-09-01
EP2540709B1 (en) 2014-08-20
SG183453A1 (en) 2012-09-27
KR20130056213A (en) 2013-05-29
US20130045989A1 (en) 2013-02-21
EP2540709A4 (en) 2013-07-31
WO2011105349A1 (en) 2011-09-01
TW201204255A (en) 2012-02-01
RU2012140431A (en) 2014-03-27
RU2545094C2 (en) 2015-03-27
JP5697655B2 (en) 2015-04-08
TWI491356B (en) 2015-07-11
EP2540709A1 (en) 2013-01-02
US8648195B2 (en) 2014-02-11
JPWO2011105349A1 (en) 2013-06-20
ES2523758T3 (en) 2014-12-01
AU2011218939A1 (en) 2012-10-04
AU2011218939B2 (en) 2015-08-13
KR101814836B1 (en) 2018-01-04
CN102884050B (en) 2014-05-28
CN102884050A (en) 2013-01-16

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B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]