AR097387A1 - Proceso para la preparación de sales de n-acil aminoácido - Google Patents
Proceso para la preparación de sales de n-acil aminoácidoInfo
- Publication number
- AR097387A1 AR097387A1 ARP140103113A ARP140103113A AR097387A1 AR 097387 A1 AR097387 A1 AR 097387A1 AR P140103113 A ARP140103113 A AR P140103113A AR P140103113 A ARP140103113 A AR P140103113A AR 097387 A1 AR097387 A1 AR 097387A1
- Authority
- AR
- Argentina
- Prior art keywords
- amino acid
- acid salt
- fatty alkyl
- alkyl ester
- acyl amino
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/45—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups
- C07C233/46—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
- C07C233/47—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a hydrogen atom or to a carbon atom of an acyclic saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
- C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D207/04—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
- C07D207/10—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D207/16—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
- C07D233/64—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms, e.g. histidine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Se describen las composiciones de sal de N-acil aminoácido y un proceso mejorado para su fabricación a partir de ésteres de alquilo grasos. El proceso comprende hacer reaccionar un éster de alquilo graso con una sal de aminoácido en presencia de un catalizador de alcóxido a una presión de al menos 135,79 kPa (5 psig). Al menos 10 por ciento en moles de catalizador se utiliza en base a la cantidad de éster de alquilo graso utilizado como un reactante. La presión y un nivel mínimo de catalizador de alcóxido se necesitan para proporcionar altas conversiones de éster de alquilo graso y buenos rendimientos de la sal de N-acil aminoácido deseada. Las composiciones de sal de N-acil aminoácido resultantes tienen color suave, un nivel aceptable de jabones de ácido graso, y una pequeña proporción de subproductos di-acilados. Las mezclas de una sola fase producidas mediante la combinación de diversas sales de aminoácido con glicinatos, o mediante el uso de un exceso de ya sea el éster de alquilo graso o sal de aminoácido, promueven altas conversiones cuando las mezclas se hacen reaccionar para proporcionar la sal de N-acil aminoácido deseada.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361867500P | 2013-08-19 | 2013-08-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR097387A1 true AR097387A1 (es) | 2016-03-09 |
Family
ID=51392423
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP140103113A AR097387A1 (es) | 2013-08-19 | 2014-08-19 | Proceso para la preparación de sales de n-acil aminoácido |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US9593072B2 (es) |
| EP (1) | EP3036214B1 (es) |
| JP (1) | JP6595472B2 (es) |
| CN (1) | CN105531256B (es) |
| AR (1) | AR097387A1 (es) |
| BR (1) | BR112016003494B1 (es) |
| ES (1) | ES2670770T3 (es) |
| SG (1) | SG11201600835RA (es) |
| WO (1) | WO2015026538A1 (es) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101880791B1 (ko) * | 2015-10-08 | 2018-07-20 | 주식회사 엘지생활건강 | 아실 글리시네이트 또는 이의 염의 합성 방법 및 이를 사용한 인체 세정제 조성물 |
| CN106076192A (zh) * | 2016-06-30 | 2016-11-09 | 江南大学 | 一种制备脂肪酰基氨基酸类表面活性剂的方法 |
| CN111886218A (zh) * | 2017-12-21 | 2020-11-03 | 罗地亚经营管理公司 | 用于通过柯尔贝电解偶联反应制备伯二胺的方法 |
| CN109369439B (zh) * | 2018-12-06 | 2021-04-16 | 盐城工学院 | 一种n-酰基氨基酸型表面活性剂的制备方法 |
| CN112048048B (zh) * | 2020-09-16 | 2021-10-15 | 南京工业大学 | 一种聚氨酯发泡材料及其制备方法 |
| CN112079761B (zh) * | 2020-09-22 | 2021-12-24 | 陕西科技大学 | 一种双酰胺非离子表面活性剂及其合成方法和应用 |
| EP4256014A1 (en) | 2020-12-01 | 2023-10-11 | Basf Se | Process for preparing surfactant solutions with n-acyl amino acid salts |
| KR102464655B1 (ko) * | 2020-12-31 | 2022-11-07 | 노승호 | 알라닌계 계면활성제 조성물 및 이를 포함하는 인체 세정용 조성물 |
| CN112812031B (zh) * | 2021-01-28 | 2023-01-31 | 常州大学 | 一种n-酰基氨基酸型表面活性剂的制备方法 |
| EP4352189A1 (en) * | 2021-06-08 | 2024-04-17 | The Procter & Gamble Company | N-acyl amino acid surfactants and derivatives thereof |
| US20220403291A1 (en) * | 2021-06-08 | 2022-12-22 | The Procter & Gamble Company | Blends of n-acyl alaninates and other n-acyl amino acid surfactants and derivatives thereof |
| CN115703716A (zh) * | 2021-08-03 | 2023-02-17 | Hg生化有限公司 | 生产氨基酸基表面活性剂的方法 |
| CN114989030B (zh) * | 2022-07-06 | 2024-04-19 | 江苏东南纳米材料有限公司 | 一种n-月桂酰肌氨酸钠的制备方法 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL7100453A (es) | 1970-01-30 | 1971-08-03 | ||
| DE3003898A1 (de) * | 1980-02-02 | 1981-08-13 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur acylierung von aminocarbonsaeuren |
| FR2705341B1 (fr) * | 1993-05-17 | 1995-06-23 | Givauban Lavirotte | Procédé de préparation de mélanges d'acides aminés N-acylés, mélanges d'acides alpha aminés N-acylés, et leurs utilisations. |
| JPH09502720A (ja) * | 1993-09-14 | 1997-03-18 | ザ、プロクター、エンド、ギャンブル、カンパニー | カルボン酸エステルおよびアミノ酸塩からのアミド酸の合成 |
| EP0719248A1 (en) * | 1993-09-14 | 1996-07-03 | The Procter & Gamble Company | Synthesis of sarcosinate surfactants |
| JP3537489B2 (ja) * | 1993-10-25 | 2004-06-14 | 花王株式会社 | Ｎ−長鎖アシルアミノ酸及びその塩の製造法、並びに中間体アミドニトリル、及びその製造法 |
| DE4408957A1 (de) | 1994-03-17 | 1995-09-21 | Basf Ag | Verfahren zur Herstellung von N-Acylaminocarbonsäuren und N-Acylaminosulfonsäuren sowie deren Alkalimetallsalzen |
| DE4433977A1 (de) * | 1994-09-23 | 1996-03-28 | Basf Ag | Verfahren zur Herstellung von N-Acylaminocarbonsäuren und N-Acylaminosulfonsäuren sowie deren Alkalimetallsalzen |
| DE19525512A1 (de) * | 1995-07-13 | 1997-01-16 | Basf Ag | Verfahren zur Herstellung von N-Acylaminocarbonsäuren und N-Acylaminosulfonsäuren sowie deren Alkalimetallsalzen |
| WO2002057217A2 (de) | 2001-01-18 | 2002-07-25 | Cognis Deutschland Gmbh & Co. Kg | Verfahren zur herstellung von acylaminosäuren |
| US6703517B2 (en) | 2001-11-26 | 2004-03-09 | Ajinomoto Co., Inc. | Method for preparing N-long chain acyl neutral amino acid |
| ES2313068T3 (es) | 2003-10-03 | 2009-03-01 | Ajinomoto Co., Inc. | Composiciones detergentes y procedimiento para su produccion. |
| DE102006038853A1 (de) | 2006-08-18 | 2008-02-21 | Clariant International Limited | Verfahren zur Herstellung von Acylglycinaten mittels Direktoxidation |
| US7674759B2 (en) | 2007-09-05 | 2010-03-09 | Conopco, Inc. | Stable liquid cleansing compositions containing high level of fatty acid isethionate surfactant products having more than 10 wt. % of fatty acid/fatty soap content |
| DE102007055265A1 (de) | 2007-11-20 | 2009-05-28 | Clariant International Ltd. | Verfahren zur Herstellung von Acylglycinaten |
| US7807612B2 (en) | 2007-12-18 | 2010-10-05 | Conopco, Inc. | Fatty acyl isethionate product-containing liquid cleansing compositions stabilized with mixture of long chain and short chain fatty acids/fatty soaps |
| DE102008003825A1 (de) | 2008-01-10 | 2009-07-16 | Clariant International Ltd. | Verfahren zur Herstellung von Acylglycinaten mittels Direktoxidation |
| US7879780B2 (en) | 2008-09-23 | 2011-02-01 | Conopco, Inc. | Stable cleansing compositions containing fatty acyl isethionate surfactant products having more than 10 wt. % of fatty acid/fatty soap content using high level of polyol and methods thereof |
| US8105994B2 (en) | 2010-03-31 | 2012-01-31 | Conopco, Inc. | Personal wash cleanser comprising defined alkanoyl compounds, defined fatty acyl isethionate surfactant product and skin or hair benefit agent delivered in flocs upon dilution |
| US8822724B2 (en) * | 2010-07-28 | 2014-09-02 | Sumitomo Chemical Company, Limited | Method for producing carboxylic acid amide |
| US8658589B2 (en) | 2011-07-28 | 2014-02-25 | Conopco, Inc. | Fatty acyl amido based surfactant concentrates |
| US8853433B2 (en) * | 2011-07-28 | 2014-10-07 | Conopco, Inc. | General method for preparing fatty acyl amido based surfactants |
| US20130029899A1 (en) | 2011-07-28 | 2013-01-31 | Conopco, Inc., D/B/A Unilever | Concentrated fatty acyl amido surfactant compositions |
| US8653018B2 (en) | 2011-07-28 | 2014-02-18 | Conopco, Inc. | Fatty acyl amido based surfactant concentrates |
| US8981134B2 (en) | 2011-07-28 | 2015-03-17 | Conopco, Inc. | Amino acid salt containing compositions |
| US8853447B2 (en) * | 2011-07-28 | 2014-10-07 | Conopco, Inc. | General method for preparing fatty acyl amido based surfactants |
| US8822711B2 (en) | 2011-07-28 | 2014-09-02 | Conopco, Inc. | Method for preparing fatty acyl amido carboxylic acid based surfactants |
| US8697897B2 (en) | 2011-07-28 | 2014-04-15 | Conopco, Inc. | Method for preparing fatty acyl amido carboxylic acid based surfactants |
| US9156777B2 (en) | 2012-07-03 | 2015-10-13 | Stepan Company | Process for preparing N-acyl amino acid salts |
-
2014
- 2014-08-07 BR BR112016003494-5A patent/BR112016003494B1/pt active IP Right Grant
- 2014-08-07 ES ES14755276.4T patent/ES2670770T3/es active Active
- 2014-08-07 JP JP2016536289A patent/JP6595472B2/ja active Active
- 2014-08-07 WO PCT/US2014/050219 patent/WO2015026538A1/en active Application Filing
- 2014-08-07 EP EP14755276.4A patent/EP3036214B1/en active Active
- 2014-08-07 CN CN201480045382.8A patent/CN105531256B/zh active Active
- 2014-08-07 SG SG11201600835RA patent/SG11201600835RA/en unknown
- 2014-08-19 AR ARP140103113A patent/AR097387A1/es active IP Right Grant
-
2016
- 2016-02-05 US US15/017,465 patent/US9593072B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| WO2015026538A1 (en) | 2015-02-26 |
| JP2016528284A (ja) | 2016-09-15 |
| JP6595472B2 (ja) | 2019-10-23 |
| CN105531256B (zh) | 2017-11-07 |
| BR112016003494A2 (pt) | 2020-04-14 |
| US20160152555A1 (en) | 2016-06-02 |
| EP3036214B1 (en) | 2018-02-28 |
| SG11201600835RA (en) | 2016-03-30 |
| US9593072B2 (en) | 2017-03-14 |
| ES2670770T3 (es) | 2018-06-01 |
| CN105531256A (zh) | 2016-04-27 |
| EP3036214A1 (en) | 2016-06-29 |
| BR112016003494B1 (pt) | 2021-02-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant, registration |