AR093155A1 - Metodos para la produccion de 5-(halometil)furfural - Google Patents

Metodos para la produccion de 5-(halometil)furfural

Info

Publication number
AR093155A1
AR093155A1 ARP130103904A ARP130103904A AR093155A1 AR 093155 A1 AR093155 A1 AR 093155A1 AR P130103904 A ARP130103904 A AR P130103904A AR P130103904 A ARP130103904 A AR P130103904A AR 093155 A1 AR093155 A1 AR 093155A1
Authority
AR
Argentina
Prior art keywords
organic
furfural
phase
halomethyl
temperature
Prior art date
Application number
ARP130103904A
Other languages
English (en)
Original Assignee
Micromidas Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Micromidas Inc filed Critical Micromidas Inc
Publication of AR093155A1 publication Critical patent/AR093155A1/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Furan Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Reivindicación 1: Un método que comprende: a) obtener una materia prima de alimentación, un ácido acuoso y un solvente orgánico, en el cual la materia prima de alimentación comprende azúcares de seis carbonos; b) combinar la materia prima de alimentación, el ácido acuoso y el solvente orgánico para formar una mezcla de reacción; c) convertir por lo menos una porción de la materia prima de alimentación contenida en la mezcla de reacción a 5-(halometil)furfural a una temperatura de reacción adecuada para producir 5-(halometil)furfural, donde la mezcla de reacción comprende una fase orgánica y una fase acuosa, donde la fase orgánica comprende por lo menos una porción del solvente orgánico y por lo menos una porción del 5-(halometil)furfural y donde la fase acuosa comprende por lo menos una porción del ácido acuoso; d) separar por lo menos una porción de la fase orgánica de la fase acuosa de la mezcla de reacción a una temperatura de separación, donde la fase orgánica comprende por lo menos una porción del 5-(halometil)furfural y por lo menos una porción del solvente orgánico a la temperatura de separación; y e) enfriar la fase orgánica separada del paso (d) a una temperatura de aislamiento para producir una mezcla orgánica multifásica, donde la temperatura de aislamiento es más baja que la temperatura de separación y donde la mezcla orgánica multifásica comprende una o más fases de producto y una fase de solvente a la temperatura de aislamiento, en el cual cada una de dichas una o más fases de producto comprende por lo menos una porción del 5-(halometil)furfural y donde la fase de solvente comprende por lo menos una porción del solvente orgánico.
ARP130103904A 2012-10-26 2013-10-25 Metodos para la produccion de 5-(halometil)furfural AR093155A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201261719322P 2012-10-26 2012-10-26
US201361785836P 2013-03-14 2013-03-14

Publications (1)

Publication Number Publication Date
AR093155A1 true AR093155A1 (es) 2015-05-20

Family

ID=49578556

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP130103904A AR093155A1 (es) 2012-10-26 2013-10-25 Metodos para la produccion de 5-(halometil)furfural

Country Status (10)

Country Link
US (1) US9388151B2 (es)
EP (1) EP2917193A1 (es)
JP (1) JP2015533851A (es)
KR (1) KR20150072453A (es)
CN (1) CN104955817B (es)
AR (1) AR093155A1 (es)
BR (1) BR112015009121A2 (es)
MX (1) MX2015005251A (es)
TW (1) TW201431844A (es)
WO (1) WO2014066746A1 (es)

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CN103930411B (zh) 2011-06-09 2016-08-17 微麦德斯公司 使用多相反应器转化生物质以制备取代呋喃
CN109020930A (zh) 2013-03-14 2018-12-18 微麦德斯公司 5-(卤代甲基)糠醛的提纯方法
EP2970167A4 (en) 2013-03-14 2016-11-16 Micromidas Inc SOLID FORMS OF 5- (HALOMETHYL) FURFURAL AND PROCESS FOR THE PREPARATION THEREOF
EP3046914B1 (en) 2013-09-20 2022-09-21 Origin Materials Operating, Inc. Methods for producing 5-(halomethyl) furfural
EP3142997A1 (en) 2014-05-12 2017-03-22 Micromidas, Inc. Methods of producing compounds from 5-(halomethyl)furfural
TWI564074B (zh) * 2014-12-16 2017-01-01 財團法人工業技術研究院 糠醛化合物的氧化反應催化劑組成及其應用方法
CN105688988B (zh) 2014-12-16 2018-11-27 财团法人工业技术研究院 糠醛化合物的氧化反应催化剂及糠醛化合物的氧化方法
WO2016149461A1 (en) * 2015-03-18 2016-09-22 Micromidas, Inc. Methods for producing 5-(halomethyl)furfural
US11028221B2 (en) 2015-12-11 2021-06-08 SOCIETE ANONYME DES EAUX MINERALES D'EVIAN et en abrégé “S.A.E.M.E” PET polymer with an anti-crystallization comonomer that can be bio-sourced
CN106220592B (zh) * 2016-07-29 2019-03-15 厦门大学 一种由果糖在低共熔体/甲基异丁基甲酮双相体系中制备5-溴甲基糠醛的方法
TWI596092B (zh) * 2016-08-02 2017-08-21 遠東新世紀股份有限公司 用於製備5-(氯甲基)糠醛的方法
EP3498699A1 (en) 2017-12-13 2019-06-19 Basf Se Chromatography method for the purification of furfural derivatives
KR102660287B1 (ko) * 2018-01-31 2024-04-23 퓨라닉스 테크놀러지스 비.브이. 고상 리그노셀룰로오스 물질의 전환 방법
JP2021512102A (ja) * 2018-01-31 2021-05-13 フラニックス・テクノロジーズ・ベーフェー 固体リグノセルロース材料の変換の方法
KR102653924B1 (ko) * 2021-10-26 2024-04-03 한국화학연구원 5-클로로메틸푸르푸랄의 제조방법 및 그 시스템
AU2023229018A1 (en) 2022-03-04 2024-09-05 Avantium Knowledge Centre B.V. Method of extracting 5-chloromethylfurfural with an organic solvent from cellulosic fibers and man-made non-cellulosic fibers hydrolysed together with hydrochloric acid

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CN103930411B (zh) 2011-06-09 2016-08-17 微麦德斯公司 使用多相反应器转化生物质以制备取代呋喃
EP2744799A1 (en) 2011-08-18 2014-06-25 Danmarks Tekniske Universitet Purification of 5-hydroxymethylfurfural (hmf) by crystallization
SG11201502939WA (en) 2012-10-16 2015-05-28 Xf Technologies Inc Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde
CN109020930A (zh) 2013-03-14 2018-12-18 微麦德斯公司 5-(卤代甲基)糠醛的提纯方法
EP2970167A4 (en) 2013-03-14 2016-11-16 Micromidas Inc SOLID FORMS OF 5- (HALOMETHYL) FURFURAL AND PROCESS FOR THE PREPARATION THEREOF

Also Published As

Publication number Publication date
US9388151B2 (en) 2016-07-12
WO2014066746A1 (en) 2014-05-01
US20150266843A1 (en) 2015-09-24
CN104955817B (zh) 2017-04-05
MX2015005251A (es) 2015-10-29
BR112015009121A2 (pt) 2017-07-04
KR20150072453A (ko) 2015-06-29
JP2015533851A (ja) 2015-11-26
EP2917193A1 (en) 2015-09-16
TW201431844A (zh) 2014-08-16
CN104955817A (zh) 2015-09-30

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Legal Events

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FD Application declared void or lapsed, e.g., due to non-payment of fee