ZA922456B - Process for the preparation of phosphorus-containing l-amino acids,their derivatives and intermediates for this process - Google Patents

Process for the preparation of phosphorus-containing l-amino acids,their derivatives and intermediates for this process

Info

Publication number
ZA922456B
ZA922456B ZA922456A ZA922456A ZA922456B ZA 922456 B ZA922456 B ZA 922456B ZA 922456 A ZA922456 A ZA 922456A ZA 922456 A ZA922456 A ZA 922456A ZA 922456 B ZA922456 B ZA 922456B
Authority
ZA
South Africa
Prior art keywords
formula
amino acids
intermediates
phosphorus
derivatives
Prior art date
Application number
ZA922456A
Other languages
English (en)
Inventor
Michael Hoffmann
Hoffmann Michael
Original Assignee
Hoechst Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Ag filed Critical Hoechst Ag
Publication of ZA922456B publication Critical patent/ZA922456B/xx

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/44—Amides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/32—Esters thereof
    • C07F9/3205—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/3211—Esters of acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/20—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated the carbon skeleton being further substituted by halogen atoms or by nitro or nitroso groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C271/00—Derivatives of carbamic acids, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
    • C07C271/06—Esters of carbamic acids
    • C07C271/08—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms
    • C07C271/10—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atoms of the carbamate groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C271/22—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atoms of the carbamate groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of hydrocarbon radicals substituted by carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/01—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms
    • C07C311/02—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C311/03—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton having the nitrogen atoms of the sulfonamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C311/06—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton having the nitrogen atoms of the sulfonamide groups bound to hydrogen atoms or to acyclic carbon atoms to acyclic carbon atoms of hydrocarbon radicals substituted by carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/15—Sulfonamides having sulfur atoms of sulfonamide groups bound to carbon atoms of six-membered aromatic rings
    • C07C311/16—Sulfonamides having sulfur atoms of sulfonamide groups bound to carbon atoms of six-membered aromatic rings having the nitrogen atom of at least one of the sulfonamide groups bound to hydrogen atoms or to an acyclic carbon atom
    • C07C311/19—Sulfonamides having sulfur atoms of sulfonamide groups bound to carbon atoms of six-membered aromatic rings having the nitrogen atom of at least one of the sulfonamide groups bound to hydrogen atoms or to an acyclic carbon atom to an acyclic carbon atom of a hydrocarbon radical substituted by carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/301—Acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Furan Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
ZA922456A 1991-04-06 1992-04-03 Process for the preparation of phosphorus-containing l-amino acids,their derivatives and intermediates for this process ZA922456B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4111188 1991-04-06

Publications (1)

Publication Number Publication Date
ZA922456B true ZA922456B (en) 1992-11-25

Family

ID=6428975

Family Applications (1)

Application Number Title Priority Date Filing Date
ZA922456A ZA922456B (en) 1991-04-06 1992-04-03 Process for the preparation of phosphorus-containing l-amino acids,their derivatives and intermediates for this process

Country Status (12)

Country Link
US (1) US5442088A (xx)
EP (1) EP0508296B1 (xx)
JP (2) JP3236337B2 (xx)
KR (1) KR920019807A (xx)
AT (1) ATE130615T1 (xx)
AU (1) AU646938B2 (xx)
CA (1) CA2065128C (xx)
DE (1) DE59204389D1 (xx)
HU (1) HU213632B (xx)
IL (1) IL101488A (xx)
TW (1) TW353663B (xx)
ZA (1) ZA922456B (xx)

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DE4407197A1 (de) * 1994-03-04 1995-09-07 Hoechst Schering Agrevo Gmbh Verfahren zur Herstellung von /L/-Homoalanin-4-yl-(methyl)phosphinsäure und deren Salze durch Racematspaltung
US6528499B1 (en) * 2000-04-27 2003-03-04 Georgetown University Ligands for metabotropic glutamate receptors and inhibitors of NAALADase
CN100375748C (zh) * 2005-04-26 2008-03-19 华中师范大学 具有杀菌除草活性的取代苯氧乙酰氧基芳杂环基烃基次膦酸酯及其制备
CA2669127C (en) 2006-11-08 2016-09-13 Molecular Insight Pharmaceuticals, Inc. Heterodimers of glutamic acid
EP2706057B1 (en) 2008-12-05 2016-04-20 Molecular Insight Pharmaceuticals, Inc. Bis(imidazolyl)compounds and radionuclide complexes
BR112012000209B8 (pt) 2009-06-15 2021-07-27 Molecular Insight Pharm Inc heterodímeros de ácido glutâmico e seus processos de preparação
CA2860504A1 (en) 2012-01-06 2013-07-11 Molecular Insight Pharmaceuticals Metal complexes of poly(carboxyl)amine-containing ligands having an affinity for carbonic anhydrase ix
US9687876B2 (en) 2012-01-30 2017-06-27 Hemlock Semiconductor Corporation Method of repairing and/or protecting a surface in a reactor
WO2014110372A1 (en) 2013-01-14 2014-07-17 Molecular Insight Pharmaceuticals Triazine based radiopharmaceuticals and radioimaging agents
CN106045947A (zh) * 2016-06-23 2016-10-26 李建中 合成L‑草铵膦中间体(S)‑3‑氨基‑γ‑丁内酯盐酸盐的方法及应用
CN106083922B (zh) * 2016-08-23 2018-08-31 山东省农药科学研究院 一种精草铵膦的制备方法
CN108164560B (zh) * 2016-12-07 2019-12-13 中国科学院成都有机化学有限公司 草铵膦的制备方法
WO2020046403A1 (en) * 2018-08-31 2020-03-05 Muhammed Majeed Novel process for the preparation of enantiopure 3- enantiopure 3-amino tetrahydrofuran and its salts
CN109232644A (zh) * 2018-09-30 2019-01-18 武汉工程大学 草铵膦的合成方法
CN109369418A (zh) * 2018-10-10 2019-02-22 河南师范大学 一种节能环保型烷基苯胺类液体抗氧剂的连续合成工艺及合成装置
KR102183111B1 (ko) * 2019-01-11 2020-11-25 씨제이제일제당 (주) L-글루포시네이트 중간체 및 l-글루포시네이트 제조 방법
CN110386882A (zh) * 2019-08-12 2019-10-29 利尔化学股份有限公司 (s)-4-氯-2-((乙氧基羰基)氨基)丁酸乙酯的制备方法
WO2021143712A1 (zh) * 2020-01-13 2021-07-22 利尔化学股份有限公司 一种制备l-草铵膦中间体的方法
WO2021143713A1 (zh) * 2020-01-13 2021-07-22 利尔化学股份有限公司 制备l-草铵膦中间体的方法
IL292593B2 (en) * 2020-01-20 2023-11-01 Lier Chemical Co Ltd A method for preparing glufosinate
CN113248537B (zh) * 2020-02-11 2023-06-06 利尔化学股份有限公司 草铵膦的制备方法
AR126158A1 (es) * 2021-06-15 2023-09-27 Upl Ltd Proceso de una sola etapa para la preparación de un aminoácido quiral
CN117412950A (zh) * 2021-06-17 2024-01-16 钱德拉塞卡·达亚尔·穆达利亚尔 用于制备l-草铵膦的中间体的方法
BR112023011898A2 (pt) * 2021-07-20 2024-03-05 Lier Chemical Co Ltd Método de preparação para glufosinato
AR126485A1 (es) * 2021-07-20 2023-10-11 Lier Chemical Co Ltd Proceso para preparar glufosinato o análogos del mismo
EP4151643A1 (en) 2021-09-16 2023-03-22 Evonik Operations GmbH Improved process for production of phosphoesters of glufosinate precursors
WO2023051768A1 (zh) * 2021-09-30 2023-04-06 利尔化学股份有限公司 (s)-4-氯-2-氨基丁酸盐酸盐及(s)-4-氯-2-氨基丁酸酯的制备方法
CN115093339A (zh) * 2022-07-20 2022-09-23 永农生物科学有限公司 一种l-草铵膦中间体的合成方法
EP4371992A1 (en) 2022-11-17 2024-05-22 YongNong BioSciences Co., Ltd Methods of preparing glufosinate
WO2024175643A1 (en) 2023-02-23 2024-08-29 Basf Se A process for preparing l-glufosinate from cyanhydrine or cyanhydrine derivatives

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4265654A (en) * 1977-12-28 1981-05-05 Meiji Seika Kaisha Ltd. Herbicidal compositions
DE3048612C2 (de) * 1980-12-23 1982-12-02 Hoechst Ag, 6000 Frankfurt "Verfahren zur enzymatischen Trennung von L-2-Ami no-4-methylphosphinobuttersäure"
JPS59219297A (ja) * 1983-05-27 1984-12-10 Meiji Seika Kaisha Ltd 光学活性な〔（３−アミノ−３−カルボキシ）プロピル−１〕−ホスフイン酸誘導体の製造法
DE3542645A1 (de) * 1985-12-03 1987-06-04 Hoechst Ag Verfahren zur herstellung von l-homoalanin-4-yl(methyl)-phosphinsaeure sowie ihrer alkylester
DE3609818A1 (de) * 1986-03-22 1987-09-24 Hoechst Ag Verfahren zur herstellung von l-phosphinothricin(derivaten) sowie ihrer alkylester
DE3786707D1 (de) * 1986-06-04 1993-09-02 Hoechst Ag Verfahren zur herstellung von l-phosphinothricin durch transaminierung.
AU599985B2 (en) * 1986-06-09 1990-08-02 Meiji Seika Kaisha Ltd. New process for the production of L-2-amino-4- (hydroxymethyl-phosphinyl)-butyric acid
DE3817956A1 (de) * 1988-05-27 1989-12-07 Hoechst Ag Verfahren zur herstellung phosphorhaltiger l-aminosaeuren sowie ihrer ester und n-derivate

Also Published As

Publication number Publication date
US5442088A (en) 1995-08-15
JPH0665268A (ja) 1994-03-08
EP0508296B1 (de) 1995-11-22
JP2002080436A (ja) 2002-03-19
IL101488A (en) 2000-07-16
DE59204389D1 (de) 1996-01-04
CA2065128A1 (en) 1992-10-07
HU213632B (en) 1997-08-28
AU1402192A (en) 1992-10-08
TW353663B (en) 1999-03-01
ATE130615T1 (de) 1995-12-15
JP3860980B2 (ja) 2006-12-20
AU646938B2 (en) 1994-03-10
CA2065128C (en) 2006-05-30
HU9201143D0 (en) 1992-06-29
HUT62301A (en) 1993-04-28
IL101488A0 (en) 1992-12-30
JP3236337B2 (ja) 2001-12-10
EP0508296A1 (de) 1992-10-14
KR920019807A (ko) 1992-11-20

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