AU2014332576B2 - Process for removal of sulphur from raw methanol - Google Patents

Process for removal of sulphur from raw methanol Download PDF

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Publication number
AU2014332576B2
AU2014332576B2 AU2014332576A AU2014332576A AU2014332576B2 AU 2014332576 B2 AU2014332576 B2 AU 2014332576B2 AU 2014332576 A AU2014332576 A AU 2014332576A AU 2014332576 A AU2014332576 A AU 2014332576A AU 2014332576 B2 AU2014332576 B2 AU 2014332576B2
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AU
Australia
Prior art keywords
methanol
organic solvent
polar organic
washing
raw
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Active
Application number
AU2014332576A
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English (en)
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AU2014332576A1 (en
Inventor
Anders Eliasson
Johan Olsson Slager
Jan Warnqvist
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Andritz Oy
Original Assignee
Andritz Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Publication of AU2014332576A1 publication Critical patent/AU2014332576A1/en
Assigned to ANDRITZ OY reassignment ANDRITZ OY Request for Assignment Assignors: INVICO METANOL AB
Application granted granted Critical
Publication of AU2014332576B2 publication Critical patent/AU2014332576B2/en
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/84—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by extractive distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0488—Flow sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0492—Applications, solvents used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/48—Sulfur compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C27/00—Processes involving the simultaneous production of more than one class of oxygen-containing compounds
    • C07C27/26—Purification; Separation; Stabilisation
    • C07C27/34—Purification; Separation; Stabilisation by extraction
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/02—Monohydroxylic acyclic alcohols
    • C07C31/04—Methanol
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Paper (AREA)
AU2014332576A 2013-10-11 2014-10-13 Process for removal of sulphur from raw methanol Active AU2014332576B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
SE1351209 2013-10-11
SE1351209-0 2013-10-11
PCT/SE2014/051205 WO2015053704A1 (en) 2013-10-11 2014-10-13 Process for removal of sulphur from raw methanol

Publications (2)

Publication Number Publication Date
AU2014332576A1 AU2014332576A1 (en) 2016-04-28
AU2014332576B2 true AU2014332576B2 (en) 2018-02-22

Family

ID=52813419

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2014332576A Active AU2014332576B2 (en) 2013-10-11 2014-10-13 Process for removal of sulphur from raw methanol

Country Status (13)

Country Link
US (1) US10160706B2 (enExample)
EP (1) EP3055280B1 (enExample)
JP (1) JP6577462B2 (enExample)
CN (1) CN105793220B (enExample)
AU (1) AU2014332576B2 (enExample)
CA (1) CA2926589C (enExample)
CL (1) CL2016000786A1 (enExample)
ES (1) ES2732048T3 (enExample)
NZ (1) NZ718740A (enExample)
PT (1) PT3055280T (enExample)
RU (1) RU2672732C2 (enExample)
SE (1) SE539579C2 (enExample)
WO (1) WO2015053704A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE1850706A1 (en) * 2018-06-11 2019-12-12 Valmet Oy A method and a system for obtaining methanol from foul condensate of a pulping process
SE542491C2 (en) * 2018-07-10 2020-05-19 Stora Enso Oyj Method for desulfurization of crude sulfate turpentine
SE542659C2 (en) 2018-07-10 2020-06-23 Stora Enso Oyj Method for desulfurization of methanol
SE2050074A1 (en) * 2020-01-28 2021-01-29 Soedra Skogsaegarna Ekonomisk Foerening Process for producing one, or more, compounds
FI130591B (en) * 2020-06-30 2023-11-28 Andritz Oy Crude methanol purification method
WO2022031967A1 (en) * 2020-08-06 2022-02-10 Air Company Holdings, Inc. Alloys and methods for enhanced impurity removal in distillation processes
SE544418C2 (en) * 2020-09-22 2022-05-17 Mill Solution And Tech Ab Method for separation of reduced nitrogen and reduced sulphur from a feed of foul methanol vapor

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013067287A1 (en) * 2011-11-03 2013-05-10 Fluor Technologies Corporation Conversion of organosulfur compounds to hydrogen sulfide in mixed alcohol synthesis reactor effluent

Family Cites Families (18)

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Publication number Priority date Publication date Assignee Title
FI52710C (fi) * 1976-04-22 1977-11-10 Kemi Oy Menetelmä sulfaattiprosessin lauhteista erotetun metanolin puhdistamis eksi.
JPS63135342A (ja) * 1986-11-28 1988-06-07 Jgc Corp エタノ−ル又はメタノ−ル液の精製方法
SE463670B (sv) 1988-10-11 1991-01-07 Eka Nobel Ab Foerfarande foer framstaellning av klordioxid
GB8927266D0 (en) * 1989-12-01 1990-01-31 Csir Production of methanol
US5138101A (en) * 1991-07-19 1992-08-11 Eastman Kodak Company Recovery of high-boiling aldehydes from rhodium-catalyzed hydroformylation processes
US5450892A (en) 1993-03-29 1995-09-19 Alliedsignal Inc. Alkaline scrubber for condensate stripper off-gases
US5718810A (en) * 1996-03-19 1998-02-17 The Dow Chemical Company Methanol recovery using extractive distillation
JP2001181265A (ja) * 1999-12-22 2001-07-03 Wako Pure Chem Ind Ltd メルカプトテトラゾール化合物の製造方法
JP3720713B2 (ja) * 2000-02-22 2005-11-30 三菱レイヨン株式会社 ２−（メタ）アクリロイルオキシメチル−２−メチルビシクロ［２．２．１］ヘプタン、その製造方法、その原料アルコールの精製方法、その原料アルデヒドの製造方法、および、その（共）重合体
AU2003224812A1 (en) * 2002-04-01 2003-10-20 E.I. Du Pont De Nemours And Company Preparation of levulinic acid esters and formic acid esters from biomass and olefins
JP2005089347A (ja) * 2003-09-16 2005-04-07 Mitsubishi Heavy Ind Ltd アルコールと水の分離方法及びその装置
FI20085400A0 (fi) 2007-11-09 2008-04-30 Upm Kymmene Oyj Menetelmä jäteveden integroidulle käsittelylle
SE531478C2 (sv) 2007-11-26 2009-04-21 Processum Biorefinery Initiative Ab Förfarande för utvinning av ammoniumsalt och metanol ur vätska emanerande från orent kondensat, som uppstår vid cellulosamassaframställning
NZ594625A (en) 2009-02-12 2013-06-28 A H Lundberg Systems Ltd Methanol purification from stripper off gas produced during the kraft pulping process and apparatus
FI127304B (fi) * 2011-02-03 2018-03-15 Stora Enso Oyj Menetelmä puhdistetun metanolin valmistamiseksi sulfaattisellukeiton lauhteesta
CN202398144U (zh) * 2011-12-28 2012-08-29 惠生（南京）清洁能源股份有限公司 一种甲醇预精馏塔二级水冷产物的分离装置
US20130172633A1 (en) * 2011-12-29 2013-07-04 Celanese International Corporation Process For Producing Ethanol From Impure Methanol
CN105324357B (zh) 2013-06-19 2018-05-29 Fp创新研究中心 用于在纸浆厂生产生物甲醇的方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013067287A1 (en) * 2011-11-03 2013-05-10 Fluor Technologies Corporation Conversion of organosulfur compounds to hydrogen sulfide in mixed alcohol synthesis reactor effluent

Also Published As

Publication number Publication date
RU2016112932A3 (enExample) 2018-06-07
CA2926589C (en) 2022-08-02
PT3055280T (pt) 2019-06-28
CA2926589A1 (en) 2015-04-16
JP6577462B2 (ja) 2019-09-18
ES2732048T3 (es) 2019-11-20
WO2015053704A1 (en) 2015-04-16
RU2016112932A (ru) 2017-11-16
NZ718740A (en) 2019-02-22
EP3055280B1 (en) 2019-04-17
SE539579C2 (en) 2017-10-17
AU2014332576A1 (en) 2016-04-28
JP2016536290A (ja) 2016-11-24
SE1650632A1 (en) 2016-05-11
US10160706B2 (en) 2018-12-25
CL2016000786A1 (es) 2016-10-21
US20160237011A1 (en) 2016-08-18
RU2672732C2 (ru) 2018-11-19
CN105793220B (zh) 2018-10-09
EP3055280A1 (en) 2016-08-17
CN105793220A (zh) 2016-07-20
EP3055280A4 (en) 2017-06-14

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Owner name: ANDRITZ OY

Free format text: FORMER APPLICANT(S): INVICO METANOL AB

FGA Letters patent sealed or granted (standard patent)