BR112023011898A2 - Método de preparação para glufosinato - Google Patents

Método de preparação para glufosinato

Info

Publication number
BR112023011898A2
BR112023011898A2 BR112023011898A BR112023011898A BR112023011898A2 BR 112023011898 A2 BR112023011898 A2 BR 112023011898A2 BR 112023011898 A BR112023011898 A BR 112023011898A BR 112023011898 A BR112023011898 A BR 112023011898A BR 112023011898 A2 BR112023011898 A2 BR 112023011898A2
Authority
BR
Brazil
Prior art keywords
glufosinate
preparation
ammonium
enantiomer
enantiomers
Prior art date
Application number
BR112023011898A
Other languages
English (en)
Inventor
Ke Cheng
Lei Zhou
Min Xu
Wei Zeng
Yongjiang Liu
Original Assignee
Lier Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lier Chemical Co Ltd filed Critical Lier Chemical Co Ltd
Publication of BR112023011898A2 publication Critical patent/BR112023011898A2/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/54—Quaternary phosphonium compounds
    • C07F9/5407—Acyclic saturated phosphonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/301—Acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C271/00—Derivatives of carbamic acids, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
    • C07C271/06—Esters of carbamic acids
    • C07C271/08—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms
    • C07C271/10—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atoms of the carbamate groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C271/22—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atoms of the carbamate groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of hydrocarbon radicals substituted by carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C237/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups
    • C07C237/02—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C237/04—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C237/06—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/23—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
    • C07C323/31—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton having the sulfur atom of at least one of the thio groups bound to a carbon atom of a six-membered aromatic ring of the carbon skeleton
    • C07C323/32—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton having the sulfur atom of at least one of the thio groups bound to a carbon atom of a six-membered aromatic ring of the carbon skeleton having at least one of the nitrogen atoms bound to an acyclic carbon atom of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
    • C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/57—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C323/58—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups with amino groups bound to the carbon skeleton
    • C07C323/59—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups with amino groups bound to the carbon skeleton with acylated amino groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/32—Esters thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)

Abstract

método de preparação para glufosinato. a presente invenção refere-se a um método de preparação para glufosinato de amônio ou um sal, um enantiômero ou uma mistura de enantiômeros em todas as proporções do mesmo, o método sendo especialmente apropriado para a preparação de glufosinato de amônio, e diminuindo grandemente as etapas em um processo de preparação existente. especialmente na preparação de l-glufosinato de amônio, o produto pode efetivamente manter o valor ee das matérias-primas
BR112023011898A 2021-07-20 2022-07-19 Método de preparação para glufosinato BR112023011898A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN202110817019 2021-07-20
PCT/CN2022/106398 WO2023001131A1 (zh) 2021-07-20 2022-07-19 草铵膦的制备方法

Publications (1)

Publication Number Publication Date
BR112023011898A2 true BR112023011898A2 (pt) 2024-03-05

Family

ID=84980040

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112023011898A BR112023011898A2 (pt) 2021-07-20 2022-07-19 Método de preparação para glufosinato

Country Status (13)

Country Link
US (1) US20230331750A1 (pt)
EP (1) EP4230634A4 (pt)
JP (1) JP2024500821A (pt)
KR (1) KR102631796B1 (pt)
CN (1) CN116368142A (pt)
AR (1) AR126480A1 (pt)
AU (1) AU2022314007B2 (pt)
BR (1) BR112023011898A2 (pt)
CA (1) CA3200300A1 (pt)
IL (1) IL303184B1 (pt)
MX (1) MX2023005220A (pt)
TW (1) TWI807923B (pt)
WO (1) WO2023001131A1 (pt)

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS53149926A (en) * 1977-05-18 1978-12-27 Kowa Co Methylmethionine sulfonium derivative
US5900237A (en) * 1983-11-29 1999-05-04 Igen International, Inc. Catalytic antibodies which hydrolyze primary amides and methods for eliciting such antibodies
TW353663B (en) * 1991-04-06 1999-03-01 Hoechst Ag Process for the preparation of phosphorus-containing L-amino acids, their derivatives and intermediates for this process
CN106083922B (zh) * 2016-08-23 2018-08-31 山东省农药科学研究院 一种精草铵膦的制备方法
CN109232644A (zh) * 2018-09-30 2019-01-18 武汉工程大学 草铵膦的合成方法
KR102582675B1 (ko) * 2019-01-11 2023-09-25 씨제이제일제당 주식회사 글루포시네이트 제조 방법
KR102183111B1 (ko) * 2019-01-11 2020-11-25 씨제이제일제당 (주) L-글루포시네이트 중간체 및 l-글루포시네이트 제조 방법
CN113490671B (zh) * 2020-01-20 2022-04-12 利尔化学股份有限公司 草铵膦的制备方法

Also Published As

Publication number Publication date
JP2024500821A (ja) 2024-01-10
EP4230634A1 (en) 2023-08-23
KR20230079459A (ko) 2023-06-07
IL303184A (en) 2023-07-01
MX2023005220A (es) 2023-05-16
AU2022314007B2 (en) 2023-09-14
EP4230634A4 (en) 2024-03-06
AU2022314007A1 (en) 2023-06-22
TWI807923B (zh) 2023-07-01
WO2023001131A1 (zh) 2023-01-26
AR126480A1 (es) 2023-10-11
CA3200300A1 (en) 2023-01-26
US20230331750A1 (en) 2023-10-19
KR102631796B1 (ko) 2024-01-30
TW202313644A (zh) 2023-04-01
CN116368142A (zh) 2023-06-30
IL303184B1 (en) 2024-05-01

Similar Documents

Publication Publication Date Title
BR112018067523A8 (pt) Métodos para preparar l-glufosinato
BR112016029906A8 (pt) formulação líquida, uso de formulação terapêutica líquida, uso de formulação terapêutica líquida injetável, método de melhoria da estabilidade de uma formulação proteica líquida e método de melhoria de um processo relacionado a proteínas
BR112014018859A8 (pt) Ração contendo ingredientes da ração adicionais e aditivos adicionais e outros agentes auxiliares, processo para preparação de uma ração, método para aumento do teor de gordura do leite e para aumento da produção de leite e ração composta de ruminantes
BR112017013748A2 (pt) método de produção & processamento de diaminas
BR112022003519A2 (pt) Forma cristalina de sal de l-glufosinato de amônio e processo para a sua produção
BR112016016342A2 (pt) Polipeptídeo variante que tem atividade de lactase, sequência de ácido nucleico, construto de ácido nucleico, vetor de expressão recombinante, método para produzir uma lactase, método para produzir uma variante de polipeptídeo de lactase, composição, uso de um polipeptídeo variante, processo para a produção de um produto lácteo e produto lácteo
BR112017003943A2 (pt) método para a produção de líquido de açúcar
BR112017025923A2 (pt) molécula de ácido nucleico recombinante, molécula de aminoácido recombinante, construto de expressão recombinante, vetor recombinante, micro-organismo recombinante, composição, métodos para produção de um micro-organismo recombinante e para cultivo e crescimento de um micro-organismo geneticamente modificado, uso de uma molécula de ácido nucleico recombinante, e, processo para produção fermentativa de um composto.
PH12017502056A1 (en) A biostimulant formulation for improving plant growth and uses thereof
BR112015002121A2 (pt) material de substituição óssea parcialmente purificado desidratado contendo grupo fosfato hidrofílico
BR112017014433A2 (pt) proteína dnase i modificada, processo para preparar proteína dnase i modificada e composição farmacêutica
BR112022020495A2 (pt) Composições compreendendo algas e métodos de uso das mesmas para aumentar a produção de produto animal
BR112023011898A2 (pt) Método de preparação para glufosinato
BR112021019072A2 (pt) Processo para enriquecimento de carotenoides em uma composição de ácido graxo
BR112017024341A2 (pt) processo de preparação de um extrato de ervilha
BR112018012355A2 (pt) composição dermocosmética, processo de produção da composição tópica, método para fortalecimento de unhas frágeis e uso da composição
BR112022025371A2 (pt) Composição agrícola para quebrar a dormência de gemas de plantas perenes lenhosas, e, métodos para promover brotação em plantas perenes lenhosas, para sincronizar brotação em plantas perenes lenhosas e para promover crescimento em plantas perenes lenhosas
BR112017007584A2 (pt) solução aquosa, processo para produzir uma solução aquosa uso de uma solução aquosa, e, mistura de sais de metal trialcalino dos enantiômeros l e d de ácido metil glicicina diacético.
BR112022016598A2 (pt) Métodos de preparação de composições de oligonucleotídeo utilizando ultrafiltração/diafiltração
BR102013004204B8 (pt) método de produção de material de aço rápido para ferramentas
ATE437869T1 (de) Verfahren zur herstellung von pyridinylmethyl-1h- benzimidazolverbindungen in enantiomerenangereicherter form oder als einzelne enantiomere
BR112017008026A2 (pt) processos de produção de composições com melhor perfil de segurança que possui atividade de lipase e composições apropriadas para uso farmacêutico
BR112015015880A2 (pt) processo para a produção do composto, composto de fórmula, preparação farmacêutica e compostos, composições, métodos e utilizações substancialmente inovadores
BR112018005934A2 (pt) formas cristalinas de intermediário de posaconazol e processo para a preparação de posaconazol amorfo
BR112017016494A2 (pt) composição para intensificar a produção de aglomerados de cristal, e, método para intensificar a produção e recuperação de aglomerados de cristal.