CN105793220B - 从粗制甲醇去除硫的工艺 - Google Patents

从粗制甲醇去除硫的工艺 Download PDF

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Publication number
CN105793220B
CN105793220B CN201480066761.5A CN201480066761A CN105793220B CN 105793220 B CN105793220 B CN 105793220B CN 201480066761 A CN201480066761 A CN 201480066761A CN 105793220 B CN105793220 B CN 105793220B
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methanol
organic solvent
polar organic
crude
washing
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Chinese (zh)
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CN105793220A (zh
Inventor
J·沃恩奎斯特
J·奥尔森斯拉格
A·埃利亚森
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Andritz Oy
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Andritz Oy
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/84—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0488—Flow sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0492—Applications, solvents used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/48—Sulfur compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C27/00—Processes involving the simultaneous production of more than one class of oxygen-containing compounds
    • C07C27/26—Purification; Separation; Stabilisation
    • C07C27/34—Purification; Separation; Stabilisation by extraction
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/02—Monohydroxylic acyclic alcohols
    • C07C31/04—Methanol
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Paper (AREA)
CN201480066761.5A 2013-10-11 2014-10-13 从粗制甲醇去除硫的工艺 Active CN105793220B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
SE1351209-0 2013-10-11
SE1351209 2013-10-11
PCT/SE2014/051205 WO2015053704A1 (en) 2013-10-11 2014-10-13 Process for removal of sulphur from raw methanol

Publications (2)

Publication Number Publication Date
CN105793220A CN105793220A (zh) 2016-07-20
CN105793220B true CN105793220B (zh) 2018-10-09

Family

ID=52813419

Family Applications (1)

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CN201480066761.5A Active CN105793220B (zh) 2013-10-11 2014-10-13 从粗制甲醇去除硫的工艺

Country Status (13)

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US (1) US10160706B2 (enExample)
EP (1) EP3055280B1 (enExample)
JP (1) JP6577462B2 (enExample)
CN (1) CN105793220B (enExample)
AU (1) AU2014332576B2 (enExample)
CA (1) CA2926589C (enExample)
CL (1) CL2016000786A1 (enExample)
ES (1) ES2732048T3 (enExample)
NZ (1) NZ718740A (enExample)
PT (1) PT3055280T (enExample)
RU (1) RU2672732C2 (enExample)
SE (1) SE539579C2 (enExample)
WO (1) WO2015053704A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE1850706A1 (en) * 2018-06-11 2019-12-12 Valmet Oy A method and a system for obtaining methanol from foul condensate of a pulping process
SE542491C2 (en) * 2018-07-10 2020-05-19 Stora Enso Oyj Method for desulfurization of crude sulfate turpentine
SE542659C2 (en) 2018-07-10 2020-06-23 Stora Enso Oyj Method for desulfurization of methanol
SE2050074A1 (en) * 2020-01-28 2021-01-29 Soedra Skogsaegarna Ekonomisk Foerening Process for producing one, or more, compounds
FI130591B (en) * 2020-06-30 2023-11-28 Andritz Oy Crude methanol purification method
US20230286888A1 (en) * 2020-08-06 2023-09-14 Air Company Holdings, Inc. Alloys and methods for enhanced impurity removal in distillation processes
SE544418C2 (en) * 2020-09-22 2022-05-17 Mill Solution And Tech Ab Method for separation of reduced nitrogen and reduced sulphur from a feed of foul methanol vapor

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63135342A (ja) * 1986-11-28 1988-06-07 Jgc Corp エタノ−ル又はメタノ−ル液の精製方法
EP0430699A2 (en) * 1989-12-01 1991-06-05 Csir Production of methanol
JP2005089347A (ja) * 2003-09-16 2005-04-07 Mitsubishi Heavy Ind Ltd アルコールと水の分離方法及びその装置
CN202398144U (zh) * 2011-12-28 2012-08-29 惠生（南京）清洁能源股份有限公司 一种甲醇预精馏塔二级水冷产物的分离装置

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI52710C (fi) 1976-04-22 1977-11-10 Kemi Oy Menetelmä sulfaattiprosessin lauhteista erotetun metanolin puhdistamis eksi.
SE463670B (sv) 1988-10-11 1991-01-07 Eka Nobel Ab Foerfarande foer framstaellning av klordioxid
US5138101A (en) * 1991-07-19 1992-08-11 Eastman Kodak Company Recovery of high-boiling aldehydes from rhodium-catalyzed hydroformylation processes
US5450892A (en) 1993-03-29 1995-09-19 Alliedsignal Inc. Alkaline scrubber for condensate stripper off-gases
US5718810A (en) * 1996-03-19 1998-02-17 The Dow Chemical Company Methanol recovery using extractive distillation
JP2001181265A (ja) * 1999-12-22 2001-07-03 Wako Pure Chem Ind Ltd メルカプトテトラゾール化合物の製造方法
JP3720713B2 (ja) * 2000-02-22 2005-11-30 三菱レイヨン株式会社 ２−（メタ）アクリロイルオキシメチル−２−メチルビシクロ［２．２．１］ヘプタン、その製造方法、その原料アルコールの精製方法、その原料アルデヒドの製造方法、および、その（共）重合体
KR20040105819A (ko) * 2002-04-01 2004-12-16 이 아이 듀폰 디 네모아 앤드 캄파니 생물 자원 및 올레핀으로부터 레불린산 에스테르 및포름산 에스테르의 제조 방법
FI20085400A0 (fi) 2007-11-09 2008-04-30 Upm Kymmene Oyj Menetelmä jäteveden integroidulle käsittelylle
SE531478C2 (sv) * 2007-11-26 2009-04-21 Processum Biorefinery Initiative Ab Förfarande för utvinning av ammoniumsalt och metanol ur vätska emanerande från orent kondensat, som uppstår vid cellulosamassaframställning
ES2698367T3 (es) 2009-02-12 2019-02-04 A H Lundberg Systems Ltd Procedimiento y aparato de purificación de metanol
FI127304B (fi) * 2011-02-03 2018-03-15 Stora Enso Oyj Menetelmä puhdistetun metanolin valmistamiseksi sulfaattisellukeiton lauhteesta
US8721995B2 (en) * 2011-11-03 2014-05-13 Fluor Technologies Corporation Conversion of organosulfur compounds to hydrogen sulfide in mixed alcohol synthesis reactor effluent
US20130172633A1 (en) * 2011-12-29 2013-07-04 Celanese International Corporation Process For Producing Ethanol From Impure Methanol
CA2916012C (en) * 2013-06-19 2017-01-03 Fpinnovations Method for producing bio-methanol at pulp mills

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63135342A (ja) * 1986-11-28 1988-06-07 Jgc Corp エタノ−ル又はメタノ−ル液の精製方法
EP0430699A2 (en) * 1989-12-01 1991-06-05 Csir Production of methanol
JP2005089347A (ja) * 2003-09-16 2005-04-07 Mitsubishi Heavy Ind Ltd アルコールと水の分離方法及びその装置
CN202398144U (zh) * 2011-12-28 2012-08-29 惠生（南京）清洁能源股份有限公司 一种甲醇预精馏塔二级水冷产物的分离装置

Also Published As

Publication number Publication date
CA2926589C (en) 2022-08-02
EP3055280A4 (en) 2017-06-14
JP2016536290A (ja) 2016-11-24
RU2016112932A (ru) 2017-11-16
SE539579C2 (en) 2017-10-17
PT3055280T (pt) 2019-06-28
CN105793220A (zh) 2016-07-20
RU2016112932A3 (enExample) 2018-06-07
WO2015053704A1 (en) 2015-04-16
EP3055280B1 (en) 2019-04-17
AU2014332576A1 (en) 2016-04-28
US10160706B2 (en) 2018-12-25
CL2016000786A1 (es) 2016-10-21
NZ718740A (en) 2019-02-22
CA2926589A1 (en) 2015-04-16
JP6577462B2 (ja) 2019-09-18
AU2014332576B2 (en) 2018-02-22
ES2732048T3 (es) 2019-11-20
EP3055280A1 (en) 2016-08-17
SE1650632A1 (en) 2016-05-11
US20160237011A1 (en) 2016-08-18
RU2672732C2 (ru) 2018-11-19

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