WO2019170651A1 - DECKELGEFÄß AUS KUNSTSTOFF FÜR DEN LABOREINSATZ - Google Patents

DECKELGEFÄß AUS KUNSTSTOFF FÜR DEN LABOREINSATZ Download PDF

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Publication number
WO2019170651A1
WO2019170651A1 PCT/EP2019/055410 EP2019055410W WO2019170651A1 WO 2019170651 A1 WO2019170651 A1 WO 2019170651A1 EP 2019055410 W EP2019055410 W EP 2019055410W WO 2019170651 A1 WO2019170651 A1 WO 2019170651A1
Authority
WO
WIPO (PCT)
Prior art keywords
vessel
lid
plug
lidded
sealing
Prior art date
Application number
PCT/EP2019/055410
Other languages
German (de)
English (en)
French (fr)
Inventor
Michael Blumentritt
Kai Holl
Original Assignee
Eppendorf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eppendorf Ag filed Critical Eppendorf Ag
Priority to US16/978,411 priority Critical patent/US11896976B2/en
Priority to CN201980017134.5A priority patent/CN111819002B/zh
Priority to JP2020546135A priority patent/JP7339269B2/ja
Publication of WO2019170651A1 publication Critical patent/WO2019170651A1/de

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L3/00Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
    • B01L3/50Containers for the purpose of retaining a material to be analysed, e.g. test tubes
    • B01L3/508Containers for the purpose of retaining a material to be analysed, e.g. test tubes rigid containers not provided for above
    • B01L3/5082Test tubes per se
    • B01L3/50825Closing or opening means, corks, bungs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L2200/00Solutions for specific problems relating to chemical or physical laboratory apparatus
    • B01L2200/06Fluid handling related problems
    • B01L2200/0684Venting, avoiding backpressure, avoid gas bubbles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L2200/00Solutions for specific problems relating to chemical or physical laboratory apparatus
    • B01L2200/06Fluid handling related problems
    • B01L2200/0689Sealing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L2300/00Additional constructional details
    • B01L2300/04Closures and closing means
    • B01L2300/041Connecting closures to device or container
    • B01L2300/042Caps; Plugs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L2300/00Additional constructional details
    • B01L2300/04Closures and closing means
    • B01L2300/041Connecting closures to device or container
    • B01L2300/043Hinged closures
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L2300/00Additional constructional details
    • B01L2300/04Closures and closing means
    • B01L2300/046Function or devices integrated in the closure
    • B01L2300/048Function or devices integrated in the closure enabling gas exchange, e.g. vents

Definitions

  • the invention relates to a lidded plastic container for laboratory use.
  • lidded vessels are also referred to as “reaction vessel” or “reaction vessel with lid”.
  • Known plastic lidded containers for laboratory use have a röhrenförmi ges vessel having a bottom of the vessel bottom, above a vessel opening and below the vessel opening on the inner wall has a sealing area.
  • a lid having a lid bottom and a stopper protruding from the inside of the lid bottom is insertable through the vessel opening into a sealing position in which the stopper seals at the sealing area.
  • the lid is held by the clamping force of the stop fens in the vessel.
  • a correspondingly high clamping force of the plug is required. To close and open the vessel, the user must spend a correspondingly high force.
  • Learners are known lidded containers in which the lid is connected via a hinge to the vessel.
  • Such lidded containers with openable and hinged lid are also referred to as "snap-lid container”.
  • Learners are known plastic lidded containers, which raise a special latch between the lid and vessel to hold the lid in the sealing position on the vessel.
  • EP 2 654 958 B1 describes a lidded container which, for easy and safe closing and easy opening, has a latching projection on the upper edge of the container and an elastic tab projecting from the underside of the lid bottom with a snap-in edge latching under the latching projection and one of the tabs laterally outwardly protruding button to unlock the lock Has locking edge with the locking projection.
  • a first lever protrudes laterally outward from the tab and projects from the first lever at a distance from the tab, a second lever upwards, in order to release the latching mechanism by pressing against the second lever.
  • lidded containers are shipped open to several in a bag protected from contamination. Delivery in a closed state does not take place, because in this case the sealing geometry would relax, so that the vessels no longer seal during use. As a result, it can come in particular special after removal of the vessels from the bag to contamination.
  • Another disadvantage is that the vessels for a labeling of the lid initially ge closed, then opened again for the filling of sample liquid and then closed again.
  • US 3,881,626 A describes a lidded container for lyophilized products.
  • a lid with a plug In the neck of a tubular vessel, a lid with a plug is used, having ventilation means.
  • the lid with the stopper In a venting position, the lid with the stopper is only partially inserted into the vessel mouth so that the venting means ventilate the interior of the vessel.
  • a sealing position In a sealing position, the lid is pushed into the neck until it rests against the mouth edge, so that the stopper seals in the neck and a rib projecting inward on a jacket of the lid is snapped with a bead on the outside of the neck.
  • the ventilation position is used for ventilation during lyophilization. In the ventilation position, the lidded container must stand upright as the lid is loosely inserted into the container.
  • US 3,164,279 A describes a test tube with a tube and a lid.
  • the lid is displaceable with a stopper in a ventilation position and in a deeper sealing position.
  • the plug on the mantle only partially encircling, interrupted bead and further up a ununterbroche nen bead. If the stopper is inserted into the coin with only the broken bead is pushed fertil of the vessel, it can pass through the interruption of the bead through air into the vessel interior or escape from it. When the plug is pushed deeper, seals the continuous bead on the inner wall of the vessel from.
  • the disadvantage is that the user can hardly control the achievement of the ventilation position and the sealing position.
  • the lid can be easily moved from the respective position.
  • the sealing area is stressed in the ventilation position and can relax.
  • EP 2 517 791 A1 describes a lidded vessel in which either a stopper of the lid has an interrupted sealing area further downwards or the vessel has an axial ventilation groove further up.
  • the interior of the vessel is vented with only partially inserted plug. Only when fully inserted to the plant of the lid at the mouth edge of the vessel stopper from a seal is achieved. Even with this lidded vessel, the ventilation position is not unique and the lid can be easily moved from the respective position who the.
  • WO 2011/108134 A1 describes a lidded container in which the stopper-like lid is connected to the container by means of a tab and has a snap connection at the outer edge with a pin projecting outwardly from the container and a clip projecting downwards from the lid. From the closed first position in which the stopper is guided concentrically in the vessel, the lid is pivotable by pushing the tab into a second position in which the stopper partially dips into the vessel and the snap connection is still be. This is to avoid that spilled liquid by the impulse when loosening the lid.
  • the snap connection can be released and the lid can be pivoted into a third position directed vertically to the opening, in which it is connected via a further snap connection to the vessel.
  • the lid can be pressed immediately from the third to the first position.
  • the lidded container is structurally complex and difficult to operate.
  • US 5,354,539 describes a lidded vessel in which the lid is flexibly connected to the vessel.
  • the lid has a plug with which the lid can be pressed into a sealing position in the vessel. From the sealing position, the lid is pivotable to a locked position in which the plug also seals in the vessel.
  • the sealing and locking of the lid requires various movements, whereby the handling is difficult.
  • the present invention seeks to provide a lidded container, which is better protected from contamination and handling friend Licher.
  • lidded vessel with the features of claim 1 ge.
  • Advantageous embodiments of the lid vessel are given in subclaims.
  • a tubular vessel having at the bottom a vessel bottom, at the top a vessel opening and below the vessel opening at the inside wall a sealing area,
  • a lid having a lid bottom and a protruding from the inside of the lid bottom plug, which is insertable through the vessel opening in a sealing position in which the plug sealingly abuts the sealing area, wherein the plug engages in a parking position in the vessel opening and not or engages with another portion in the sealing area, as in the sealing position, and • A first locking device with a first locking element on the inner wall of the vessel and a second locking element on the outside of the plug for releasably locking the lid with the vessel in the park position is present.
  • the lid can be placed in a parking position, in which the lid closes the vessel substantially or completely.
  • the lid In the parking position, the lid is held by the first latching device of the lidded vessel.
  • a relaxation of the plastic is avoided by tensions between sealing area and plug, which no longer allows sealing of the plug in the sealing area in the sealing position.
  • the lidded vessel can later be closed in a sealing manner.
  • the lid is brought into the sealing position, in which the plug rests sealingly on the sealing area. The tensions between the sealing area and the plug are large enough to seal the lidded vessel.
  • both the sealing area and the sealing area engaging portion of the plug are not subjected to any stresses or only low stresses at which the plastic relaxes only slightly so that sealing in the sealing position is still present he follows.
  • the first latching device has a first latching element on the inner wall of the vessel and a second latching element on the outside of the plug, so that the lid and vessel are simply locked together by pressing the plug into the vessel opening to the parking position.
  • the first locking device facilitates finding the parking position.
  • the lidded container is also particularly suitable This is good for automatically locking the cover in the parking position.
  • the production and the provision of a variety of lidded vessels in park positions in the bag is facilitated.
  • Correspondingly easy locking in the parking position can be selectively canceled.
  • Locking elements on the outside of the lidded container which complicate the handling, are square and can be easily opened by the action of force from the outside, eliminated.
  • a large number of lidded containers with the lid in parking position can be delivered in a bag. Since the lidded containers are closed, the risk of contaminants is reduced, especially after removal from the bag.
  • NEN extracted lidded vessels can be labeled immediately on the top of the lid, since they are already closed. By protected in the lidded container arranged first latching device unwanted opening or further closing Shen the lid due to external force in the bag or when labeling is avoided. Since in the parking position voltages between the plug and vessel can be avoided as in the sealing position, the opening of the lid after labeling for the filling of sample liquid can be easier than in conven- union vessels. When in the park position the plug seals in the vessel, relaxation of the plastic can facilitate opening the lid after labeling.
  • the stopper engages in the parking position in a parking area on the inner wall of the vessel, which is arranged above the sealing region Ches.
  • the parking position can be achieved by partially inserting the plug into the vessel. This simplifies the achievement of Park posi tion and the opening of the vessel.
  • the park area is disposed on the inner wall of the vessel below the sealing area. In order to reach the parking position, the lid with the stopper must be inserted deeper into the vessel than to reach the sealing position.
  • the plug and the parking area are formed so that in the parking position a clearance fit between the plug and the parking area is present.
  • plug and parking area are formed so that in the parking position an interference fit between plug and parking area is present. Due to the interference fit, the lid can sealingly abut the parking area. This greatly reduces the risk of contamination. Due to the interference fit, the plug can relax in the parking position. Nevertheless, the plug can seal in the sealing position rich in Dichtbe, since the sealing area is not relaxed and can build up sufficient for sealing voltage between plug and sealing area.
  • the interference fit can also be chosen so that the voltage between plug and parking area in the parking position is less than the voltage between the plug and sealing area in the sealing position. As a result, a relaxation and the plug is kept relatively low.
  • the parking area is arranged above the sealing area Ches and widens upwards. As a result, the insertion of the plug is facilitated in the parking area.
  • the parking area is conical.
  • the sealing region is a cylindrical or conical region on the inner wall of the vessel to which the plug in sealing position abuts sealingly.
  • the Dichtbe is arranged rich concentric to the central axis of the vessel, that is, the central axis of the Sealing area coincides with the central axis of the vessel.
  • the diameter of the conical region expands upwards or downwards.
  • the first latching device has a radially inwardly projecting first latching projection on the inner wall of the vessel.
  • first latching projection runs around at least a part of the circumference on the inner wall of the vessel.
  • the first latching projection is arranged above the parking area.
  • the first latching device has a radially outwardly projecting second latching projection on the outside of the plug.
  • the plug can be latched to the second locking projection behind the first Rastvor jump.
  • the lid is even better ge secured in the parking position.
  • the second latching projection at least partially revolves around the plug.
  • the lid may be hinged to the vessel or a removable lid completely detachable from the vessel.
  • the first latching device comprises a groove or groove circulating at least partially on the inner wall of the vessel and / or a bead which runs at least partially around the outside of the plug.
  • the plug engages in the parking position with the bead in the groove or groove.
  • the groove has the function of a parking area.
  • the upper flank of the groove has the function of the first latching projection.
  • the bead has the function of the second locking projection.
  • the lower flank of the groove can prevent unintentional penetration of the plug into the sealing area.
  • the outer diameter of the bead larger than the inner diameter of the vessel directly next to the groove or groove. Before preferably, the outer diameter of the bead is smaller than or equal to the inner diameter of the groove or groove.
  • the term "groove” in this application denotes an elongated recess and with “groove” a narrow elongated recess. Together, the term “groove” can be used.
  • the first latching device comprises a groove or groove at least partially encircling the inner wall of the vessel and a radially outwardly projecting second latching projection on the outside of the plug or an edge at the lower end of the plug.
  • the plug with the second locking projection or the edge at the lower end of the plug in the groove or groove is locked.
  • the first locking device on the inner wall of the housing comprises a radially inwardly projecting first locking projection and the outside of the plug at least partially encircling bead.
  • the bead is locked behind the first locking projection.
  • the first locking projection or the groove or groove runs completely around the circumference on the inner wall of the vessel.
  • the first locking projection or the groove or groove is arranged on the inner wall of the vessel on the side opposite the hinge and does not completely run around the circumference on the inner wall of the vessel.
  • the first locking projection or the groove or groove runs over an angle of at most 180 °, preferably of not more than 90 °, preferably not more than 45 °, preferably not more than 22.5 °, preferably not more than 11.25 ° Inner wall of the vessel around.
  • the bead runs completely around the outside of the plug and lies around the plug with the bead in the sealing position sealingly on the sealing area.
  • the bead additionally has the function of a sealing element. In the sealing position, the bead lies in a narrow, preferably linear, circumferential region on the sealing region, so that there is a high surface pressure, which causes a seal.
  • a second locking device for releasably locking the lid with the vessel in the sealing position.
  • the second locking device holds the lid in the sealing position on the vessel, so that in the sealing position only the sealing required for sealing between Stop fen and sealing area must act.
  • the second latching device jump at least one at the upper edge of the vessel radially outwardly projecting third Rastvor jump and at least one protruding from the bottom of the lid bottom elas table tab with a locking edge at a distance from the lid bottom, which upon insertion of the plug in the sealing area can be snapped under the locking projection.
  • a particularly secure, with low forces forth adjustable and re-releasable latching of the lid is achieved on the vessel.
  • the tab is at a distance from the lid bottom laterally before a first lever outwards.
  • the first lever makes it easier Dissolving the locking of the lid with the vessel. It corresponds to the key of EP 2 654 958 Bl.
  • a second lever projects upwardly from the first lever at a distance from the tab.
  • the second lever facilitates the release of the locking of the lid with the vessel.
  • the second lever is provided with an outwardly projecting rib.
  • the rib can be used for opening and closing the lid by means of a working cone of a metering device or other tool.
  • the rib is arranged on the second lever so that it extends in the lid in sealing position and vertically aligned central axis of the vessel in the horizontal direction Rich.
  • a working cone is used for opening and closing the lid, which has a circumferential groove on the outer circumference.
  • the working cone is preferably pushed with the circumferential groove from the side of the rib on to move by displacing the working cone to the vessel up and down the lid and open or close by moving the working cone down.
  • the working cone of a metering machine, a laboratory machine or a handheld pipette can be used.
  • the vessel is preferably held in a receptacle.
  • the lid and vessel are connected to each other via a hinge.
  • the hinge facilitates the opening and closing of the lid.
  • the hinge is a band hinge.
  • a hinge band is particularly advantageous for the one-piece production of the lid vessel by injection pour.
  • the hinge is a butterfly hinge.
  • the Butterfly-Schamier has two parallel and one in one Distance from one another arranged hinge bands, which are each connected to the outer edge of a first pocket in the upper edge of the vessel and are connected to the outer edge of a second pocket at the bottom of the lid bottom, the hinge straps are so short that they are folded and tightened with the underside on the upper edge of the vessel lid and at least partially received by the first and second pockets.
  • the Butterfly-Schamier does not project outwards when the vessel is closed, so that the vessel has only a small space requirement. As a result, several vessels can be accommodated next to each other to save space. Further, it is advantageous that the butterfly-hinge lid and vessel connects together so that it does not rise at he elevated réelledmck on the side of the hinge. As a result, it can be prevented that the first latching device releases inadvertently.
  • the lid with the stopper in parking position is aligned at an acute angle to the central axis of the vessel and in the sealing position concentric with the central axis of the vessel.
  • the parking area of the vessel is at an acute angle to the central axis of the Ge vessel and the sealing area aligned concentrically to the central axis of the vessel.
  • the parking area is an at least partially on the inner wall of the vessel at an acute angle to the central axis of the vessel circumferential groove or groove and the sealing area is concentric to the central axis, a circular cylindrical or conical region on the inner wall of the vessel.
  • the first latching device and / or the second latching device is / are arranged diametrically opposite the hinge.
  • the cover is held in the parking position and in the sealing position respectively on diametrically opposite sides of the hinge and the first latching device or the second latching device.
  • the lid is completely detachable from the vessel. In this case, lid and vessel are not connected to each other via a hinge. In this embodiment, the lid with the plug in the axial direction of the Ge vessel is inserted into the vessel and removed from this. Thus, the plug is arranged concentrically with the vessel both in the parking position and in the sealing position.
  • the parking area is formed for example by a completely on the inner wall of the vessel above the sealing area circumferential groove or groove, in which engages the stopper in the parking position with a umlau on its outer circumference fenden bead.
  • the sealing region is, for example, a cylindrical or conical region on the inner wall of the vessel, against which the bead of the plug sealingly abuts in the sealing position.
  • the inner diameter of the Dichtbe is rich at the point where the bead sealingly applied, less than the outer diameter of the bead.
  • the lid In a lidded vessel in which the lid is detachable from the vessel, the lid may be held in the sealing position solely by the clamping force of the plug, or by a plurality of second latching devices, for example as in EP 2 654 958 B1 with reference to FIGS. 21 to 23 described.
  • the lidded vessel has a nominal volume of at least 0.5 ml, preferably at least 1.5 ml, preferably at least 2 ml, preferably at least 5 ml, preferably at least 15 ml, preferably at least 30 ml, preferably of at least 50 ml.
  • the lidded vessel has one of the following nominal volumes: 0.5 ml, 1.5 ml, 2 ml, 5 ml, 15 ml, 30 ml, 50 ml.
  • the nominal volume is the volume of the sample liquid for its uptake the lidded vessel is designed. It is specified by the manufacturer.
  • the lidded vessel is made by injection molding, preferably in one piece.
  • the lidded container is made of polypropylene,
  • Polyethylene a cyclic olefin (CO) polymer or other polyol produced fin.
  • Cover container made of plastic for laboratory use comprising
  • a tubular vessel having at the bottom a vessel bottom, at the top a vessel opening and below the vessel opening at the inside wall a sealing area,
  • a lid having a lid bottom and a stopper projecting from the inside of the lid bottom, which can be inserted through the container opening into a sealing position in which the stopper sealingly bears against the sealing area,
  • the lid engages in a parking position with the stopper into the vessel opening, without sealingly abut the sealing area, and
  • a first latching device for releasably locking the lid with the Ge vessel in the parking position is present.
  • Lidded vessel according to embodiment 1 or 2 wherein the parking area is arranged above the sealing area and widens upwards, wherein the parking area is preferably conical.
  • Lid vessel according to embodiment 5 wherein the bead completely surrounds the outside of the plug and sealingly abuts the sealing area in the sealing position.
  • Lidded vessel according to one of the embodiments 1 to 6 which has a second Rastein direction for releasably locking the lid with the vessel in the sealing position.
  • Lidded vessel according to embodiment 8 in which a first lever protrudes laterally from the lug at a distance from the bottom of the lids, whereby Preferably, from the first lever at a distance from the tab, a second lever projects upwards.
  • Lidded vessel according to one of the embodiments 1 to 10, wherein the lid and vessel are connected to each other via a hinge, wherein preferably the hinge is a hinge band.
  • FIG. 1a-e a first lidded container with hinge and latching projection with geöff netem lid in front view (Fig la), side view (Fig lb), a vertical section (Fig. Lc), plan view (Fig ld), a Perspek tivansicht diagonally from above and from the side (Fig le);
  • FIG. 3a-f the same lidded container with the lid in sealing position in Vorderan view (Fig. 3a), side view (Fig. 3b), a vertical section (Fig. 3c), an enlarged detail of the vertical section (Fig. 3d), top view ( Fig. 3e) and a perspective view obliquely from above and from the side (Fig. 3f).
  • Fig. 4 the same lid tube when opening by means of a machine tool in an enlarged perspective detail view obliquely from above and from the side;
  • FIG. 5 is a second lid vessel with laterally projecting rib for opening by means of a working cone of a metering device in a verierten perspective detail view obliquely from above and from the side.
  • Fig. 6 the same lidded vessel when opened by means of a working cone in a vertical section
  • Fig. 7 is a third lidded vessel with hinge and completely circumferential
  • FIG. 7a Groove with lid open in front view (Fig. 7a), side view (Fig. 7b), a vertical section (Fig. 7c), plan view (Fig. 7d), a perspective view obliquely from above and from the side (Fig. 7e);
  • FIG. 8f the same lidded container with a cover in parking position in Vorderan view (Fig. 8a), side view (Fig. 8b), a vertical section (Fig. 8c), an enlarged detail of the vertical section (Fig. 8d), top 8e), a perspective view obliquely from above and from the side (FIG. 8f);
  • FIG. 10 shows a fourth lidded vessel with an enlarged lid and vessel in an axial direction of the vessel.
  • top and bottom as derived therefrom as “above” and “below” refer to the lidded vessel with the lid in the sealing position, the central axis of the tubular vessel oriented vertically and the bottom of the vessel below the lid is arranged.
  • connection device Riviere connection
  • locking in the same sense as the terms “Schnappeinrich direction”, “snap connection” and “snap” used.
  • snap connection positive connections in which a projecting point of a connection partner is briefly deflected and into a recess (behind section) of the other connection partner snaps.
  • a connection of the connection partners is also possible at several successive joining positions.
  • the cover vessel 1.1 of FIGS. 1-3 has a tubular vessel 2 with a circular circular cross-section, which has a hollow-cylindrical section 3 at the top and a conical section 4 at the bottom.
  • a vessel opening 6 At the bottom of the vessel 2 has a flat bottom 5 and at the top of a vessel opening 6.
  • Under the vessel opening 6 is in hohlzylind- 3 a conically downwardly tapering parking area 7 IN ANY, below which a downwardly extending sealing area 8 is present (see Figures 2d, 3d).
  • Under the sealing area 8 is a down conically tapered end transition region 9 is present.
  • the hollow cylindrical section 3 has a substantially constant wall thickness.
  • the hollow cylindrical portion 3 has outside and inside below the Kochgangsbe 9 rich a slight conicity in order to facilitate removal from an injection mold convincing.
  • the vessel 2 has a circumferential, radially outwardly projecting the flange 10.1 in the form of a circular disk.
  • the flange 10.1 has at the upper outer edge a first chamfer 10.2 (see Figures 2d, 3d).
  • the lower edge has a sharp edge 10.3.
  • a series of crenellated projections 11 which serve to support on the edge of a vessel holder.
  • the lid tube 1.1 has a lid 12, which has a lid bottom 13 and a top of the lid 13 protruding plug 14.
  • the plug 14 has a hollow cylindrical plug portion 14.1.
  • the lid bottom 13 projects laterally beyond the stopper 14 also.
  • the Deckelbo the 13 has a circular arc-shaped lid edge 13.1, which extends approximately over an angle of approximately 240 ° (see Fig .. ld). This is followed by twoitli surface, rectilinear cover edges 13.2, 13.3 and a front, straight lid edge 13.4 at. From the arcuate lid edge 13.1 and the side cover edges 13.2, 13.3 is down a lid projection 15, which serves to support the lid 12 on the top of the flange 10.1.
  • the lid 12 is connected via a hinge 16 with the vessel 2, which is designed as a butter fly hinge with two parallel hinge bands 16.1, 16.2.
  • the hinge 16 is arranged in the middle of the circular-arc-shaped lid edge 13.1 or ge compared to the front lid edge 13.4.
  • One end of the hinge bands 16.1, 16.2 is connected to the flange 10.1 at the outer edge of first pockets 17.1, 17.2, and the other end is connected to the circular-arc-shaped lid edge 13.1 at the outer edge of second pockets 18.1, 18.2.
  • the vessel 2 has at the top of the parking area 7 on the hinge 16 diametrically opposite side a radially inwardly projecting first locking projection 19 (see Fig. 2d and 3d).
  • the first latching projection 19 extends in the circumferential direction of the vessel 2 over an angle of approximately 10 ° (see Fig. Ld).
  • the bead 14.2 is at the same time a second latching projection 20.
  • the first latching projection 19 and the second latching projection 20 together form a first latching device 21.
  • a flexible and elastic bag 23 protrudes from the front lid edge 13.4 downwards.
  • the bag 23 comprises two lateral Faschenstsammlung 23.1, 23.2, between tween which a recess 24 is present (see Fig .. ld).
  • the Faschenstsammlung 23.1, 23.2 are each arranged at a corner between the front edge of the cover 13.4 and the two lateral Deckelrändem 13.2, 13.3.
  • the two tab strips 23.1, 23.2 are connected at the bottom with a strip-shaped first lever 25, which extends parallel to the lid bottom 13 to the outside.
  • the outer edge of the first lever 25 is circular arc-shaped.
  • the first lever 25 limits the recess 24 below.
  • the inner, upper edge of the first lever 25 is a latching edge 26 (see Figures 2d, 3d).
  • the first lever 25 has at its inner edge on the lower side a second bevel 27.
  • the hinge straps 16.1, 16.2 and the tab strips 23.1, 23.2 are flexible.
  • the first and second levers 25, 28, however, are rigid.
  • the plug 14 and / or the sealing area 8 are flexible and / or rigid.
  • the remaining lidded vessel 2 is preferably rigid before.
  • the rigid and flexible properties are achieved by the Formge staltung and / or the wall thicknesses and / or materials of the respective parts.
  • the third latching projection 22 and the latching edge 26 form a second latching device 29 (see Fig. 3d).
  • the lid vessel 1.1 is manufactured in the open arrangement shown in Fig. 1 by injection molding.
  • the first locking projection 19 and the bead 14.2 form undercuts, which allow due to their small dimensions, a production by means of a simple injection molding tool having only two mold halves, which can be moved apart for removal along an axis.
  • the cover 12 is brought by folding into the locking position GE, in which the bead 14.2 engages under the first locking projection 19.
  • the first latching device 21 formed by the first latching projection and bead 14.2 holds the cover 12 firmly in the parking position on the vessel 2. This is shown in FIG. 2. In this state, a plurality of lidded vessels 1.1 can be packed in a bag.
  • the bead 14.2 bears with negligible force on the first latching projection 19.
  • the sealing area 8 is not under tension. As a result, sealing area 8 and bead 14.2 do not relax in the parking position, even if they are maintained for longer periods of time (eg months or years).
  • the user removes individual lidded containers 1.1. If appropriate, he provides the lid bottom 13 outside with a label to mark the respective lid vessel 1.1. This can be done in the park position. Due to the fact that the cross section of the vessel 2 in the parking area 7 ver downwards ver, the lid 12 is not hineinge suppressed even when labeling hineinge into the vessel.
  • the user can open the lid 12, preferably in the position shown in Fig. 1 or in a less widely unfolded inter mediate position. Thereafter, the vessel 2 can be filled with sample liquid.
  • the user can press against the outside of the lid bottom 13, so that the lid pivots about the hinge 16.
  • the lid 12 enters the vessel opening 6 with the stopper, which is facilitated by the extended parking area 7. Thereafter, the bead reaches 14.2 in the sealing area 8 and seals up there from.
  • the tab strips 23.1, 23.2 are deflected laterally outward (see Figures 2d, 3d).
  • the bead 14.2 bears against the sealing region 8 under a prestress which is sufficiently high to seal the vessel 2 in a liquid-tight and possibly gas-tight manner.
  • the user presses against the outside of the second lever 28.
  • the force is applied horizontally and with a component upwards.
  • the second lever 28 is pivoted to the lid bottom 13 and the first lever 25 is released with the locking edge 26 of the third locking projection 22.
  • Further pressing against the second lever 28 causes the first lever 25 with the top on the lower outer edge of the third locking projection 22 slides up until the locking edge 26 slides over the lower outer edge of the third Rastvor jump 22 and gets free.
  • the lid 12 is pivoted to the open position (see Fig. 1).
  • the lid 12 by means of a hook-shaped Maschinenzeu tot 30 of a laboratory machine can be opened.
  • the tool 30 is set with an angled leg 31 at its lower end under the first lever 25 at.
  • the first lever 25 is pivoted up, so that the latching edge 26 is released from the third latching projection 22.
  • the lid 12 is folded up by means of the tool 30.
  • the lidded vessel 1.2 of FIG. 5 differs from that described above in that at the upper end of the second lever 28, a rib 32 extending in the horizontal direction projects outwardly.
  • the second lever 28 by counterpressure of a working cone 33, which is used for clamping a pipette tip to the vessel 2 pivoting bar to cancel the latching of the second latching device 29.
  • the rib 32 engages in a circumferential annular groove 34 of the working cone 33 a.
  • FIG. 7 to 9 show a third lidded vessel 1.3 with hinge 16 and a fully constantly on the inner wall of the vessel circumferential groove 35 at the lower end of the parking area 7.
  • the third lid vessel 1.3 has in contrast to the first lid vessel 1.1 no first latching projection 19th
  • the third lidded vessel 1.3 coincides with the first lidding vessel 1.1.
  • the upper flank 36 of the groove 35 forms the first latching projection 19 which is engaged by the bead 14.2 in the parking position, as shown in FIG.
  • the lower edge 37 of the groove 35 engages under the bead 14.2 and prevents the plug 14 in the parking position unintentionally hineinge deeper into the vessel 2 is suppressed.
  • the bead 14.2 sealingly abuts the sealing region 8 in the sealing position.
  • FIG. 10 shows a fourth lid vessel 1.4, in which lid 12 and vessel 2 are not connected to one another by a hinge 16.
  • the vessel 2 has a conical insertion region 38 on the vessel opening 6 on the inside. Directly below the conical insertion region 38, it has a peripheral groove 35 on the inner circumference, which defines a parking area.
  • the groove 35 has a triangular cross section with an upper flank 36 and a lower flank 37.
  • the vessel 2 has a circumferential flange 10, the radially projecting radially outwardly from a hollow cylindrical portion 3 of the vessel area forming a locking projection 10.1.
  • the lid 12 has a lid bottom and a downwardly projecting plug 14.
  • the plug has a bead around the outside at the bottom 14.2.
  • a portion of the plug 14 is shown in solid lines in the park position. In this position, the bead 14.2 engages in the groove 35. As a result, an inadvertent emergence of the plug 14 from the vessel 2 or deep res entry of the plug 14 is prevented in the vessel 2. As the bead 14.2 sits with clearance in the groove 35, the bead 14.2 does not relax. Since the sealing area 8 is not overloaded, it also does not relax.
  • a lower part of the plug 14 is shown in dash-dotted lines in the sealing position. Since the inner diameter of the vessel 2 is smaller than the outer diameter of the bead 14.2 in the sealing region 8, the bead 14.2 seals against the sealing region 8 in the sealing position. Furthermore, in solid lines, a latching hook 39 of the lid 12 is shown in the sealing position. The latching hook 39 engages under the flange 10. This is also the case with the remaining catch hooks 39, not shown. As a result, the lid 12 is held in the sealing position.
  • the vessel 2 can be opened by the locking hooks 39 are bent outwards.
  • the lid 12 In the park position, the lid 12 can be held in the groove 36 on the vessel 2 solely by the engagement of the bead 14.2.

Landscapes

  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Hematology (AREA)
  • Clinical Laboratory Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Closures For Containers (AREA)
  • Devices For Use In Laboratory Experiments (AREA)
PCT/EP2019/055410 2018-03-07 2019-03-05 DECKELGEFÄß AUS KUNSTSTOFF FÜR DEN LABOREINSATZ WO2019170651A1 (de)

Priority Applications (3)

Application Number Priority Date Filing Date Title
US16/978,411 US11896976B2 (en) 2018-03-07 2019-03-05 Lidded vessel assembly for laboratory use
CN201980017134.5A CN111819002B (zh) 2018-03-07 2019-03-05 用于实验室应用的由塑料制成的带盖器皿
JP2020546135A JP7339269B2 (ja) 2018-03-07 2019-03-05 実験室用のプラスチック製蓋付き容器

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP18160393.7 2018-03-07
EP18160393.7A EP3536403B1 (de) 2018-03-07 2018-03-07 Deckelgefäss aus kunststoff für den laboreinsatz

Publications (1)

Publication Number Publication Date
WO2019170651A1 true WO2019170651A1 (de) 2019-09-12

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US (1) US11896976B2 (ja)
EP (1) EP3536403B1 (ja)
JP (1) JP7339269B2 (ja)
CN (1) CN111819002B (ja)
WO (1) WO2019170651A1 (ja)

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* Cited by examiner, † Cited by third party
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USD1008489S1 (en) * 2021-03-17 2023-12-19 Eppendorf Se Lid for test tubes
IT202100013640A1 (it) * 2021-05-26 2022-11-26 Vacutest Kima S R L Contenitore a tenuta ermetica per liquidi

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EP2517791A1 (en) 2011-04-18 2012-10-31 Vibod GmbH Sample tube with improved lid
EP2654958A1 (de) 2010-12-23 2013-10-30 Eppendorf AG Reaktionsgefäss mit deckel
EP2965816A1 (de) 2014-07-09 2016-01-13 Eppendorf Ag Reaktionsgefäß mit Deckel

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US3164279A (en) 1965-01-05 Test tube closure
US3881626A (en) 1972-11-20 1975-05-06 Warner Lambert Co Container closure for lyophilized products
US4883641A (en) * 1987-06-26 1989-11-28 Minnesota Mining And Manufacturing Company Closure and container assembly for biological sterility indicator
US5354539A (en) 1993-11-12 1994-10-11 Hovatter Kenneth R Microtube having press-to-seal and twist-to-lock closure cap
WO1995020527A1 (en) * 1994-01-28 1995-08-03 Innervision, Inc. Sealing cap for containers
WO2011108134A1 (ja) 2010-03-03 2011-09-09 株式会社サンプラテック 容器、および容器用アタッチメント
EP2654958A1 (de) 2010-12-23 2013-10-30 Eppendorf AG Reaktionsgefäss mit deckel
EP2517791A1 (en) 2011-04-18 2012-10-31 Vibod GmbH Sample tube with improved lid
EP2965816A1 (de) 2014-07-09 2016-01-13 Eppendorf Ag Reaktionsgefäß mit Deckel

Also Published As

Publication number Publication date
CN111819002A (zh) 2020-10-23
EP3536403A1 (de) 2019-09-11
JP7339269B2 (ja) 2023-09-05
JP2021516148A (ja) 2021-07-01
US11896976B2 (en) 2024-02-13
CN111819002B (zh) 2023-04-11
US20210039090A1 (en) 2021-02-11
EP3536403B1 (de) 2021-11-03

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