BE818695A - Procede pour eliminer le mercure des effluents liquides - Google Patents
Procede pour eliminer le mercure des effluents liquidesInfo
- Publication number
- BE818695A BE818695A BE147475A BE147475A BE818695A BE 818695 A BE818695 A BE 818695A BE 147475 A BE147475 A BE 147475A BE 147475 A BE147475 A BE 147475A BE 818695 A BE818695 A BE 818695A
- Authority
- BE
- Belgium
- Prior art keywords
- emi
- mercury
- thiourea
- hydroxylamine
- salt
- Prior art date
Links
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 title claims abstract description 34
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Natural products NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 150000002443 hydroxylamines Chemical class 0.000 title claims abstract description 7
- 229910052753 mercury Inorganic materials 0.000 title abstract description 30
- 238000005189 flocculation Methods 0.000 title abstract description 6
- 239000002351 wastewater Substances 0.000 title abstract description 4
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 title description 29
- 150000002730 mercury Chemical class 0.000 title description 5
- 230000016615 flocculation Effects 0.000 title description 2
- 238000000034 method Methods 0.000 claims abstract description 19
- 239000000725 suspension Substances 0.000 claims abstract description 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 7
- 239000002253 acid Substances 0.000 claims abstract description 6
- 239000000701 coagulant Substances 0.000 claims abstract description 5
- 229920002401 polyacrylamide Polymers 0.000 claims abstract description 3
- 150000005846 sugar alcohols Polymers 0.000 claims abstract description 3
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims abstract 3
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 11
- 239000007864 aqueous solution Substances 0.000 claims description 10
- 239000002244 precipitate Substances 0.000 claims description 9
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 7
- 239000000460 chlorine Substances 0.000 claims description 7
- 229910052801 chlorine Inorganic materials 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 5
- 239000000440 bentonite Substances 0.000 claims description 4
- 229910000278 bentonite Inorganic materials 0.000 claims description 4
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 4
- 230000001376 precipitating effect Effects 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 3
- ZNBNBTIDJSKEAM-UHFFFAOYSA-N 4-[7-hydroxy-2-[5-[5-[6-hydroxy-6-(hydroxymethyl)-3,5-dimethyloxan-2-yl]-3-methyloxolan-2-yl]-5-methyloxolan-2-yl]-2,8-dimethyl-1,10-dioxaspiro[4.5]decan-9-yl]-2-methyl-3-propanoyloxypentanoic acid Chemical group C1C(O)C(C)C(C(C)C(OC(=O)CC)C(C)C(O)=O)OC11OC(C)(C2OC(C)(CC2)C2C(CC(O2)C2C(CC(C)C(O)(CO)O2)C)C)CC1 ZNBNBTIDJSKEAM-UHFFFAOYSA-N 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 229910000378 hydroxylammonium sulfate Inorganic materials 0.000 claims description 2
- 239000008394 flocculating agent Substances 0.000 claims 2
- 239000004927 clay Substances 0.000 claims 1
- 150000004679 hydroxides Chemical class 0.000 claims 1
- 239000010802 sludge Substances 0.000 abstract description 17
- 150000003839 salts Chemical class 0.000 abstract description 11
- 238000001914 filtration Methods 0.000 abstract description 8
- 238000000746 purification Methods 0.000 abstract description 8
- 238000010908 decantation Methods 0.000 abstract description 4
- 239000003638 chemical reducing agent Substances 0.000 abstract description 3
- 238000011084 recovery Methods 0.000 abstract description 3
- -1 HgS Chemical class 0.000 abstract description 2
- 238000011144 upstream manufacturing Methods 0.000 abstract description 2
- 239000003513 alkali Substances 0.000 abstract 1
- 239000003295 industrial effluent Substances 0.000 abstract 1
- 239000002002 slurry Substances 0.000 abstract 1
- 239000002699 waste material Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 23
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 description 8
- 238000005352 clarification Methods 0.000 description 7
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 5
- 239000003643 water by type Substances 0.000 description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 238000009434 installation Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 229910052979 sodium sulfide Inorganic materials 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- LWJROJCJINYWOX-UHFFFAOYSA-L mercury dichloride Chemical compound Cl[Hg]Cl LWJROJCJINYWOX-UHFFFAOYSA-L 0.000 description 3
- 229940008718 metallic mercury Drugs 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- HYHCSLBZRBJJCH-UHFFFAOYSA-M sodium hydrosulfide Chemical compound [Na+].[SH-] HYHCSLBZRBJJCH-UHFFFAOYSA-M 0.000 description 2
- QXKXDIKCIPXUPL-UHFFFAOYSA-N sulfanylidenemercury Chemical class [Hg]=S QXKXDIKCIPXUPL-UHFFFAOYSA-N 0.000 description 2
- WZFUQSJFWNHZHM-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)CC(=O)N1CC2=C(CC1)NN=N2 WZFUQSJFWNHZHM-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- 229920006063 Lamide® Polymers 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- YUCJFSWWUVRFED-UHFFFAOYSA-N aminomercury Chemical compound [Hg]N YUCJFSWWUVRFED-UHFFFAOYSA-N 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- BQPIGGFYSBELGY-UHFFFAOYSA-N mercury(2+) Chemical compound [Hg+2] BQPIGGFYSBELGY-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 238000003969 polarography Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000012279 sodium borohydride Substances 0.000 description 1
- 229910000033 sodium borohydride Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000004763 sulfides Chemical class 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G13/00—Compounds of mercury
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5272—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using specific organic precipitants
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/70—Treatment of water, waste water, or sewage by reduction
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S210/00—Liquid purification or separation
- Y10S210/902—Materials removed
- Y10S210/911—Cumulative poison
- Y10S210/912—Heavy metal
- Y10S210/914—Mercury
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Inorganic Chemistry (AREA)
- Removal Of Specific Substances (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT2771673A IT995170B (it) | 1973-08-09 | 1973-08-09 | Procedimento per l eliminazione del mercurio da effluenti liquidi |
| IT2771573A IT998338B (it) | 1973-08-09 | 1973-08-09 | Procedimento per l eliminazione del mercurio da effluenti liquidi |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE818695A true BE818695A (fr) | 1975-02-10 |
Family
ID=26328742
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE147475A BE818695A (fr) | 1973-08-09 | 1974-08-09 | Procede pour eliminer le mercure des effluents liquides |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4087359A (de) |
| JP (1) | JPS5741991B2 (de) |
| BE (1) | BE818695A (de) |
| CA (1) | CA1031875A (de) |
| DE (1) | DE2437779A1 (de) |
| ES (1) | ES429069A1 (de) |
| FR (1) | FR2240192A1 (de) |
| NL (1) | NL178962C (de) |
| SE (1) | SE399869B (de) |
| SU (1) | SU865124A3 (de) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110642447A (zh) * | 2019-09-12 | 2020-01-03 | 上海申欣环保实业有限公司 | 废水脱氯除汞的方法及处理设备 |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE399869B (sv) * | 1973-08-09 | 1978-03-06 | Montedison Spa | Sett att avlegsna kvicksilver eller kvicksilversalter fran ett vetskeavflode medelst tiokarbamid eller ett hydroxyl-aminsalt |
| US4549973A (en) * | 1983-04-25 | 1985-10-29 | Ethyl Corporation | Decolorization of calcium bromide brines |
| DE3839222A1 (de) * | 1988-11-19 | 1990-05-23 | Degussa | Verwendung von substituierten thioharnstoffen zur abtrennung komplex gebundener schwermetallionen |
| DE4013974C1 (de) * | 1990-04-30 | 1991-09-19 | Guenter Dipl.-Ing. 5100 Aachen De Straten | |
| US6797178B2 (en) * | 2000-03-24 | 2004-09-28 | Ada Technologies, Inc. | Method for removing mercury and mercuric compounds from dental effluents |
| US6911570B2 (en) | 2000-11-28 | 2005-06-28 | Ada Technologies, Inc. | Method for fixating sludges and soils contaminated with mercury and other heavy metals |
| US7048781B1 (en) | 2002-10-07 | 2006-05-23 | Ada Technologies, Inc. | Chemically-impregnated silicate agents for mercury control |
| US6942840B1 (en) | 2001-09-24 | 2005-09-13 | Ada Technologies, Inc. | Method for removal and stabilization of mercury in mercury-containing gas streams |
| US7183235B2 (en) * | 2002-06-21 | 2007-02-27 | Ada Technologies, Inc. | High capacity regenerable sorbent for removing arsenic and other toxic ions from drinking water |
| DE10336534A1 (de) * | 2003-08-05 | 2005-02-24 | Stockhausen Gmbh | Verfahren zur Verminderung der Schwermetallkonzentration in Abwasseraufbereitungsschlämmen |
| WO2005032394A2 (en) * | 2003-10-01 | 2005-04-14 | Ada Technologies, Inc. | System for removing mercury and mercuric compounds from dental wastes |
| JP5889059B2 (ja) * | 2011-04-04 | 2016-03-22 | アークレイ株式会社 | 金属の回収方法 |
| WO2013117996A1 (en) * | 2012-02-10 | 2013-08-15 | Kemira Oyj | Processes for the removal of metals and oxyanions from aqueous streams |
| EP2746230A1 (de) * | 2012-12-18 | 2014-06-25 | Total SA | Verfahren zum Entfernen von Quecksilber aus Produktionswasser und Kondensaten |
| CA3082354A1 (en) * | 2017-11-10 | 2019-05-16 | Reticle Inc. | Methods of treating water to remove contaminants and water treatment plants for the practice thereof |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3369886A (en) * | 1964-09-23 | 1968-02-20 | Exxon Research Engineering Co | Process of producing finely divided metals and alloys |
| US3377274A (en) * | 1965-01-05 | 1968-04-09 | Nalco Chemical Co | Method of coagulation of low turbidity water |
| US3476552A (en) * | 1966-09-07 | 1969-11-04 | Mountain Copper Co Of Californ | Mercury process |
| DE1954828B2 (de) * | 1969-10-31 | 1974-07-18 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Verringerung der Quecksilber-Verluste bei der Chlor-Alkali-Elektrolyse nach dem Amalgam-Verfahren |
| DE2057358C3 (de) * | 1970-11-21 | 1975-10-02 | Friedrich Uhde Gmbh, 4600 Dortmund | Verfahren zur Aufarbeitung von Abwasser mit Quecksilber-Verunreinigungen |
| US3674428A (en) * | 1970-12-22 | 1972-07-04 | Ppg Industries Inc | Mercury removal |
| US3847598A (en) * | 1970-12-31 | 1974-11-12 | Bp Chem Int Ltd | Mercury recovery process |
| US3857704A (en) * | 1971-03-05 | 1974-12-31 | Bp Chem Int Ltd | Mercury recovery process |
| US3764495A (en) * | 1971-04-21 | 1973-10-09 | Allied Chem | Removal of mercury from caustic solutions |
| US3740331A (en) * | 1971-06-23 | 1973-06-19 | Sybron Corp | Method for precipitation of heavy metal sulfides |
| JPS5112188B2 (de) * | 1972-03-02 | 1976-04-16 | ||
| SE399869B (sv) * | 1973-08-09 | 1978-03-06 | Montedison Spa | Sett att avlegsna kvicksilver eller kvicksilversalter fran ett vetskeavflode medelst tiokarbamid eller ett hydroxyl-aminsalt |
| FR2291156A1 (fr) * | 1974-11-18 | 1976-06-11 | Potasse & Produits Chimiques | Procede de demercurisation de liqueurs ou de solutions polluees |
-
1974
- 1974-08-05 SE SE7410019A patent/SE399869B/xx not_active IP Right Cessation
- 1974-08-05 NL NLAANVRAGE7410471,A patent/NL178962C/xx not_active IP Right Cessation
- 1974-08-06 CA CA206,637A patent/CA1031875A/en not_active Expired
- 1974-08-06 SU SU742048216A patent/SU865124A3/ru active
- 1974-08-06 DE DE2437779A patent/DE2437779A1/de not_active Withdrawn
- 1974-08-07 FR FR7427448A patent/FR2240192A1/fr active Granted
- 1974-08-09 BE BE147475A patent/BE818695A/fr not_active IP Right Cessation
- 1974-08-09 JP JP49090891A patent/JPS5741991B2/ja not_active Expired
-
1976
- 1976-02-18 US US05/658,976 patent/US4087359A/en not_active Expired - Lifetime
- 1976-06-04 ES ES429069A patent/ES429069A1/es not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110642447A (zh) * | 2019-09-12 | 2020-01-03 | 上海申欣环保实业有限公司 | 废水脱氯除汞的方法及处理设备 |
Also Published As
| Publication number | Publication date |
|---|---|
| NL178962C (nl) | 1986-06-16 |
| FR2240192B1 (de) | 1979-02-09 |
| JPS5044976A (de) | 1975-04-22 |
| JPS5741991B2 (de) | 1982-09-06 |
| NL178962B (nl) | 1986-01-16 |
| SE399869B (sv) | 1978-03-06 |
| DE2437779A1 (de) | 1975-02-20 |
| SU865124A3 (ru) | 1981-09-15 |
| US4087359A (en) | 1978-05-02 |
| ES429069A1 (es) | 1977-01-16 |
| NL7410471A (nl) | 1975-02-11 |
| FR2240192A1 (en) | 1975-03-07 |
| CA1031875A (en) | 1978-05-23 |
| SE7410019L (de) | 1975-02-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RE20 | Patent expired |
Owner name: MONTEDISON S.P.A. Effective date: 19940809 |