WO2017088698A1 - 一种合成革用亮烫亮处理剂及其制备方法 - Google Patents

一种合成革用亮烫亮处理剂及其制备方法 Download PDF

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WO2017088698A1
WO2017088698A1 PCT/CN2016/106293 CN2016106293W WO2017088698A1 WO 2017088698 A1 WO2017088698 A1 WO 2017088698A1 CN 2016106293 W CN2016106293 W CN 2016106293W WO 2017088698 A1 WO2017088698 A1 WO 2017088698A1
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weight
parts
synthetic leather
bright
treatment agent
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PCT/CN2016/106293
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French (fr)
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陈勇刚
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江苏宝泽高分子材料股份有限公司
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them

Definitions

  • the invention relates to the field of surface treatment agents for synthetic leather, in particular to a brightening and brightening treatment agent for synthetic leather used in the process of synthesizing the back of the leather, and the invention relates to a preparation method of the brightening and brightening treatment agent for the synthetic leather .
  • the synthetic leather surface treatment agent can be surface-coated according to the type of the product, which can improve the brightness, color and feel of the synthetic leather.
  • the synthetic leather surface treatment agent can be surface-coated according to the type of the product, which can improve the brightness, color and feel of the synthetic leather.
  • it is necessary not only to increase the touch of the synthetic leather, but also to ensure the brightness and color of the surface of the synthetic leather.
  • the existing surface treatment agents can not meet the increasing demands of consumers for the brightness and feel of synthetic leather. Therefore, there is an urgent need for a comprehensive effect of improving the touch of synthetic leather and improving the feel, brightness and gloss of synthetic leather. Treatment agent.
  • an object of the present invention is to provide a brightening and brightening treatment agent for synthetic leather.
  • the invention also provides a preparation method of the brightening and brightening treatment agent for the synthetic leather.
  • the utility model relates to a bright scalding treatment agent for synthetic leather, which is used for the later stage process of synthetic leather, and comprises the following components: bright and bright polyurethane resin, hot glaze powder, slip agent, DMF, butyl acetate and methyl ethyl ketone.
  • the components are as follows: 30-50 parts by weight of brightly lit polyurethane resin, 1-3 parts by weight of hot-bright powder, 0.5-2 parts by weight of slip agent, 15-20 parts by weight of DMF, acetic acid 20-25 parts by weight of butyl ester and 15-20 parts by weight of methyl ethyl ketone.
  • composition of the components is as follows: 35-45 parts by weight of the brightly lit polyurethane resin, 1-3 parts by weight of hot glitter, 0.7-1.8 parts by weight of slip agent, 16-19 parts by weight of DMF, 21-24 parts by weight of butyl acetate, and 16-19 parts by weight of methyl ethyl ketone.
  • the components are formulated as follows: 40 parts by weight of brightly lit polyurethane resin, 2 parts by weight of hot-bright powder, 1 part by weight of slipping agent, 19 parts by weight of DMF, 20 parts by weight of butyl acetate, butanone 18 parts by weight.
  • the invention also provides a preparation method of a brightening and brightening treatment agent for synthetic leather, comprising the following steps:
  • the components are as follows: 30-50 parts by weight of brightly lit polyurethane resin, 1-3 parts by weight of hot glaze, 0.5-2 parts by weight of slip agent, 15-20 parts by weight of DMF, butyl acetate 20-25 parts by weight, butanone 15-20 parts by weight.
  • the present invention has the following beneficial technical effects as compared with the prior art:
  • the components of the bright leather treatment agent for synthetic leather of the invention cooperate and work together, and the leather surface has strong layering feeling after ironing, with a certain skin feel, and the leather gloss made by the treatment agent is natural and the color is clear.
  • the leather surface is bright and transparent, and the effect of the leeches is strong after the scalding, and the comprehensive effect is excellent;
  • the brightening and brightening treatment agent for synthetic leather of the invention is a novel material for the latter stage treatment, and can be used in the existing synthetic leather production line, the process is simple, the production equipment does not need to be changed, and the production cost is not increased.
  • the brightening and brightening treatment agent for synthetic leather is composed of the following proportioning components: 30 parts by weight of bright glazed polyurethane resin, 1 part by weight of glazing powder, 0.5 parts by weight of slip agent, and 15 parts by weight of DMF (dimethylformamide). Parts: 20 parts by weight of butyl acetate and 15 parts by weight of methyl ethyl ketone.
  • the method for preparing the above-mentioned synthetic leather brightening and brightening treatment agent is: dissolving 30 parts by weight of the bright and bright polyurethane resin with 15 parts by weight of DMF under normal temperature and normal pressure, and then adding 1 part by weight of the hot bright powder, 0.5 weight A portion of the slip agent, 20 parts by weight of butyl acetate and 15 parts by weight of methyl ethyl ketone, stirred for at least 30 minutes until the mixture is uniformly mixed, and the bright leather treatment agent for the synthetic leather is obtained.
  • the performance indexes of the obtained bright leather brightening treatment agent for synthetic leather are shown in Table 1.
  • the brightening and brightening treatment agent for synthetic leather is composed of the following proportioning components: 35 parts by weight of bright glazed polyurethane resin, 2 parts by weight of glazing powder, 0.8 parts by weight of slip agent, 16 parts by weight of DMF, and 22 parts by weight of butyl acetate. Parts, 16 parts by weight of butanone.
  • the method for preparing the above-mentioned synthetic leather brightening and brightening treatment agent comprises: dissolving 35 parts by weight of the bright and bright polyurethane resin with 16 parts by weight of DMF under normal temperature and normal pressure, and then adding 2 parts by weight of the hot bright powder, 0.8 weight A portion of the slip agent, 22 parts by weight of butyl acetate and 16 parts by weight of methyl ethyl ketone, stirred for at least 30 minutes until the mixture is uniformly mixed, and the bright leather treatment agent for the synthetic leather is obtained.
  • the performance indexes of the obtained bright leather brightening treatment agent for synthetic leather are shown in Table 1.
  • the brightening and brightening treatment agent for synthetic leather is composed of the following proportioning components: 40 parts by weight of brightly glazed polyurethane resin, 2 parts by weight of glazing powder, 1 part by weight of slipping agent, 19 parts by weight of DMF, and 20 parts by weight of butyl acetate. Parts, butanone 18 parts by weight.
  • the above-mentioned synthetic leather with bright brightening treatment agent is prepared by dissolving 40 parts by weight of bright bright polyurethane resin with 19 parts by weight of DMF under normal temperature and normal pressure, and then adding 2 parts by weight of hot bright powder, 1 weight a slipper, 20 parts by weight of butyl acetate and 18 parts by weight of butanone, After stirring for at least 30 minutes until the mixture is uniformly mixed, the synthetic leather is treated with a brightening treatment agent.
  • the performance indexes of the obtained bright leather brightening treatment agent for synthetic leather are shown in Table 1.
  • the brightening and brightening treatment agent for synthetic leather is composed of the following proportioning components: 45 parts by weight of brightly glazed polyurethane resin, 2.5 parts by weight of glazing powder, 1.5 parts by weight of slipping agent, 17 parts by weight of DMF, and 23 parts by weight of butyl acetate. Parts, butanone 18 parts by weight.
  • the method for preparing the above-mentioned synthetic leather brightening and brightening treatment agent comprises: dissolving 45 parts by weight of the bright and bright polyurethane resin with 17 parts by weight of DMF under normal temperature and normal pressure, and then adding 2.5 parts by weight of the hot bright powder, 1.5 weight A portion of the slip agent, 23 parts by weight of butyl acetate and 18 parts by weight of methyl ethyl ketone, stirred for at least 30 minutes until the mixture is uniformly mixed, that is, the synthetic leather is treated with a brightening treatment agent.
  • the performance indexes of the obtained bright leather brightening treatment agent for synthetic leather are shown in Table 1.
  • the brightening and brightening treatment agent for synthetic leather is composed of the following proportioning components: 50 parts by weight of bright glazed polyurethane resin, 3 parts by weight of glazing powder, 2 parts by weight of slip agent, 20 parts by weight of DMF, and 25 parts by weight of butyl acetate. Parts, butanone 20 parts by weight.
  • the above-mentioned synthetic leather brightening treatment agent is prepared by dissolving 50 parts by weight of brightly bright polyurethane resin with 20 parts by weight of DMF under normal temperature and normal pressure, and then adding 3 parts by weight of hot bright powder, 2 weights. A portion of the slip agent, 25 parts by weight of butyl acetate and 20 parts by weight of methyl ethyl ketone, stirred for at least 30 minutes until the mixture is uniformly mixed, and the bright leather treatment agent for the synthetic leather is obtained.
  • the performance indexes of the obtained bright leather brightening treatment agent for synthetic leather are shown in Table 1.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Treatment And Processing Of Natural Fur Or Leather (AREA)

Abstract

一种合成革用亮烫亮处理剂，其用于合成革的后段工艺，包含以下组分：亮烫亮聚氨酯树脂，烫亮粉，滑爽剂，DMF，醋酸丁酯，丁酮。一种合成革用亮烫亮处理剂的制备方法。合成革用亮烫亮处理剂的各组分相互协调、共同作用，烫光后革面层次感强，带有一定肤感，用此种处理剂做出的革光泽自然，色泽清晰，革面艳度与通透感佳，烫光后水揉真皮效果强，综合效果优；合成革用亮烫亮处理剂是后段的一种新型材料，能够用于现有的合成革生产线，工艺简单，无需改变生产设备，不会增加生产成本。

Description

一种合成革用亮烫亮处理剂及其制备方法 技术领域
本发明涉及合成革用表面处理剂领域，具体地，涉及一种用于合成革后段工艺的合成革用亮烫亮处理剂，本发明同时涉及该合成革用亮烫亮处理剂的制备方法。
背景技术
合成革表面处理剂可以根据产品的类别进行表面涂饰,其可以改善合成革的亮度、色泽以及手感。然而,随着消费者对皮革表面的色泽和手感要求越来越高,不但要增加合成革的触感,还要保证合成革表面的亮度及色泽度等。而现有的表面处理剂已经不能满足消费者对合成革的亮度及手感日益增加的要求,因此急需一种既能提高合成革触感，又能提高合成革的手感，亮度、光泽等综合效果的处理剂。
发明内容
为了解决上述问题及缺陷，本发明的目的是提供一种合成革用亮烫亮处理剂。本发明还提供该合成革用亮烫亮处理剂的制备方法。
本发明的合成革用亮烫亮处理剂通过以下技术方案实现：
一种合成革用亮烫亮处理剂，其用于合成革的后段工艺，包含以下组分：亮烫亮聚氨酯树脂，烫亮粉，滑爽剂，DMF，醋酸丁酯，丁酮。
进一步地，所述各组分的配比如下：亮烫亮聚氨酯树脂30-50重量份，烫亮粉1-3重量份，滑爽剂0.5-2重量份，DMF 15-20重量份，醋酸丁酯20-25重量份，丁酮15-20重量份。
进一步地，所述各组分的配比如下：亮烫亮聚氨酯树脂35-45重量份， 烫亮粉1-3重量份，滑爽剂0.7-1.8重量份，DMF 16-19重量份，醋酸丁酯21-24重量份，丁酮16-19重量份。
进一步地，所述各组分的配比如下：亮烫亮聚氨酯树脂40重量份，烫亮粉2重量份，滑爽剂1重量份，DMF 19重量份，醋酸丁酯20重量份，丁酮18重量份。
本发明还提供一种合成革用亮烫亮处理剂的制备方法，包含以下步骤：
按重量配比称取各组分物质，用DMF将亮烫亮聚氨酯树脂溶解，然后加入烫亮粉，滑爽剂，醋酸丁酯和丁酮搅拌均匀，即得所述合成革用亮烫亮处理剂。
进一步地，各组分的配比如下：亮烫亮聚氨酯树脂30-50重量份，烫亮粉1-3重量份，滑爽剂0.5-2重量份，DMF 15-20重量份，醋酸丁酯20-25重量份，丁酮15-20重量份。
进一步地，所有步骤均在常温常压下进行。
由于采用以上技术方案，本发明与现有技术相比具有如下有益技术效果：
本发明的合成革用亮烫亮处理剂的各组分相互协调、共同作用，烫光后革面层次感强，带有一定肤感，用此种处理剂做出的革光泽自然，色泽清晰，革面艳度与通透感佳，烫光后水揉真皮效果强，综合效果优；
本发明的合成革用亮烫亮处理剂是后段处理的一种新型材料，能够用于现有的合成革生产线，工艺简单，无需改变生产设备，不会增加生产成本。
具体实施方式
为了使本发明的目的、技术方案及优点更加清楚明白，下面结合实施例，对本发明进行进一步详细说明。应当理解，此处所描述的具体实施例仅用以解释本发明，并不用于限定本发明。
实施例1
合成革用亮烫亮处理剂由以下配比的组分组成：亮烫亮聚氨酯树脂30重量份，烫亮粉1重量份，滑爽剂0.5重量份，DMF(二甲基甲酰胺)15重量份，醋酸丁酯20重量份，丁酮15重量份。
上述合成革用亮烫亮处理剂的制备方法是：在常温常压下，用15重量份的DMF将30重量份的亮烫亮聚氨酯树脂溶解，然后加入1重量份的烫亮粉，0.5重量份的滑爽剂，20重量份的醋酸丁酯和15重量份的丁酮，搅拌至少30分钟至混合物混合均匀后，即得所述合成革用亮烫亮处理剂。所得到的合成革用亮烫亮处理剂的性能指标见表1。
上述制备过程中所采用的搅拌等方法均为本领域内惯用的方法。
实施例2
合成革用亮烫亮处理剂由以下配比的组分组成：亮烫亮聚氨酯树脂35重量份，烫亮粉2重量份，滑爽剂0.8重量份，DMF 16重量份，醋酸丁酯22重量份，丁酮16重量份。
上述合成革用亮烫亮处理剂的制备方法是：在常温常压下，用16重量份的DMF将35重量份的亮烫亮聚氨酯树脂溶解，然后加入2重量份的烫亮粉，0.8重量份的滑爽剂，22重量份的醋酸丁酯和16重量份的丁酮，搅拌至少30分钟至混合物混合均匀后，即得所述合成革用亮烫亮处理剂。所得到的合成革用亮烫亮处理剂的性能指标见表1。
上述制备过程中所采用的搅拌等方法均为本领域内惯用的方法。
实施例3
合成革用亮烫亮处理剂由以下配比的组分组成：亮烫亮聚氨酯树脂40重量份，烫亮粉2重量份，滑爽剂1重量份，DMF 19重量份，醋酸丁酯20重量份，丁酮18重量份。
上述合成革用亮烫亮处理剂的制备方法是：在常温常压下，用19重量份的DMF将40重量份的亮烫亮聚氨酯树脂溶解，然后加入2重量份的烫亮粉，1重量份的滑爽剂，20重量份的醋酸丁酯和18重量份的丁酮， 搅拌至少30分钟至混合物混合均匀后，即得所述合成革用亮烫亮处理剂。所得到的合成革用亮烫亮处理剂的性能指标见表1。
上述制备过程中所采用的搅拌等方法均为本领域内惯用的方法。
实施例4
合成革用亮烫亮处理剂由以下配比的组分组成：亮烫亮聚氨酯树脂45重量份，烫亮粉2.5重量份，滑爽剂1.5重量份，DMF 17重量份，醋酸丁酯23重量份，丁酮18重量份。
上述合成革用亮烫亮处理剂的制备方法是：在常温常压下，用17重量份的DMF将45重量份的亮烫亮聚氨酯树脂溶解，然后加入2.5重量份的烫亮粉，1.5重量份的滑爽剂，23重量份的醋酸丁酯和18重量份的丁酮，搅拌至少30分钟至混合物混合均匀后，即得所述合成革用亮烫亮处理剂。所得到的合成革用亮烫亮处理剂的性能指标见表1。
上述制备过程中所采用的搅拌等方法均为本领域内惯用的方法。
实施例5
合成革用亮烫亮处理剂由以下配比的组分组成：亮烫亮聚氨酯树脂50重量份，烫亮粉3重量份，滑爽剂2重量份，DMF 20重量份，醋酸丁酯25重量份，丁酮20重量份。
上述合成革用亮烫亮处理剂的制备方法是：在常温常压下，用20重量份的DMF将50重量份的亮烫亮聚氨酯树脂溶解，然后加入3重量份的烫亮粉，2重量份的滑爽剂，25重量份的醋酸丁酯和20重量份的丁酮，搅拌至少30分钟至混合物混合均匀后，即得所述合成革用亮烫亮处理剂。所得到的合成革用亮烫亮处理剂的性能指标见表1。
上述制备过程中所采用的搅拌等方法均为本领域内惯用的方法。
表1
Figure PCTCN2016106293-appb-000001
Figure PCTCN2016106293-appb-000002
以上所述仅为本发明的较佳实施例，并非用来限定本发明的实施范围；如果不脱离本发明的精神和范围，对本发明进行修改或者等同替换，均应涵盖在本发明权利要求的保护范围当中。

Claims (7)

  1. 一种合成革用亮烫亮处理剂，其用于合成革的后段工艺，其特征在于，包含以下组分：亮烫亮聚氨酯树脂，烫亮粉，滑爽剂，DMF，醋酸丁酯，丁酮。
  2. 根据权利要求1所述的合成革用亮烫亮处理剂，其特征在于，所述各组分的配比如下：亮烫亮聚氨酯树脂30-50重量份，烫亮粉1-3重量份，滑爽剂0.5-2重量份，DMF 15-20重量份，醋酸丁酯20-25重量份，丁酮15-20重量份。
  3. 根据权利要求2所述的合成革用亮烫亮处理剂，其特征在于，所述各组分的配比如下：亮烫亮聚氨酯树脂35-45重量份，烫亮粉1-3重量份，滑爽剂0.7-1.8重量份，DMF 16-19重量份，醋酸丁酯21-24重量份，丁酮16-19重量份。
  4. 根据权利要求2或3所述的合成革用亮烫亮处理剂，其特征在于，所述各组分的配比如下：亮烫亮聚氨酯树脂40重量份，烫亮粉2重量份，滑爽剂1重量份，DMF 19重量份，醋酸丁酯20重量份，丁酮18重量份。
  5. 一种上述权利要求所述的合成革用亮烫亮处理剂的制备方法，其特征在于，包含以下步骤：
    按重量配比称取各组分物质，用DMF将亮烫亮聚氨酯树脂溶解，然后加入烫亮粉，滑爽剂，醋酸丁酯和丁酮搅拌均匀，即得所述合成革用亮烫亮处理剂。
  6. 根据权利要求5所述的合成革用亮烫亮处理剂的制备方法，其特征在于，各组分的配比如下：亮烫亮聚氨酯树脂30-50重量份，烫亮粉1-3重量份，滑爽剂0.5-2重量份，DMF 15-20重量份，醋酸丁酯20-25重量份，丁酮15-20重量份。
  7. 根据权利要求5所述的合成革用亮烫亮处理剂的制备方法，其特征在于，所有步骤均在常温常压下进行。
PCT/CN2016/106293 2015-11-27 2016-11-17 一种合成革用亮烫亮处理剂及其制备方法 WO2017088698A1 (zh)

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CN106521958A (zh) * 2016-10-27 2017-03-22 江苏宝泽高分子材料股份有限公司 一种合成革用雾烫亮处理剂及其制备方法
CN106521960A (zh) * 2016-10-28 2017-03-22 江苏宝泽高分子材料股份有限公司 一种合成革用水性亮烫亮处理剂及其制备方法
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