WO2017170217A1 - 化粧料セット - Google Patents

化粧料セット Download PDF

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Publication number
WO2017170217A1
WO2017170217A1 PCT/JP2017/011982 JP2017011982W WO2017170217A1 WO 2017170217 A1 WO2017170217 A1 WO 2017170217A1 JP 2017011982 W JP2017011982 W JP 2017011982W WO 2017170217 A1 WO2017170217 A1 WO 2017170217A1
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Prior art keywords
composition
component
cosmetic set
oil
set according
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PCT/JP2017/011982
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English (en)
French (fr)
Japanese (ja)
Inventor
知明 篠田
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株式会社コーセー
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Priority to KR1020187030527A priority Critical patent/KR102396751B1/ko
Priority to CN201780021285.9A priority patent/CN108883043B/zh
Priority to JP2018509236A priority patent/JP6918780B2/ja
Publication of WO2017170217A1 publication Critical patent/WO2017170217A1/ja

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/88—Two- or multipart kits
    • A61K2800/884—Sequential application

Definitions

  • the present invention relates to a cosmetic set including a first composition and a second composition, and relates to a cosmetic set in which the second composition is applied after the first composition is applied to the application part.
  • Patent Document 1 A technique (Patent Document 1) has been proposed in which a second composition containing methylphenylpolysiloxane having a molecular weight of 1000 cs to 7000 cs is applied.
  • polyisobutylene which is a hydrocarbon-based resin
  • the volatilization of the volatile hydrocarbon oil in the first composition is hindered, and it takes time to obtain the effect of preventing makeup collapse. In some cases, color blur occurs.
  • the content of polyisobutylene having a relative mass of 3,000 to 1,000,000 in the first composition is increased in order to further improve the cosmetic disintegration effect over time, there may be a feeling of a crispness. .
  • a cosmetic set comprising a first composition and a second composition, wherein the second composition is applied after the first composition is applied to the application part, and the first composition And the 2nd composition is related with the cosmetics set which is what contains the following components, respectively.
  • First composition (A) Film-forming silicone resin (B) Silicone oil having a kinematic viscosity of 1,000 to 1,000,000 cs at 25 ° C. (C) Volatile hydrocarbon oil (D) Colored pigment (second composition) Oil of component (E) phase-separated when mixed in an equal amount with a mixture in which component (A) and component (C) are mixed at a mass ratio of 1: 1 and left to stand at 25 ° C. for 60 minutes.
  • the component (A) is one or more selected from trimethylsiloxysilicic acid, polymethylsilsesquioxane, (acrylates / dimethicone) copolymer, and (acrylates / stearyl acrylate / dimethicone methacrylate) copolymer
  • the content of the component (A) in the first composition is 10 to 50% by mass, the content of the component (B) is 1 to 50% by mass, and the content of the component (C) is 20
  • the present invention relates to the cosmetic set according to any one of [1] to [4], which is 85% by mass.
  • One or more oil agents wherein the component (E) is selected from isostearic acid ester, hydroxystearic acid ester, lanolin derivative, trimellitic acid ester, paramethoxycinnamic acid ester and vinylpyrrolidone copolymer
  • the component (E) comprises polyglyceryl-2 isostearate, polyglyceryl-2 triisostearate, polyglyceryl-2 tetraisostearate, polyglyceryl-10 nonaisostearate, polyglyceryl-10 decaisostearate, pentaisotetrastearate
  • One or more oils selected from erythrityl, glyceryl triisostearate, ethylhexyl hydroxystearate, lanolin acetate, tritridecyl trimellitate, ethylhexyl paramethoxycinnamate, and (vinylpyrrolidone / hexadecene) copolymer [1 ]
  • the present invention uses a combination of the first composition and the second composition containing a specific oil agent, and is excellent in the effect of preventing color migration without causing color blurring during use.
  • the present invention also provides a cosmetic set that does not lose its makeup over time.
  • Example 2 it is the photograph which confirmed the color transfer at the time of combining the 1st composition of the formulation example 1 and the 2nd composition of the formulation example 19 or the comparative formulation example 8.
  • FIG. 2 it is the photograph which confirmed the color transfer at the time of combining the 1st composition of the formulation example 1 and the 2nd composition of the formulation example 19 or the comparative formulation example 8.
  • the film-forming silicone resin of the component (A) used in the first composition of the present invention is a compound having a crosslinked structure having a siloxane structure as a main skeleton, and the silicone oil of the component (B) or the component (C).
  • an oil agent such as volatile hydrocarbon oil and used in cosmetics
  • the film-forming property means having a property of forming a film after a solution obtained by dissolving a silicone resin in the volatile hydrocarbon oil of component (C) is spread on a petri dish and dried.
  • membrane may produce a crack with drying, and does not need to be obtained as one film.
  • trimethylsiloxysilicic acid polymethylsilsesquioxane, (acrylates / dimethicone) copolymer, (acrylates / stearyl acrylate / dimethicone methacrylate) copolymer, and the like can be used. it can.
  • the content of the film-forming silicone resin of component (A) in the first composition of the present invention is not particularly limited, but is preferably 10 to 50% by mass (hereinafter simply referred to as “%”), more preferably 15 Is 35%, more preferably 15-30%. Within this range, it is more preferable in that a cosmetic film excellent in the effect of preventing the slipperiness and preventing the collapse of the makeup is obtained.
  • the silicone oil having a kinematic viscosity at 25 ° C. of 1,000 to 1,000,000 cs of the component (B) used in the first composition of the present invention is a silicone oil having fluidity under the conditions of 1 atm and 25 ° C. If it is used for cosmetics, such as siloxane, methyl hydrogen polysiloxane, phenyl modified silicone, alkyl modified silicone, etc., it will not restrict
  • the kinematic viscosity at 25 ° C. of component (B) is preferably from 1,000 to 1,000,000 cs, more preferably from 10,000 to 1,000,000 cs, and particularly preferably from 10,000 to 100,000 cs.
  • the silicone oil has a kinematic viscosity at 25 ° C. of less than 1000 cs, it may not be possible to obtain a satisfactory color bleed prevention effect or anti-decoration effect. If the silicone oil has a kinematic viscosity at 25 ° C. of more than 1,000,000 cs, In some cases, the volatilization rate of the component (C) becomes slow, and a satisfactory color blur prevention effect cannot be obtained.
  • KF-96-1000cs / 3000cs / 5000cs KF-96H-6000cs / 10,000cs / 12500cs / 30,000cs / 50,000cs / 60,000cs / 100,000cs / 300,000cs / 500,000cs / 1 million cs, KF-50-1000 cs (from Shin-Etsu Chemical Co., Ltd.), SH-200 C Fluid 1000CS / 3000CS / 5000CS / 10000CS / 12500CS / 30000CS / 60000CS / 100000CS / 1000000CS, BY11-040 / 003 / 007/014/026/320 (above, manufactured by Toray Dow Corning).
  • the kinematic viscosity is a value measured at 25 ° C. by the ASTM D445 measuring method.
  • the content of component (B) in the first composition of the present invention is not particularly limited, but is preferably 1 to 50%, more preferably 3 to 35%, and still more preferably 5 to 30%. Within this range, it is more preferable in terms of being able to suppress the feeling of touch due to the silicone resin and obtaining a decorative film having an excellent effect of preventing makeup collapse.
  • the volatile hydrocarbon oil of component (C) used in the first composition of the present invention is liquid at 1 atm and 25 ° C., has volatility, has a boiling point in the range of 68 to 260 ° C., carbon Examples thereof include hydrocarbons having a number of 6 to 30. Usually, it is not particularly limited as long as it is used as a cosmetic raw material. Specifically, it is a straight chain hydrocarbon such as normal heptane, isooctane (2,2,4-trimethylpentane, 2,3-dimethylhexane, etc.
  • isododecane (2,2,4,6,6-pentamethylheptane, etc.)
  • hydrocarbons having side chains such as isohexadecane, isoeicosaene, etc., or mixtures thereof, isobutene, n-butene, etc. (The degree of polymerization is preferably 4 to 6), and then hydrogenated ones can be mentioned, and one or more can be used in combination as necessary.
  • Examples of the commercially available products include Isopar H (manufactured by ExxonMobil Chemical), Isododecane (manufactured by Bayer), Isohexadecane (manufactured by Unikema), IP Solvent 1620MU, IP Solvent 2028MU, IP Solvent 2835 (above, manufactured by Idemitsu Kosan) Is mentioned. These can use 1 type (s) or 2 or more types.
  • the content of the volatile hydrocarbon oil of component (C) in the first composition of the present invention is not particularly limited, but is preferably 20 to 85%, more preferably 25 to 80%, still more preferably 30 to 70%. If it is this range, it is more preferable at the point etc. which are excellent in the feeling of no feeling of a touch and the color bleeding at the time of use.
  • the colorant of component (D) used in the first composition of the present invention is a colorant usually used in cosmetics, shapes such as spheres, plates, spindles, needles, fumes, fine particles
  • the particle size such as pigment grade or the particle structure such as porous or nonporous is not particularly limited, and inorganic colored pigments, organic colored pigments, dyes, glitter pigments, metals and the like can be used. .
  • Specific powders include white inorganic pigments such as titanium oxide, zinc oxide, cerium oxide, and barium sulfate, colored inorganic pigments such as iron oxide, carbon black, chromium oxide, chromium hydroxide, bitumen, ultramarine, and bengara, mica Titanium, bismuth oxychloride, organic pigment-treated mica titanium, titanium dioxide-coated mica, titanium dioxide-coated synthetic phlogopite, titanium dioxide-coated bismuth oxychloride, iron oxide mica titanium, bituminized mica titanium, carmine-treated mica titanium, fish scale foil, dioxide Luminous pigments such as titanium coated glass powder, polyethylene terephthalate / aluminum / epoxy laminated powder, polyethylene terephthalate / polyolefin laminated film powder, polyethylene terephthalate / polymethyl methacrylate laminated film powder, etc., red 201, red 202, Red 205 Organic pigment powders such as red 226, red 228, orange 203, orange 204,
  • zirconium, barium or aluminum lake or other organic pigment powders or metal powders such as aluminum powder, gold powder, silver powder, fine titanium oxide coated mica titanium, fine zinc oxide
  • metal powders such as aluminum powder, gold powder, silver powder, fine titanium oxide coated mica titanium, fine zinc oxide
  • composite powders such as coated mica titanium, barium sulfate-coated mica titanium, titanium oxide-containing silicon dioxide, zinc oxide-containing silicon dioxide, and the like, and if necessary, one or a combination of two or more may be used. it can.
  • Surface treatment may be performed using
  • the content of the colorant of component (D) in the first composition of the present invention is not particularly limited, but is preferably 0.0001 to 30%, more preferably 0.001 to 20%.
  • the first composition of the present invention can contain, in addition to the above components (A) to (D), components that are usually used in cosmetics as long as the effects of the present invention are not hindered. ), Oils other than components (B) and (C), surfactants, monohydric alcohols, polyhydric alcohols, water-soluble polymers, paraoxybenzoic acid derivatives, preservatives such as phenoxyethanol, ultraviolet absorption Agent, moisturizer, antibacterial agent, fragrance, salt, antioxidant, pH adjuster, chelating agent, refreshing agent, anti-inflammatory agent, skin beautifying agent (whitening agent, cell activator, rough skin improver, blood circulation promoter, skin Astringents, antiseborrheic agents, etc.), vitamins, amino acids, nucleic acids, hormones, inclusion compounds and the like can be appropriately contained.
  • Oils other than components (B) and (C) Oils other than components (B) and (C), surfactants, monohydric alcohols, polyhydric alcohols, water-soluble polymers, paraoxybenzoic
  • oil agents include hydrocarbons, fats and oils, waxes, hardened oils, ester oils, regardless of the origin, such as animal oils, vegetable oils, synthetic oils, and properties such as solid oils, semi-solid oils, and liquid oils. , Fatty acids, higher alcohols, silicone oils, fluorine oils, lanolin derivatives, oily gelling agents, oil-soluble resins, volatile oils, and the like.
  • hydrocarbons such as liquid paraffin, squalane, petrolatum, paraffin wax, ceresin wax, microcrystalline wax, ethylene propylene copolymer, montan wax, Fischer-Tropsch wax, molasses, olive oil, castor oil, mink oil, macadamian Fats and oils such as nut oil, beeswax, carnauba wax, candelilla wax, waxes such as gay wax, jojoba oil, cetyl isooctanoate, isopropyl myristate, isopropyl palmitate, octyldodecyl myristate, glyceryl trioctanoate, diisostearic acid Polyglyceryl, diglyceryl triisostearate, glyceryl tribehenate, diisostearyl malate, neopentyl glycol dioctanoate, cholesterol Fatty acid esters, esters such as N-lauroyl-L
  • the content of the oil agent in the first composition of the present invention is not particularly limited with respect to the oil agent that is liquid at 25 ° C., but the second composition described later Is preferably from 0 to 10%, more preferably from 0 to 5%, from the viewpoint that color bleeding is less likely to occur when the above is applied.
  • component (A) and the component (C) used in the second composition of the present invention are mixed in an equal amount with a mixture in which the mass ratio is 1: 1 and the mixture is allowed to stand at 25 ° C. for 60 minutes
  • the oil agent of component (E) to be separated is not particularly limited as long as it is used in cosmetics, and can be used.
  • oil of component (E) used in the second composition of the present invention examples include, but are not limited to, polyglyceryl-2 isostearate, polyglyceryl-2 triisostearate, polyglyceryl-2 tetraisostearate, nonaisostearate Polyglyceryl-10, polyglyceryl decaisostearate, pentaerythrityl tetraisostearate, glyceryl triisostearate, isostearic acid esters such as ethylhexyl hydroxystearate, lanolin, lanolin acetate, lanolin fatty acid isopropyl, lanolin Lanolin derivatives such as alcohol, trimellitic acid tritridecyl, trimellitic acid ester such as trioctyl trimellitic acid, ethyl hexyl paramethoxycinnamate Para-methoxy cinnamic acid esters, (vinylpyrrolidone / hexadec
  • the mixture of component (A) and component (C) at a mass ratio of 1: 1 is mixed in an equal amount, and is easy to phase separate when left at 25 ° C. for 60 minutes, and to that.
  • polyglyceryl-2 isostearate polyglyceryl-2 triisostearate, polyglyceryl-2 tetraisostearate, polyglyceryl-10 nonaisostearate, polyglyceryl-10 decaisostearate, pentaerythrityl tetraisostearate, glyceryl triisostearate, acetic acid It is particularly preferable to use one or more selected from lanolin, tritridecyl trimellitate, and (vinylpyrrolidone / hexadecene) copolymer.
  • isostearic acid means one kind of branched stearic acid or a mixture of two or more kinds.
  • 5,7,7-trimethyl-2- (1,3,3-trimethylbutyl) -octanoic acid is converted to a branched aldehyde having 9 carbons by oxo reaction of isobutylene dimer, and then carbon is obtained by aldol condensation of this aldehyde.
  • the branched unsaturated aldehyde of formula 18 can be produced by hydrogenation and oxidation (hereinafter abbreviated as “aldol condensation type”), which is commercially available, for example, from Nissan Chemical Industries.
  • 2-Heptylundecanoic acid can be produced by dimerizing nonyl alcohol by a gerbet reaction (also referred to as Guerbet reaction or Gerbe reaction) and oxidizing it, which is commercially available from, for example, Mitsubishi Chemical Corporation.
  • a gerbet reaction also referred to as Guerbet reaction or Gerbe reaction
  • oxidizing it which is commercially available from, for example, Mitsubishi Chemical Corporation.
  • a slightly different similar mixture is commercially available from Nissan Chemical Industries, and a methyl branched type in which the starting alcohol is not linearly saturated is also commercially available from Nissan Chemical Co. (hereinafter abbreviated as "garbet reaction type").
  • methyl-branched isostearic acid is obtained as a by-product at the time of dimer production of oleic acid, for example [for example, J. Amer. Oil Chem. Soc.
  • dimer acid which is a starting material of emery type isostearic acid may include not only oleic acid but also linoleic acid, linolenic acid and the like.
  • the content of component (E) in the second composition of the present invention is not particularly limited, but is preferably 50 to 99.9%, and more preferably 70 to 99.9%. Within this range, by using in combination with the first composition, the effect of preventing the color transfer of the first composition is enhanced, the color does not transfer to a coffee cup or the like, and the makeup does not collapse over time. It is more preferable in that a decorative film excellent in the above can be obtained.
  • the second composition of the present invention is an oily component, an oil gelling agent, a powder and a surface-treated product thereof, a surfactant, an aqueous component, as long as the effects of the present invention are not hindered.
  • Other components usually contained in cosmetics, such as ultraviolet absorbers, humectants, antioxidants, cosmetic ingredients, preservatives, pigments, and fragrances can be contained.
  • Oil components include hydrocarbons, regardless of the properties of solid oils, semi-solid oils, liquid oils, volatile oils, etc. that originate from animal oils, vegetable oils, synthetic oils, etc. , Oils and fats, waxes, hardened oils, ester oils, fatty acids, higher alcohols, silicone oils, fluorine-based oils, oily gelling agents and the like.
  • waxes such as beeswax, gay wax, carnauba wax, candelilla wax
  • fatty acids such as stearic acid, lauric acid, myristic acid, behenic acid, isostearic acid, oleic acid, stearyl alcohol, cetyl alcohol, lauryl Higher alcohols such as alcohol, oleyl alcohol, isostearyl alcohol, and behenyl alcohol
  • fluorinated oils such as perfluorodecane, perfluorooctane, and perfluoropolyether, dextrin octoate, dextrin laurate, dextrin palmitate, dextrin myristate
  • Stearic acid dextrin behenic acid dextrin
  • coconut oil fatty acid dextrin (palmitic acid / octanoic acid) dextrin
  • sucrose fatty acid ester starch fatty acid ester Le
  • aluminum isostearate potassium stea
  • the powder is not particularly limited by, for example, a spherical shape, a plate shape, a needle shape, a particle shape such as a haze shape, a fine particle, and a pigment grade, and a particle structure such as a porous shape and a nonporous shape. , Organic powders, pigment powders, composite powders and the like.
  • pearlescent pigments bismuth oxychloride, mica titanium, iron oxide coated mica, iron oxide coated mica titanium, organic pigment coated mica titanium, aluminum powder, etc., UV blocking agent, fine particle titanium oxide, fine particle zinc oxide, cerium oxide
  • composite powders such as fine particle titanium oxide-coated mica titanium, fine particle zinc oxide-coated mica titanium, and barium sulfate-coated mica titanium can be used, and one or more of these can be used.
  • these powders are used after surface treatment with a surface treatment agent such as silicones, fluorine compounds, metal soaps, oils and the like by a generally known method. Also good.
  • any surfactant that is generally used in cosmetics can be used.
  • Nonionic surfactants anionic surfactants, cationic surfactants, amphoteric surfactants, etc. Is mentioned.
  • glycerin fatty acid ester and its alkylene glycol adduct polyglycerin fatty acid ester and its alkylene glycol adduct, sorbitan fatty acid ester and its alkylene glycol adduct, polyoxyethylene hydrogenated castor oil, polyoxyalkylene alkyl co-modified organopolysiloxane, Examples include polyether-modified organopolysiloxane and lecithin.
  • aqueous component examples include, in addition to water, alcohols such as ethyl alcohol, glycols such as propylene glycol, 1,3-butylene glycol, 1,2-pentanediol, dipropylene glycol, and polyethylene glycol, glycerin, diglycerin, and the like.
  • alcohols such as ethyl alcohol
  • glycols such as propylene glycol, 1,3-butylene glycol, 1,2-pentanediol, dipropylene glycol, and polyethylene glycol
  • glycerin, diglycerin, and the like examples include glycerols such as glycerin and polyglycerin, and plant extracts such as aloe vera, witch hazel, hamamelis, cucumber, lemon, lavender and rose.
  • UV absorber examples include UV absorbers such as benzophenone, PABA, and salicylic acid, 4-tert-butyl-4′-methoxydibenzoylmethane, oxybenzone, and the like.
  • humectant examples include proteins, Examples include mucopolysaccharides, collagen, elastin, and keratin.
  • antioxidants examples include ⁇ -tocopherol and ascorbic acid.
  • beauty ingredients include vitamins, anti-inflammatory agents, and herbal medicines.
  • the agent examples include paraoxybenzoic acid ester, phenoxyethanol, and 1,2 pentadiol.
  • the shape of the first composition and the second composition of the present invention is not particularly limited, and examples thereof include solid, semi-solid, and liquid forms.
  • the liquid or semi-solid form is preferable, and the liquid form is particularly preferable.
  • the dosage form of the first composition and the second composition of the present invention is not particularly limited, but an oily or water-in-oil type in which the oil phase is a continuous phase is preferable from the viewpoints of usability and cosmetic durability. From the standpoint that the effects of the present invention can be remarkably exhibited, it is more preferable that the oil type has a water content of 1% or less.
  • the shape and dosage form of a 1st composition and a 2nd composition may be the same or different, it is preferable that it is the same from the point which the effect of this invention is exhibited easily.
  • the method for producing the first composition and the second composition of the present invention is not particularly limited.
  • the first composition after components (A) to (D) and an optional oily component are heated and mixed
  • the second composition for example, the component (E) and the optional oily component can be mixed and dispersed after mixing and dispersing any powder or aqueous component uniformly in the container.
  • These powders, aqueous components, and the like can be uniformly heated and mixed, and then poured into a container or mold after pouring and filling, and cooled.
  • a cosmetic set containing the first composition and the second composition of the present invention it is used as a lip cosmetic set such as lipstick, lip gloss, lip treatment, lip balm, lip base for foundation, lipstick overcoat, etc. Is preferred.
  • a method of use a method of applying the second composition after applying the first composition to the application part such as the lips is suitable. If this method of use is used, the effect of the present invention is remarkably exhibited. . For example, after apply
  • the time interval from the application of the first composition to the application of the second composition is not particularly limited, and the second composition may be applied immediately after the application of the first composition.
  • the application amount of the first composition and the second composition is not particularly limited.
  • the mass ratio of the application amount of the first composition and the application amount of the second composition in the coating region is 2: 1 to 1: 5.
  • the degree is preferable, and it is more preferably about 1: 1 to 1: 3.
  • Example 1 As is clear from Table 1, the experimental examples 1 to 12 were phase-separated, while the comparative experimental examples 1 to 6 were homogeneous solutions without phase separation.
  • Example 1 using polyglyceryl triisostearate having an emery type isostearic acid group, phase separation was observed, but a comparative experiment using polyglyceryl-2 triisostearate having an isole type isostearic acid group. In Example 1, no phase separation was observed.
  • the 1st composition shown in Table 2 and the 2nd composition shown in Table 3 were prepared according to the following manufacturing method. When used in combination with the first composition and the second composition obtained in Table 2 and Table 3, respectively, there is no color blur at the time of use, an effect of preventing color transfer, an effect of preventing makeup collapse, and a lack of tactile feeling.
  • the results evaluated by the following methods are shown in Tables 4 to 7, respectively.
  • Method for producing second composition A. Components (1) to (9) are mixed and dissolved by heating. B. (10) to (11) were added to A and mixed uniformly to obtain a second composition.
  • the 2nd composition shown in Table 8 was prepared according to the following manufacturing method.
  • each second composition is used in combination with the first composition of Formulation Example 1 shown in Table 2 above, there is no color blur at the time of use, an effect of preventing color transfer, an effect of preventing makeup loss, and a lack of feeling of touch.
  • the results are also shown in Table 8.
  • the color transfer prevention effect was further evaluated with the following test method. The result is shown in FIG.
  • Formulation Example 25 Lipstick (first composition) (Ingredient) (%) 1. (Acrylates / stearyl acrylate / Dimethicone methacrylate) copolymer 35 2. Dimethylpolysiloxane * 25 10 3. Dimethylpolysiloxane * 18 10 4). Hydrogenated polyisobutene * 26 35 5. 5. Talc remaining amount Silica * 21 1 7). Titanium oxide coated glass powder * 27 2 8). Red No. 202 1 9. Yellow No. 4 aluminum rake 1 10. Black iron oxide 0.2 11.
  • Formulation Example 26 Lipstick (first composition) (Ingredient) (%) 1. (Acrylates / Dimethicone) Copolymer * 16 45 2. Dimethylpolysiloxane * 28 5 3. Dimethylpolysiloxane * 18 3 4). Hydrogenated polyisobutene * 26 40 5. Boron nitride remaining 6. Silica * 21 1 7). Red No. 202 1 8). Yellow No. 4 aluminum rake 1 9. Black iron oxide 0.2 10. Fragrance 0.01 * 28: KF-96H-50,000 cs (manufactured by Shin-Etsu Chemical Co., Ltd.) (Production method) A. Ingredients (1) to (4) are heated and mixed to dissolve uniformly. B. Add components (5) to (10) to A and mix uniformly. C. B was filled into a container to obtain a lipstick.
  • Formulation Example 27 Lip gloss (second composition) (Ingredient) (%) 1. Fischer-Tropsch wax 2 2. Dextrin palmitate 5 3. (Vinylpyrrolidone / hexadecene) copolymer * 8 10 4). Diisostearyl malate * 13 5 5. Pentaerythrityl tetraisostearate * 29 30 6). Polyisobutene 5 7). Tridecyl trimellitate 25 8). Trimethylpentaphenyltrisiloxane 2 9. Lauroyl glutamate di (octyldodecyl / Phytosteryl / behenyl) 5 10. 10. 10.
  • Decaisostearate polyglyceryl-10 remaining amount Silica * 21 1 12 Titanium oxide coated glass powder * 30 2 13. Red No. 202 0.2 14 Yellow No. 4 aluminum lake 0.3 15. Black iron oxide 0.2 16. Ethylhexyl paramethoxycinnamate 1 17. dl- ⁇ -topherol 0.1 18. Fragrance 0.01 19. Propyl paraoxybenzoate 0.1 * 29: CRODAMOL PTIS-LQ- (JP) (manufactured by Croda Japan Co., Ltd.) * 30: Metashine 1080RC-R (Nippon Sheet Glass Co., Ltd.) (Production method)
  • A. Ingredients (1) to (10) are heated to 110 ° C. and uniformly dissolved.
  • Ingredients (11) to (19) are added to A and mixed uniformly.
  • Formulation Example 28 Lip gloss (oil-based solid dish cast, second composition) (Ingredient) (%) 1. Synthetic wax 7 2. Lanolin acetate 10 3. 3. Polyglyceryl triisostearate-2 * 3 remaining amount Ethyl hexyl hydroxystearate 8 5. Polyglyceryl-2 tetraisostearate-2 * 31 25 6). Polyglyceryl pentaisostearate * 32 10 7). N-lauroyl-L-glutamic acid (phytosteryl / octyldodecyl) 5 8). Dimer linoleic acid (phytosteryl / Isostearyl / cetyl / stearyl / beheni 10 9.
  • Trimethylsiloxyphenyl dimethicone 5 10.
  • Diphenylsiloxyphenyl trimethicone 1 11.
  • Cross polymer 2 12
  • Silica * 21 3 13.
  • Red 202 0.5 14 Yellow No. 4 0.03
  • Titanium oxide 0.4 16.
  • C After defoaming B, fill the container at 90 ° C. to obtain a product.
  • Formulation Example 29 Formulation Example 17: Lipstick (first composition) (Ingredient) (%) 1. Trimethylsiloxysilicic acid * 1 29 2. 2. Isododecane remaining amount Dimethylpolysiloxane * 18 22 4). Trimethylsiloxyphenyl dimethicone * 34 6 5. Disteadimonium hectorite 3 6.1,3-Butylene glycol 1 7). Red No. 104 1 8). Red No. 202 0.5 9. Yellow No.5 0.5 10. Titanium oxide 0.5 11. PEG-9 polydimethylsiloxyethyl dimethicone 0.1 12 Fragrance 0.01 * 34: BELSIL PDM 1000 (Asahi Kasei Wacker) (Production method) A. Ingredients (1) to (6) are heated and mixed to dissolve uniformly. B. Add components (7) to (12) to A and mix uniformly. C. B was filled into a container to obtain a lipstick.
  • Formulation Example 30 Lip Gloss (Second Composition) (Ingredient) (%) 1. Dextrin palmitate 7 2. Glyceryl triisostearate 50 3. 3. Decaisostearate polyglyceryl-10 remaining amount Dimethylsilylated silica 2 5.1,2-Pentanediol 0.2 (Production method)
  • Formulation Example 31 Lipstick (first composition) (Ingredient) (%) 1. Trimethylsiloxysilicic acid * 1 15 2. Polymethylsilsesquioxane 10 3. Polypropylsilsesquioxane 3 4). 4. Isododecane remaining amount Dimethylpolysiloxane * 18 15 6). Dimethiconol * 35 5 7). Trimethylsiloxyphenyl dimethicone * 33 8 8). Disteadimonium hectorite 3 9. 1,3-Butylene glycol 1 10. Red No. 226 1 11. Red No. 202 0.5 12 Yellow No. 0.5 13. Titanium oxide 0.5 14 PEG-9 polydimethylsiloxyethyl dimethicone 0.1 15.
  • Formulation Example 32 Lip gloss (oil-based solid dish cast, second composition) (Ingredient) (%) 1. Dibutyl lauroylglutamide 5 2. Dibutylethylhexanoylglutamide 2 3. Ethylhexyl hydroxystearate 40 4). 4. Non-isoisostearate polyglyceryl-10 remaining amount Dimethylsilylated silica 2 6.1,2-octanediol 0.1 7). Perfluorooctyltriethoxysilane treatment Iron oxide / titanium oxide coated glass powder * 36 0.5 8).

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KR102539387B1 (ko) * 2021-12-06 2023-06-07 (주)나우코스 광택감과 보습감 및 슬라이딩감이 뛰어난 유중수형 에멀젼 입술용 화장품 조성물

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WO2021140913A1 (ja) * 2020-01-06 2021-07-15 株式会社 資生堂 固形口唇化粧料
JP2021109830A (ja) * 2020-01-06 2021-08-02 株式会社 資生堂 固形口唇化粧料
CN114929186A (zh) * 2020-01-06 2022-08-19 株式会社资生堂 嘴唇用固体化妆品
JP7426828B2 (ja) 2020-01-06 2024-02-02 株式会社 資生堂 固形口唇化粧料
CN114929186B (zh) * 2020-01-06 2024-04-30 株式会社资生堂 嘴唇用固体化妆品

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