AR063179A1 - Elaboracion de particulas polimericas solidas discretas - Google Patents
Elaboracion de particulas polimericas solidas discretasInfo
- Publication number
- AR063179A1 AR063179A1 ARP070104458A ARP070104458A AR063179A1 AR 063179 A1 AR063179 A1 AR 063179A1 AR P070104458 A ARP070104458 A AR P070104458A AR P070104458 A ARP070104458 A AR P070104458A AR 063179 A1 AR063179 A1 AR 063179A1
- Authority
- AR
- Argentina
- Prior art keywords
- flow
- liquid precursor
- drops
- spheres
- polymerizable liquid
- Prior art date
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/12—Polymerisation in non-solvents
- C08F2/16—Aqueous medium
- C08F2/18—Suspension polymerisation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/318—Preparation characterised by the starting materials
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/336—Preparation characterised by gaseous activating agents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/342—Preparation characterised by non-gaseous activating agents
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/44—Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/14—Treatment of polymer emulsions
- C08F6/16—Purification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/14—Powdering or granulating by precipitation from solutions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0083—Nucleating agents promoting the crystallisation of the polymer matrix
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/13—Phenols; Phenolates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Materials Engineering (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Polymerisation Methods In General (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Abstract
Proceso para producir esferas solidas discretas de un material polimérico por ejemplo unir resina fenolica que tiene una estructura mesoporosa donde dicho proceso permite producir esferas de resina a escala industrial sin agregados de resinas que se acumulan rápidamente e interrumpen la produccion. El proceso comprende los pasos de: (a) combinar un flujo de un precursor líquido polimerizable, por ejemplo un novolac y hexamina como agente de entrecruzamiento disuelto en un primer líquido orgánico polar, por ejemplo etilenglicol con un flujo de un medio de suspension líquido que es un segundo líquido orgánico no polar en el cual el precursor líquido es sustancialmente o completamente inmiscible, por ejemplo aceite de transformador que contiene un aceite secante, (b) mezclar el flujo combinado para dispersar el precursor líquido polimerizable como gotas en el medio de suspension por ejemplo usando un mezclador estático en línea, (c) permitir que las gotas se polimericen en un flujo laminar del medio de suspension como para formar esferas solidas discretas que no se aglomeran, y (d) recuperar las esferas del medio de suspension. También se provee un aparato para formar esferas solidas discretas de material polimérico, donde dicho aparato comprende: una primera línea para transportar un flujo de un precursor líquido polimerizable, una segunda línea para transportar un flujo de un medio de dispersion en el cual el precursor líquido polimerizable es sustancialmente o completamente inmiscible; un mezclador en línea configurado para recibir un flujo combinado de la primera y segunda línea y para dispersar el precursor líquido polimerizable corno gotas en el medio de dispersion, una columna de polimerizacion vertical configurada para recibir el medio de dispersion con las gotas dispersas en el mismo para permitir que se polimerice el precursor líquido polimerizable mientras va descendiendo por la columna en un flujo descendente de medio de polimerizacion, y un recipiente en la base de la columna para recibir el flujo descendente de medio de dispersion y recolectar las esferas solidas polimerizadas. En otras realizaciones, se provee un método para carbonizar y activar un material carbonoso que comprende suministrar el material en un horno rotatorio con calentamiento externo que es mantenido a temperaturas carbonizantes y activantes, donde dicho horno tiene una pendiente descendente para que el material progrese a medida que rota, el horno tiene una atmosfera sustancialmente libre de oxigeno provista por una contracorriente de vapor o dioxido de carbono, y bafles anulares a intervalos a lo largo del horno para controlar el avance del material. Se provee además un horno rotatorio con calentamiento externo para carbonizar y activar un material carbonoso, que tiene un cuerpo rotatorio hueco que presenta una pendiente descendente hacia el extremo de descarga del mismo y que presenta a intervalos a lo largo de toda su longitud bafles anulares para controlar el avance del material carbonoso.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB0619974A GB0619974D0 (en) | 2006-10-09 | 2006-10-09 | Process |
GBGB0710007.6A GB0710007D0 (en) | 2007-05-24 | 2007-05-24 | Process |
Publications (1)
Publication Number | Publication Date |
---|---|
AR063179A1 true AR063179A1 (es) | 2008-12-30 |
Family
ID=38969316
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP070104458A AR063179A1 (es) | 2006-10-09 | 2007-10-09 | Elaboracion de particulas polimericas solidas discretas |
Country Status (10)
Country | Link |
---|---|
US (1) | US8383703B2 (es) |
EP (1) | EP2054342B1 (es) |
JP (2) | JP5358443B2 (es) |
KR (1) | KR101482283B1 (es) |
CN (1) | CN101952199B (es) |
AR (1) | AR063179A1 (es) |
BR (1) | BRPI0719161A2 (es) |
CA (1) | CA2665052C (es) |
RU (1) | RU2466931C2 (es) |
WO (1) | WO2008043983A2 (es) |
Families Citing this family (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8119555B2 (en) | 2008-11-20 | 2012-02-21 | R. J. Reynolds Tobacco Company | Carbonaceous material having modified pore structure |
US8511319B2 (en) | 2008-11-20 | 2013-08-20 | R. J. Reynolds Tobacco Company | Adsorbent material impregnated with metal oxide component |
RU2494182C2 (ru) * | 2009-01-13 | 2013-09-27 | Биогасоль Ипр Апс | Аппарат для обработки органического материала, такой как разрезание, вымачивание и/или промывка, и способ эксплуатации аппарата для обработки органического материала |
GB0921528D0 (en) | 2009-12-09 | 2010-01-27 | Mast Carbon Internat Ltd | Carbon and its use in blood cleansing applications |
TWI542407B (zh) | 2010-08-19 | 2016-07-21 | Meiji Co Ltd | Performance Evaluation Method and Amplification Method of Micro - granulation Device |
CA2808574C (en) * | 2010-08-19 | 2018-11-13 | Meiji Co., Ltd. | Particle size breakup apparatus |
JP2012116832A (ja) * | 2010-11-11 | 2012-06-21 | Sumitomo Chemical Co Ltd | 有害生物防除成分を含有する分散液の製造方法及びマイクロカプセルの製造方法 |
GB201204696D0 (en) | 2012-03-16 | 2012-05-02 | Ucl Business Plc | Therapy |
US9714172B2 (en) * | 2012-11-26 | 2017-07-25 | Georgia-Pacific Chemicals Llc | Preparation of polymeric resins and carbon materials |
GB201221227D0 (en) | 2012-11-26 | 2013-01-09 | Mast Carbon Internat Ltd | Carbon materials and their use |
GB201512468D0 (en) | 2015-07-16 | 2015-08-19 | C Tex Ltd And University Of Brighton | Shaped nanoporous bodies |
WO2018089294A1 (en) * | 2016-11-08 | 2018-05-17 | Dow Global Technologies Llc | Controlled particle size distribution |
JP2021508310A (ja) * | 2017-12-19 | 2021-03-04 | イムトリクス セラピューティクス、インコーポレイテッド | 気孔率が調整された材料ならびにその作製および使用方法 |
CN109179405A (zh) * | 2018-09-27 | 2019-01-11 | 凯瑞环保科技股份有限公司 | 一种利用废离子交换树脂制备炭化树脂的方法 |
JP2020059765A (ja) * | 2018-10-05 | 2020-04-16 | 国立大学法人 熊本大学 | 蛍光性重合体および蛍光性重合体の製造方法、ならびに蛍光性ポリマー粒子、分散液、複合体、蛍光性重合体の被覆方法 |
CN109850863B (zh) * | 2019-01-16 | 2020-10-13 | 浙江大学 | 一种类齿轮状介孔炭纳米球材料、制备方法及应用 |
CN115103715A (zh) * | 2020-03-02 | 2022-09-23 | 千禧年材料和设备公司 | 一种用于合成碳珠的方法 |
CN114685742B (zh) * | 2020-12-31 | 2024-03-29 | 上海昶法新材料有限公司 | 一种酚醛树脂的制备方法 |
Family Cites Families (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1505517A (en) | 1919-05-05 | 1924-08-19 | John C Woodruff | Process of activating carbon |
GB228954A (en) * | 1923-08-09 | 1925-02-09 | Johan Nicolaas Adolf Sauer | Improvements in and relating to processes for the production of active carbon |
US3620988A (en) * | 1968-10-31 | 1971-11-16 | Goodrich Co B F | Method of preparing bead-type polymers |
CH642564A5 (de) | 1979-10-26 | 1984-04-30 | Sulzer Ag | Statische mischvorrichtung. |
US4344821A (en) | 1979-11-19 | 1982-08-17 | Angelo Ii James F | Apparatus for continuously carbonizing and activating carbonaceous materials |
FR2484421A1 (fr) | 1980-06-13 | 1981-12-18 | Dia Prosim Sa France | Procede continu de polymerisation en lit fluidise |
CA1166413A (en) | 1980-10-30 | 1984-05-01 | Edward E. Timm | Process and apparatus for preparing uniform size polymer beads |
US4666673A (en) * | 1980-10-30 | 1987-05-19 | The Dow Chemical Company | Apparatus for preparing large quantities of uniform size drops |
US4487898A (en) * | 1981-06-12 | 1984-12-11 | Kanegafuchi Chemical Industry Co., Ltd. | Process of continuous suspension polymerization |
SU1610211A1 (ru) * | 1989-01-17 | 1990-11-30 | Предприятие П/Я Р-6956 | Вращающа с муфельна печь |
KR0161286B1 (ko) * | 1989-08-08 | 1999-01-15 | 엠. 윌킨스 | 중합방법과 반응기 |
IT1273678B (it) * | 1993-08-12 | 1997-07-09 | Bluecher Hasso Von | Processo per la produzione di carbone attivo |
RU2085486C1 (ru) * | 1994-01-01 | 1997-07-27 | Вячеслав Евгеньевич Чиликин | Способ получения сферического углеродного адсорбента |
AUPM807094A0 (en) * | 1994-09-09 | 1994-10-06 | Commonwealth Scientific And Industrial Research Organisation | Polymer beads and method for preparation thereof |
DE19600237A1 (de) | 1995-01-11 | 1996-07-18 | Bluecher Hasso Von | Verfahren zur Herstellung von körniger Aktivkohle |
DE19912154C5 (de) | 1999-03-17 | 2007-02-01 | Carbotex Produktions-Und Veredelungsbetriebe Gmbh | Verfahren zur Herstellung von geformter Aktivkohle |
DE19920794A1 (de) | 1999-05-06 | 2000-11-09 | Merck Patent Gmbh | Verfahren zur Herstellung von Perlpolymerisaten |
JP3777123B2 (ja) | 2000-04-28 | 2006-05-24 | ブリュッヒャー ゲゼルシャフト ミット ベシュレンクテル ハフツング | 球状活性炭を製造する方法 |
EP1289883B1 (de) * | 2000-05-24 | 2006-01-04 | Carbotex Produktions- und Veredelungsbetriebe GmbH | Verfahren zur herstellung von geformter aktivkohle |
GB0019417D0 (en) * | 2000-08-09 | 2000-09-27 | Mat & Separations Tech Int Ltd | Mesoporous carbons |
JP2003171405A (ja) * | 2001-12-04 | 2003-06-20 | Sekisui Chem Co Ltd | 樹脂微粒子の製造装置、および、この製造装置を用いた樹脂微粒子の製造方法 |
AU2003259124A1 (en) | 2002-07-15 | 2004-02-02 | Sulzer Chemtech Usa, Inc. | Assembly of crossing elements and method of constructing same |
EP1398083B1 (en) * | 2002-09-05 | 2005-10-26 | Rohm And Haas Company | A method of producing fine solid particles and dispersions thereof |
US6610798B1 (en) * | 2002-10-08 | 2003-08-26 | Nova Chemical Inc. | Controlled suspension polymerization process without mechanical agitation |
JP2005255910A (ja) * | 2004-03-12 | 2005-09-22 | Hitachi Chem Co Ltd | 高分子粒子分散物とその製造方法 |
US6943223B1 (en) * | 2004-04-27 | 2005-09-13 | Nova Chemicals Inc. | Controlled shear and turbulence flow pattern within a liquid in a vessel |
GB0506278D0 (en) * | 2005-03-29 | 2005-05-04 | British American Tobacco Co | Porous carbon materials and smoking articles and smoke filters therefor incorporating such materials |
CN101247884A (zh) * | 2005-05-23 | 2008-08-20 | 康奈尔研究基金股份有限公司 | 用于在微流控装置中执行界面反应的方法和系统 |
-
2007
- 2007-10-04 WO PCT/GB2007/003759 patent/WO2008043983A2/en active Application Filing
- 2007-10-04 US US12/444,839 patent/US8383703B2/en active Active
- 2007-10-04 JP JP2009531895A patent/JP5358443B2/ja not_active Expired - Fee Related
- 2007-10-04 CA CA2665052A patent/CA2665052C/en not_active Expired - Fee Related
- 2007-10-04 CN CN200780037656.9A patent/CN101952199B/zh not_active Expired - Fee Related
- 2007-10-04 BR BRPI0719161-8A patent/BRPI0719161A2/pt not_active IP Right Cessation
- 2007-10-04 KR KR1020097009577A patent/KR101482283B1/ko active IP Right Grant
- 2007-10-04 EP EP07824015.7A patent/EP2054342B1/en not_active Not-in-force
- 2007-10-04 RU RU2009117384/04A patent/RU2466931C2/ru not_active IP Right Cessation
- 2007-10-09 AR ARP070104458A patent/AR063179A1/es not_active Application Discontinuation
-
2013
- 2013-06-28 JP JP2013136644A patent/JP2013241605A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
BRPI0719161A2 (pt) | 2014-02-04 |
JP2013241605A (ja) | 2013-12-05 |
KR20090081383A (ko) | 2009-07-28 |
JP5358443B2 (ja) | 2013-12-04 |
US20100086469A1 (en) | 2010-04-08 |
JP2010511064A (ja) | 2010-04-08 |
CA2665052A1 (en) | 2008-04-17 |
US8383703B2 (en) | 2013-02-26 |
RU2009117384A (ru) | 2010-11-20 |
WO2008043983A3 (en) | 2010-03-25 |
CA2665052C (en) | 2014-12-09 |
EP2054342B1 (en) | 2019-07-31 |
CN101952199B (zh) | 2014-09-17 |
EP2054342A2 (en) | 2009-05-06 |
KR101482283B1 (ko) | 2015-01-13 |
RU2466931C2 (ru) | 2012-11-20 |
CN101952199A (zh) | 2011-01-19 |
WO2008043983A2 (en) | 2008-04-17 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG | Grant, registration | ||
FD | Application declared void or lapsed, e.g., due to non-payment of fee |