ATE62236T1 - Verfahren zur herstellung von 5hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel. - Google Patents

Verfahren zur herstellung von 5hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel.

Info

Publication number
ATE62236T1
ATE62236T1 AT87100311T AT87100311T ATE62236T1 AT E62236 T1 ATE62236 T1 AT E62236T1 AT 87100311 T AT87100311 T AT 87100311T AT 87100311 T AT87100311 T AT 87100311T AT E62236 T1 ATE62236 T1 AT E62236T1
Authority
AT
Austria
Prior art keywords
solvent
water
hydroxymethylfurfuraldehyde
hmf
manufacture
Prior art date
Application number
AT87100311T
Other languages
German (de)
English (en)
Inventor
Knut M Dr Dipl-Chem Rapp
Original Assignee
Suedzucker Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suedzucker Ag filed Critical Suedzucker Ag
Application granted granted Critical
Publication of ATE62236T1 publication Critical patent/ATE62236T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Saccharide Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Furan Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
AT87100311T 1986-01-17 1987-01-13 Verfahren zur herstellung von 5hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel. ATE62236T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19863601281 DE3601281A1 (de) 1986-01-17 1986-01-17 Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
EP87100311A EP0230250B1 (de) 1986-01-17 1987-01-13 Verfahren zur Herstellung von 5-Hydroxymethylfurfural einschliesslich eines kristallinen Produktes unter ausschliesslicher Verwendung von Wasser als Lösungsmittel

Publications (1)

Publication Number Publication Date
ATE62236T1 true ATE62236T1 (de) 1991-04-15

Family

ID=6292062

Family Applications (1)

Application Number Title Priority Date Filing Date
AT87100311T ATE62236T1 (de) 1986-01-17 1987-01-13 Verfahren zur herstellung von 5hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel.

Country Status (4)

Country Link
US (1) US4740605A (ref)
EP (1) EP0230250B1 (ref)
AT (1) ATE62236T1 (ref)
DE (2) DE3601281A1 (ref)

Families Citing this family (64)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3936522A1 (de) * 1989-11-02 1991-05-08 Suedzucker Ag 5-((alpha)-d-glucopyranosyloxymethyl)-furan-2-carboxaldehyd und dessen derivate und folgeprodukte sowie verfahren zur herstellung der verbindungen und deren verwendung
FR2741345B1 (fr) * 1995-11-20 1998-08-07 Agrichimie Sa Procede et installation de condensation selective d'un derive aromatique avec un derive carbonyle dans un reacteur continu multicontact vertical
FR2741344B1 (fr) * 1995-11-20 1998-01-23 Agrichimie Sa Procede et installation de fabrication selective d'hydroxymethylfurfural par hydroxymethylation du furfural
US6603026B2 (en) 2001-08-07 2003-08-05 Gene E. Lightner Heterocyclic compounds produced from biomass
US6441202B1 (en) 2001-08-20 2002-08-27 Gene E. Lightner Heterocyclic compounds extracted by a hydrocarbon
US6706900B2 (en) * 2001-09-17 2004-03-16 E. I. Du Pont De Nemours And Company Process for preparing 2,5-diformylfuran from carbohydrates
US7317116B2 (en) 2004-12-10 2008-01-08 Archer-Daniels-Midland-Company Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives
US7393963B2 (en) 2004-12-10 2008-07-01 Archer-Daniels-Midland Company Conversion of 2,5-(hydroxymethyl)furaldehyde to industrial derivatives, purification of the derivatives, and industrial uses therefor
EP1834950A1 (en) 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of 5-alkoxymethylfurfural ethers and their use
EP1834951A1 (en) 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of organic acid esters of 5-hydroxymethylfurfural and their use
JP2007261990A (ja) * 2006-03-28 2007-10-11 Canon Inc フラン−２，５−ジカルボン酸の製造方法
EP2032550B1 (en) * 2006-06-06 2013-11-20 Wisconsin Alumni Research Foundation Catalytic process for producing furan derivatives from carbohydrates in a biphasic reactor
US7880049B2 (en) * 2006-06-06 2011-02-01 Wisconsin Alumni Research Foundation Production of liquid alkanes in the jet fuel range (C8-C15) from biomass-derived carbohydrates
DE102007007629A1 (de) 2007-02-16 2008-08-21 Evonik Degussa Gmbh Verfahren zur Herstellung von 5-Hydroxymethyl-furfural über 5-Acyloxymethyl-furfural als Zwischenprodukt
DK2164975T3 (da) 2007-07-06 2012-05-29 Basf Se Fremgangsmåde til fremstilling af en koncentreret vandig glukoseopløsning af majs
CN101456851B (zh) * 2007-12-12 2012-10-24 中国科学院大连化学物理研究所 一种微波促进制备5-羟甲基糠醛的方法
MY169437A (en) * 2007-12-12 2019-04-10 Archer Daniels Midland Co Conversion of carbohydrates to hydroxy-methylfurfural (hmf) and derivatives
DE102008009933A1 (de) 2008-02-18 2009-08-20 Friedrich-Schiller-Universität Jena Verfahren zur Herstellung von 5-Hydroxymethylfurfural mit Hilfe von ionischen Flüssigkeiten
WO2009155297A1 (en) 2008-06-17 2009-12-23 Wisconsin Alumni Research Foundation Chemical transformation of lignocellulosic biomass into fuels and chemicals
US8669397B2 (en) 2009-06-13 2014-03-11 Rennovia, Inc. Production of adipic acid and derivatives from carbohydrate-containing materials
CA2763177C (en) * 2009-06-13 2017-08-01 Thomas R. Boussie Production of glutaric acid and derivatives from carbohydrate-containing materials
EP2440515B1 (en) * 2009-06-13 2018-08-15 Archer-Daniels-Midland Company Production of adipic acid and derivatives from carbohydrate-containing materials
US8314267B2 (en) * 2009-06-26 2012-11-20 Uop Llc Carbohydrate route to para-xylene and terephthalic acid
CN102498122B (zh) * 2009-07-01 2016-08-03 威斯康星校友研究基金会 生物质水解
US8669393B2 (en) * 2010-03-05 2014-03-11 Rennovia, Inc. Adipic acid compositions
CN101812039B (zh) * 2010-05-14 2012-09-26 天津大学 一种利用离子液体催化生成5－羟甲基糠醛的方法
US9770705B2 (en) 2010-06-11 2017-09-26 Rennovia Inc. Oxidation catalysts
TWI421243B (zh) * 2010-07-15 2014-01-01 Ind Tech Res Inst 製備５-羥甲基糠醛之方法及裝置
WO2012038969A1 (en) 2010-09-03 2012-03-29 Ganapati Dadasaheb Yadav Process for converting fructose into 5-hydroxymethylfurfural using a mesoporous silica based catalyst impregnated with rare earth metals
FR2975396B1 (fr) * 2011-05-16 2013-12-27 Centre Nat Rech Scient Procede de preparation de 5-hydroxymethylfurfural
DE102011053034A1 (de) 2011-08-26 2013-02-28 Ava-Co2 Schweiz Ag Verfahren zur Extraktion von Furfuralen aus Biomasse
IN2014CN03466A (ref) * 2011-10-12 2015-07-03 Novozymes As
CN104169263B (zh) 2011-12-13 2016-06-15 巴斯夫欧洲公司 在蒸汽存在下由己糖溶液制备5-羟甲基糠醛(hmf)
WO2013087523A1 (de) 2011-12-13 2013-06-20 Basf Se Abtrennung von 5-hydroxymethylfurfural (hmf) aus reaktionslösungen durch wasserdampf-destillation
US9162998B2 (en) 2011-12-13 2015-10-20 Basf Se Preparation of 5-hydroxymethylfurfural (HMF) from saccharide solutions in the presence of a solvent having a boiling point greater than 60° C. and less than 200° C. (at standard pressure, called low boiler for short)
US9169227B2 (en) 2011-12-13 2015-10-27 Basf Se Production of 5 hydroxymethyulfurfural (HMF) from hexose solutions in the presence of steam
RU2014128459A (ru) 2011-12-13 2016-02-10 Басф Се ПОЛУЧЕНИЕ 5-ГИДРОКСИМЕТИЛФУРФУРАЛЯ (ГМФ) ИЗ РАСТВОРОВ САХАРИДОВ В ПРИСУТСТВИИ РАСТВОРИТЕЛЯ С ТЕМПЕРАТУРОЙ КИПЕНИЯ БОЛЬШЕ 60оС И МЕНЬШЕ 200оС (ПРИ НОРМАЛЬНОМ ДАВЛЕНИИ, КОРОТКО НАЗЫВАЕМОГО НИЗКОКИПЯЩИМ РАСТВОРИТЕЛЕМ)
US9156802B2 (en) 2011-12-13 2015-10-13 Basf Se Separating off 5-hydroxymethylfurfural (HMF) from reaction solutions by steam distillation
AU2012364787A1 (en) * 2012-01-10 2014-07-03 Archer Daniels Midland Company Process for making HMF and HMF derivatives from sugars, with recovery of unreacted sugars suitable for direct fermentation to ethanol
AR089707A1 (es) 2012-01-18 2014-09-10 Rennovia Inc Proceso para la produccion de hexametilendiamina a partir de materiales que contienen carbohidratos y compuestos intermedios para la misma
WO2013138153A1 (en) 2012-03-12 2013-09-19 Archer Daniels Midland Company Process for making sugar and/or sugar alcohol dehydration products
EP2813494A1 (de) 2013-06-12 2014-12-17 Basf Se Verfahren zur Herstellung von 5-Hydroxymethylfurfural (HMF)
DE102013223496A1 (de) 2013-11-18 2015-05-21 Tesa Se Neuartiges Polyester geeignet zur Herstellung von Trägermaterialien für Klebebändern
EA201691459A1 (ru) 2014-01-27 2016-12-30 Ренновия Инк. Преобразование фруктозосодержащего исходного сырья в hmf-содержащий продукт
EP2985280A1 (en) 2014-08-11 2016-02-17 Reliance Industries Limited A process for synthesis of furfural or derivatives thereof
KR101629699B1 (ko) 2014-09-02 2016-06-14 한국화학연구원 5-히드록시메틸푸푸랄의 제조방법
JP2017537920A (ja) 2014-12-02 2017-12-21 レノビア インコーポレイテッド ５−ヒドロキシメチルフルフラールから２，５−ビスヒドロキシメチルフラン、２，５−ビス−ヒドロキシメチルテトラヒドロフラン、１，６−ヘキサンジオールおよび１，２，６−ヘキサントリオールを生成する工程
CA2990588C (en) * 2015-07-01 2020-04-14 Furanix Technologies B.V. Process for the preparation of a furfural derivative comprising neutralizing an acid reaction mixture
WO2017003293A1 (en) * 2015-07-01 2017-01-05 Furanix Technologies B.V. Process for the preparation of a furfural derivative
US11000781B2 (en) * 2015-11-04 2021-05-11 Ddp Specialty Electronic Materials Us 8, Llc Purifying aqueous solutions
EP3402787A4 (en) 2016-01-13 2019-11-27 Stora Enso Oyj PROCESS FOR THE PREPARATION OF 2,5-FURANDIC ACETIC ACID AND INTERMEDIATES AND DERIVATIVES THEREOF
WO2017184545A1 (en) * 2016-04-18 2017-10-26 Rennovia, Inc. Conversion of fructose-containing feedstocks to hmf-containing product
DE102016224073A1 (de) * 2016-12-02 2018-06-07 Südzucker AG Verbessertes HMF-Herstellungsverfahren
EP3366712A1 (de) * 2017-02-27 2018-08-29 AVALON Industries AG Neue hmf-oligomere
EP3652161A1 (en) 2017-07-12 2020-05-20 Stora Enso Oyj Purified 2,5-furandicarboxylic acid pathway products
CN107805230A (zh) * 2017-10-31 2018-03-16 安徽省利夫生物产业控股有限公司 一种由生物质制备5‑羟甲基糠醛的方法
EP3498699A1 (en) 2017-12-13 2019-06-19 Basf Se Chromatography method for the purification of furfural derivatives
DE102018208510A1 (de) * 2018-05-29 2019-12-05 Südzucker AG Salz- und Säuregemisch-katalysierte HMF-Herstellung
DE102018208507A1 (de) * 2018-05-29 2019-12-05 Südzucker AG Anolytfraktion-katalysierte HMF-Herstellung
KR102219915B1 (ko) 2019-04-10 2021-02-23 부산대학교 산학협력단 가스-액체 계면 플라즈마 공정을 이용한 술폰화된 고체산 촉매의 제조방법
KR102193018B1 (ko) 2019-04-23 2020-12-18 부산대학교 산학협력단 셀룰로오스 가수분해를 위한 -Cl 및 -SO3H의 이중 기능성을 갖는 탄소계 고체산 촉매 및 이의 제조방법
CN116082278A (zh) * 2021-11-05 2023-05-09 中国科学院宁波材料技术与工程研究所 一种提高制备5-羟甲基-2-呋喃甲醛选择性的方法
CN114805254A (zh) * 2022-04-11 2022-07-29 合肥利夫生物科技有限公司 一种5-羟甲基糠醛的制备方法
WO2025043536A1 (zh) * 2023-08-30 2025-03-06 乔璞科技股份有限公司 5-羟甲基糠醛的纯化方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2776948A (en) * 1953-08-03 1957-01-08 Dendrol Inc Synthetic resins derived from hydroxymethylfurfural and phenols
US2929823A (en) * 1956-11-26 1960-03-22 Merck & Co Inc Production of 5-hydroxymethylfurfural
FR2464260A1 (fr) * 1979-09-05 1981-03-06 Roquette Freres Procede de fabrication du 5-hydroxymethylfurfural
DE3309564A1 (de) * 1983-03-17 1984-09-20 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von 5-acetoxymethyl-furfural

Also Published As

Publication number Publication date
DE3601281C2 (ref) 1988-08-04
EP0230250A3 (en) 1988-08-31
EP0230250A2 (de) 1987-07-29
US4740605A (en) 1988-04-26
DE3768965D1 (de) 1991-05-08
DE3601281A1 (de) 1987-07-23
EP0230250B1 (de) 1991-04-03

Similar Documents

Publication Publication Date Title
ATE62236T1 (de) Verfahren zur herstellung von 5hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel.
DE69400496D1 (de) Verfahren zur Herstellung von Alkylpolyglucosiden
EP2423205B9 (en) Conversion of carbohydrates to hydroxymethylfurfural (HMF) and derivatives
Hirama et al. Use of the E-vinyloxyborane derived from S-phenyl propanethioate for stereospecific aldol-type condensation. A simplified synthesis of the prelog-djerassi lactonic acid
KR20020003400A (ko) 트리메틸올알칸 비스-모노 선형 포름알을 포함하는조성물의 처리
KR900017987A (ko) 아크릴산 에스테르의 제조방법
US3117156A (en) Preparation of acetoacetic acid esters from diketene and alcohol in the presence of an acid catalyst
US4775447A (en) Process for the production of 2,2-dimethoxypropane
MX9801490A (es) Proceso de produccion de olefinas terciarias mediante descomposicion de eter alquilico terciario, que incluye una primera etapa de purificacion mediante lavado con agua.
EP0376122A1 (de) Verfahren zur Herstellung von Caprolactam
US4270011A (en) Process for the production of tertiary butyl alcohol
Onaka et al. Regioselective ring-opening reactions of 2, 3-epoxy alcohols with sodium azide supported on zeolite CaY
US4097522A (en) Synthesis of m-benzoyl-hydratropic acid
US10227668B2 (en) Method for preparing fructose or xylulose from biomass containing glucose or xylose using butanol, and method for separating the same
EP0983993A1 (en) Process for producing allyl-2-hydroxyisobutyrate
SU681059A1 (ru) Способ получени 4,4-диметилдиоксана -1,3 и изоамиленовых спиртов
US4701561A (en) Separation of aldehydes from ketones via acid-catalyzed cyclotrimerization of the aldehyde
SU1010054A1 (ru) Способ получени бензоата натри
SU333830A1 (ref)
US4585893A (en) Process for producing 4-homoisotwistane-3-carboxylic acid
JPH0459304B2 (ref)
SU390081A1 (ru) Способ получения гр?г-бутилового эфира гидразинугольной кислоты
SU450810A1 (ru) Способ получени фосфорилированных сульфенамидов
SU727615A1 (ru) Способ получени метилвинилкетона
SU1393831A1 (ru) Способ получени фуронитрила

Legal Events

Date Code Title Description
REN Ceased due to non-payment of the annual fee