WO2015007861A1 - Vorrichtung und verfahren zum sequentiellen schmelzen und raffinieren in einem kontinuierlichen verfahren - Google Patents
Vorrichtung und verfahren zum sequentiellen schmelzen und raffinieren in einem kontinuierlichen verfahren Download PDFInfo
- Publication number
- WO2015007861A1 WO2015007861A1 PCT/EP2014/065429 EP2014065429W WO2015007861A1 WO 2015007861 A1 WO2015007861 A1 WO 2015007861A1 EP 2014065429 W EP2014065429 W EP 2014065429W WO 2015007861 A1 WO2015007861 A1 WO 2015007861A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- treatment chamber
- treatment
- liquid
- liquid material
- transfer channel
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 86
- 238000010924 continuous production Methods 0.000 title claims description 8
- 238000002844 melting Methods 0.000 title abstract description 13
- 230000008018 melting Effects 0.000 title abstract description 13
- 238000007670 refining Methods 0.000 title abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 69
- 239000007788 liquid Substances 0.000 claims abstract description 15
- 229910052751 metal Inorganic materials 0.000 claims abstract description 10
- 239000002184 metal Substances 0.000 claims abstract description 10
- 239000000919 ceramic Substances 0.000 claims abstract description 5
- 239000011344 liquid material Substances 0.000 claims description 40
- 238000010894 electron beam technology Methods 0.000 claims description 22
- 239000000155 melt Substances 0.000 claims description 12
- 230000005672 electromagnetic field Effects 0.000 claims description 7
- 229910052710 silicon Inorganic materials 0.000 claims description 5
- 239000010703 silicon Substances 0.000 claims description 5
- 239000004020 conductor Substances 0.000 claims description 2
- 238000007711 solidification Methods 0.000 claims 2
- 230000008023 solidification Effects 0.000 claims 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- 239000000956 alloy Substances 0.000 abstract description 4
- 229910045601 alloy Inorganic materials 0.000 abstract description 4
- 150000002739 metals Chemical class 0.000 abstract description 3
- 238000010438 heat treatment Methods 0.000 description 8
- 239000007789 gas Substances 0.000 description 7
- 239000012535 impurity Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- 238000005192 partition Methods 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000010309 melting process Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000005275 alloying Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000001404 mediated effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 239000003870 refractory metal Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- -1 semimetals Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/04—Refining by applying a vacuum
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/037—Purification
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27B—FURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
- F27B19/00—Combinations of furnaces of kinds not covered by a single preceding main group
- F27B19/02—Combinations of furnaces of kinds not covered by a single preceding main group combined in one structure
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D11/00—Arrangement of elements for electric heating in or on furnaces
- F27D11/06—Induction heating, i.e. in which the material being heated, or its container or elements embodied therein, form the secondary of a transformer
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D11/00—Arrangement of elements for electric heating in or on furnaces
- F27D11/08—Heating by electric discharge, e.g. arc discharge
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D11/00—Arrangement of elements for electric heating in or on furnaces
- F27D11/12—Arrangement of elements for electric heating in or on furnaces with electromagnetic fields acting directly on the material being heated
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D3/00—Charging; Discharging; Manipulation of charge
- F27D3/14—Charging or discharging liquid or molten material
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/30—Electron-beam or ion-beam tubes for localised treatment of objects
- H01J37/305—Electron-beam or ion-beam tubes for localised treatment of objects for casting, melting, evaporating, or etching
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/32—Gas-filled discharge tubes
- H01J37/32009—Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/16—Remelting metals
- C22B9/22—Remelting metals with heating by wave energy or particle radiation
- C22B9/226—Remelting metals with heating by wave energy or particle radiation by electric discharge, e.g. plasma
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/16—Remelting metals
- C22B9/22—Remelting metals with heating by wave energy or particle radiation
- C22B9/228—Remelting metals with heating by wave energy or particle radiation by particle radiation, e.g. electron beams
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27B—FURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
- F27B19/00—Combinations of furnaces of kinds not covered by a single preceding main group
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D27/00—Stirring devices for molten material
Definitions
- This invention relates to an apparatus and method practicable with the apparatus for sequentially melting and refining materials.
- the materials treated in the process are converted to a liquid state by one or more heat sources or are already in such a state prior to treatment.
- the method is particularly suitable for treating metals, semi-metals and ceramics, for example to produce alloys and / or to refine the materials.
- One such method is the electron beam method, in which an electron beam is directed onto a material in order to generate heat there in a targeted manner. This process is particularly flexible because a specific portion of material can be heated to very high temperatures. When larger portions of material are to be heat treated, the electron beam can be scanned across the material to be heated.
- the electron beam melting process can be carried out only under vacuum. Due to the inherent process control in vacuum, there is the advantage that any impurities present in the material can be removed. The material is refined. On the other hand, due to the vacuum in the electron beam method, the material composition can also be changed by evaporation of volatiles, which may be advantageous, for example, in refining. This volatilization of volatile constituents naturally occurs particularly strongly in material mixtures which are inhomogeneous, for example mixtures of metal chips and additives which have not yet melted. Evaporation may be desirable or a problem if the original composition is to be preserved. Of course, this problem also occurs in other melting and refining processes, which are carried out under vacuum at temperatures> 500 ° C. Another known from the prior art method is the plasma melting, in which the material is heated at pressures that are well above 1 mbar, in particular above 100 mbar. Plasma melting is good for melting many materials.
- the processes can be divided into three categories: the high vacuum processes are processes which are carried out in a pressure range between 10 ⁇ 7 mbar and 10 ⁇ 2 mbar.
- the vacuum processes are processes which are carried out in a pressure range between 10 -2 mbar and 100 mbar.
- the low pressure processes are carried out in a pressure range between 100 mbar and 1 atm.
- a melt has to be treated successively at different pressures and the heating methods used in the methods work only or only preferably or efficiently in the respective pressure range, then today it is necessary to carry out this treatment in a batch process.
- the material has to be removed from one crucible in between and transferred to another one.
- Continuous treatment with various procedures is often desirable.
- a reactive gas such as oxygen
- DE 1 291 760 A describes a process in which a basic charge of a metal is first heated by means of electron beam heating in vacuo. Volatile alloy components are then added and heated with plasma jet. The treatment The treatment of the metal, however, takes place in a single treatment vessel, where the corresponding melt is heated successively by different methods at different pressures. Continuous operation is only possible with a very complex system. Further, the process described therein requires sequential addition of alloying ingredients, which preferably does not occur according to the present invention. Furthermore, pressure differences are not made available for the transport of the material, because the transfer channel does not open into the second process container, but ends above the level of the melt in the second container. Incidentally, the transport of the melt through the transfer channel is not effected by traveling electromagnetic fields.
- This invention thus provides a method and apparatus.
- the method comprises the following steps
- a liquid material is heated and / or refined at different pressures in different treatment chambers, the delimitation of the pressure levels being effected by the liquid material itself,
- the liquid material is transferred from a first treatment chamber to another second treatment chamber, wherein the transfer of the material is achieved by pressure differences in combination with electromagnetic influencing the flow rate between the treatment chambers, and
- the heat sources used in the treatment chambers operate independently of each other, characterized in that the electromagnetic interference takes place using means which generate a traveling electromagnetic field and the influencing comprises slowing down and / or stopping the flow of the liquid material, and the Pressure in the second treatment chamber is lower than in the first treatment chamber.
- the at least two heat sources operate independently of one another preferably means that they are different heat sources or the same heat sources operating at different pressures.
- one heat source is a plasma torch and another heat source is an electron beam gun, or both heat sources are electron beam guns or both heat sources are plasma torches that operate at different pressures.
- Electromagnetic flow rate control occurs using means that can generate a traveling electromagnetic field. Through these means, the flow of the liquid material can be induced, accelerated, slowed or even stopped. By slowing down or stopping the flow of material, differences in level of the melts in the various treatment chambers due to the pressure difference can be reduced and / or prevented.
- Preferred means are one or more coils, in particular segmented coils or a plurality of sequential coils arranged along a transfer channel.
- the method according to the invention for sequential heat treatment is used in particular for the production of alloys and / or for refining. It can include one or more of the following steps: Introducing the material to be treated into the first treatment chamber,
- the treatment of the material is preferably carried out at a pressure of> 10 mbar, more preferably> 100 mbar, more preferably> 300 mbar, more preferably> 500 mbar and particularly preferably> 800 mbar.
- the pressure is preferably lower, in particular the pressure there is only up to 10 mbar, preferably up to 1 mbar, more preferably up to 0.1 mbar and particularly preferably up to 0.01 mbar.
- the transfer of the liquid material from the one treatment chamber into the other treatment chamber preferably takes place by means of a transfer channel which allows a continuous flow of the liquid material.
- the method can therefore be operated continuously.
- a semi-continuous or batch operation is possible, which is less preferred for economic reasons.
- the transfer channel preferably allows the transfer of the liquid material from the first to the second treatment chamber.
- the transfer of the liquid material occurs inter alia due to pressure differences between the treatment chambers.
- the liquid material flows along the pressure gradients and / or mediated by the electromagnetic influence of the liquid material from the first to the second treatment chamber.
- the pressure in the second treatment chamber is lower than in the first treatment chamber, so that the liquid material is conveyed by means of an existing pressure gradient, preferably in combination with existing differences in height targeted.
- the method is preferably carried out or the device designed such that the transfer channel in operation completely with Material is filled. This ensures that the different pressures are maintained in the treatment chambers.
- the treatment chambers are preferably designed such that they are hermetically sealable with respect to the environment, so that the process pressure can be adjusted accordingly. This is especially true for the treatment chamber in which lower pressure prevails.
- the treatment chambers can be either completely separate treatment chambers or by dividing a large chamber into two treatment chambers, such as by introducing a separating element, such as a partition, done in the large chamber.
- a process container in particular a crucible or a pan, can be arranged, in which the material is located during the process.
- the process container can also be designed as part of the treatment chamber or be identical to it.
- each treatment chamber contains a process container.
- a process vessel extends from one treatment chamber to the other, wherein the transfer channel may be an opening in the separation element.
- the device according to the invention preferably has a supply device which allows a continuous introduction of the material into the first treatment chamber.
- a feeder can be, for example, a conveyor trough.
- the treated material can be removed after carrying out the method according to the invention from the second treatment chamber.
- the device preferably comprises a removal device, which allows a removal of the material.
- the second treatment chamber is operated at a process pressure which is below the ambient pressure, it is advantageous to make the removal of the treated material so that the negative pressure in the chamber is maintained. This can preferably be done by the
- Removal device is designed as a drain.
- a collection container for the treated material is in the treatment Lower pressure chamber so that the container can remain in the treatment chamber until it is removed.
- the transfer channel establishes a connection between the two treatment chambers. It is preferably heated, such as with an induction heater or a burner, so that the liquid material does not solidify. In embodiments without heating the transfer channel, the treatment chambers should be placed very close together when using material with a high melting point and / or unfavorable viscosity-temperature profile.
- the transfer channel advantageously has two openings, one proximal and one distal. Through the proximal opening, the liquid material from the first treatment chamber can enter the transfer channel, through the distal opening it can emerge again into the second treatment chamber.
- the proximal opening of the transfer channel may be arranged so that the liquid material from the first treatment chamber or from the first process container falls down into the transfer channel.
- the first treatment chamber or the first process container therefore does not have to be connected to the transfer channel.
- the proximal opening of the transfer channel is preferably arranged in the lower region of the first treatment chamber or, if the treatment chamber is not also the process container, in the lower region of the first process container. This has proved to be advantageous because the supply of material to be treated can most easily take place from above and also the heating preferably takes place from above.
- the material is already in a sufficiently liquid state to flow through the transfer channel.
- the distal opening opens into the second treatment chamber, in particular in its lower region, or, if the treatment chamber is not also the process container, in its lower region. In particular, it opens into a region of the second treatment chamber, which lies below the level of the melt in this treatment chamber.
- the level of the liquid material is preferably higher in one treatment chamber than in the other treatment chamber. This level difference arises in particular because of the different process pressures in the two chambers. For this reason, the second treatment chamber or the second process chamber container preferably arranged higher than the first treatment chamber or the first process container. However, this height difference can be much smaller than in the prior art, since counteracting can be counteracted according to the invention.
- the melting and refining processes in the first treatment chamber are preferably carried out using a low pressure process, in particular by a plasma melting process.
- the material is preferably heated to temperatures of 1000 to 3000 ° C, more preferably 1200 to 2500 ° C, particularly preferably 1400 to 2000 ° C.
- reactive gases e.g., oxygen, hydrogen, nitrogen
- inert gases e.g., argon, helium
- the device according to the invention preferably comprises a gas inlet, in particular in order to be able to introduce gases controlled into the first treatment chamber.
- the treatment chamber in which a lower pressure prevails, preferably does not include such gas inlets.
- the melting and refining processes in the second treatment chamber are preferably carried out using high vacuum methods, or vacuum methods, in particular by an electron beam method.
- the material is preferably heated to temperatures of 1000 to 4000 ° C, more preferably 1200 to 3800 ° C, particularly preferably 1400 to 3500 ° C.
- the introduction of a reactive gas is dispensed with or small quantities of gas are used which do not preclude maintaining the operating pressure.
- the material to be treated preferably comprises metals, semimetals, ceramics or mixtures thereof.
- the material to be treated is preferably substantially metallic, semi-metallic and / or has sufficient electrical conductivity in the liquid state.
- Preferred materials to be treated are titanium and silicon; however, it is also possible to use steels, reactive and refractory metals or composite materials which comprise ceramics.
- it preferably has a conductivity in the liquid state of at least 1 * 10 2 S / m.
- the melting point of the material to be treated is preferably> 1000 ° C at atmospheric pressure.
- the material to be melted may contain contaminants which are removed under the different conditions of the process.
- contaminants which are removed under the different conditions of the process.
- impurities which may be included in the material to be melted are boron and phosphorus.
- the material to be treated comprises silicon, in particular in a proportion of more than 95% (m / m).
- this is heated in the first treatment chamber to remove impurities, under the conditions of the invention, for example, boron can be removed; Thereafter, the silicon is transferred as a liquid melt via the transfer channel in the second treatment chamber, where due to the low pressure, other impurities such as phosphorus can be removed.
- the device according to the invention is also suitable for carrying out the method.
- the device preferably comprises a first treatment chamber, a second treatment chamber, and a transfer channel connecting the two chambers, wherein both treatment chambers are each provided with at least one heat source.
- the heat sources preferably operate independently of each other and are independently controllable.
- the transfer channel is preferably arranged so that it rises from one to the other treatment chamber.
- the device comprises means for electromagnetic influencing the flow rate. These agents affect the flow rate of a liquid, conductive material that is in the transfer channel. These means are those that can generate traveling electromagnetic fields. These are preferably one or more coils, in particular segmented coils.
- the means are preferably around the transfer channel arranged. In addition to coils but other means are conceivable with which electromagnetic fields can be generated, which allow influencing the flow ß Malawi in terms of a magnetohydrodynamic influence.
- the first treatment chamber has a heat source selected from plasma torch and electron gun, while the second treatment chamber comprises an electron beam gun as the heat source.
- each treatment chamber 1 contains one process container 2 each.
- the material to be treated 3 which must be liquid at the latest when entering the transfer channel 4.
- Heat source 5 may for example be a plasma torch
- heat source 6 may be for example an electron beam gun.
- the level of the liquid material in the second treatment chamber is higher than in the first one.
- the liquid material must therefore rise in the transfer channel 4. This is caused by a pressure difference, because the plasma torch is operated in the low pressure region in this example, while the electron beam gun is operated in vacuum.
- the arrows show the flow direction of the liquid material.
- the liquid material completely fills the transfer channel 4 so that the pressure levels in both chambers can be maintained.
- the feeder 7 supplies new material to be treated for a continuous process to be possible.
- the container 8 collects the treated material.
- FIG. 2 shows a device according to the invention with a large-sized chamber 1, which is divided using a partition 9 in two treatment chambers.
- the material to be treated 3 which must be liquid at the latest when entering the transfer channel 4.
- the transfer channel is designed very short here. This has the advantage that the liquid material cools only slightly when it passes from one treatment chamber to another.
- Heat source 5 may for example be a plasma torch
- heat source 6 may be for example an electron beam gun. It can be seen that the level of the liquid material in the second treatment chamber is higher than in the first one.
- each treatment chamber 1 contains one process container 2 each.
- the material to be treated 3 which must be liquid at the latest when entering the transfer channel 4.
- Heat source 5 may for example be a plasma torch
- heat source 6 may be for example an electron beam gun.
- the level of the liquid material in the second treatment chamber is higher than in the first one. The liquid material must therefore rise in the transfer channel 4. This is caused by a pressure difference, because the plasma torch is operated in the low pressure region in this example, while the electron beam gun is operated in vacuum.
- the arrows show the flow direction of the liquid material.
- the liquid material completely fills the transfer channel 4 so that the pressure levels in both chambers can be maintained.
- the feeder 7 supplies new material to be treated for a continuous process to be possible.
- the container 8 collects the treated material.
- the apparatus comprises means for magnetohydrodynamically regulating the flow, such as coils 10.
- the proximal opening of the transfer channel is here arranged so that the liquid material from the first process container falls down into the transfer channel.
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Engineering & Computer Science (AREA)
- Plasma & Fusion (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Electromagnetism (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Power Engineering (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Furnace Details (AREA)
- Continuous Casting (AREA)
Abstract
Description
Claims
Priority Applications (7)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP14741282.9A EP3022325B1 (de) | 2013-07-18 | 2014-07-17 | Vorrichtung und verfahren zum sequentiellen schmelzen und raffinieren in einem kontinuierlichen verfahren |
RU2016105398A RU2639083C2 (ru) | 2013-07-18 | 2014-07-17 | Устройство и способ для последовательной плавки и рафинирования непрерывным методом |
JP2016526650A JP2016530400A (ja) | 2013-07-18 | 2014-07-17 | 連続工程における連続的溶融及び精製のための装置及び方法 |
PL14741282T PL3022325T3 (pl) | 2013-07-18 | 2014-07-17 | Urządzenie i sposób sekwencyjnego topienia i rafinacji w sposobie ciągłym |
US14/903,725 US20160160314A1 (en) | 2013-07-18 | 2014-07-17 | Apparatus and method for sequential melting and refining in a continuous process |
CN201480040667.2A CN105378120A (zh) | 2013-07-18 | 2014-07-17 | 连续处理过程中用于顺序熔化和精炼的方法及设备 |
CA2916477A CA2916477A1 (en) | 2013-07-18 | 2014-07-17 | Apparatus and method for sequential melting and refining in a continuous process |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102013107685.8 | 2013-07-18 | ||
DE102013107685.8A DE102013107685B3 (de) | 2013-07-18 | 2013-07-18 | Vorrichtung und Verfahren zum sequentiellen Schmelzen und Raffinieren in einem kontinuierlichen Verfahren |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2015007861A1 true WO2015007861A1 (de) | 2015-01-22 |
Family
ID=51211225
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2014/065429 WO2015007861A1 (de) | 2013-07-18 | 2014-07-17 | Vorrichtung und verfahren zum sequentiellen schmelzen und raffinieren in einem kontinuierlichen verfahren |
Country Status (9)
Country | Link |
---|---|
US (1) | US20160160314A1 (de) |
EP (1) | EP3022325B1 (de) |
JP (1) | JP2016530400A (de) |
CN (1) | CN105378120A (de) |
CA (1) | CA2916477A1 (de) |
DE (1) | DE102013107685B3 (de) |
PL (1) | PL3022325T3 (de) |
RU (1) | RU2639083C2 (de) |
WO (1) | WO2015007861A1 (de) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20220349026A1 (en) * | 2021-04-26 | 2022-11-03 | Kabushiki Kaisha Toyota Chuo Kenkyusho | Metal purifying method and metal purifying apparatus |
CN113368522B (zh) * | 2021-07-02 | 2022-12-23 | 上海大学 | 一种铟的真空蒸馏装置和蒸馏方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1291760B (de) * | 1963-11-08 | 1969-04-03 | Suedwestfalen Ag Stahlwerke | Verfahren und Vorrichtung zum diskontinuierlichen und kontinuierlichen Vakuum-Schmelzen und -Giessen von Staehlen und stahlaehnlichen Legierungen (Superiegierungen) |
DE2118894A1 (de) * | 1970-04-21 | 1971-11-04 | Groupement Atomique Alsacienne Atiantique , Le Plessis Robinson (Frank reich) | Anordnung zum Behandeln und Fordern flussiger Metalle zum Zwecke ihres Ver gießens |
US4027722A (en) * | 1963-02-01 | 1977-06-07 | Airco, Inc. | Electron beam furnace |
US5503655A (en) * | 1994-02-23 | 1996-04-02 | Orbit Technologies, Inc. | Low cost titanium production |
EP0796820A1 (de) * | 1996-03-19 | 1997-09-24 | Kawasaki Steel Corporation | Verfahren und Vorrichtung zur Raffinierung von Silicium |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2132534B2 (de) * | 1971-04-07 | 1974-11-08 | Activite Atom Avance | |
DE2501603B2 (de) * | 1975-01-16 | 1977-08-25 | Institut problem htja Akademn Nauk Ukrainskoj SSR, Kiew (Sowjetunion) | Einrichtung zur vakuumbehandlung fluessiger metalle |
JPH0421727A (ja) * | 1990-05-14 | 1992-01-24 | Daido Steel Co Ltd | チタン鋳塊の製造方法および装置 |
JPH05285638A (ja) * | 1992-04-07 | 1993-11-02 | Toshiba Mach Co Ltd | 電磁ポンプのダクト |
NL1001976C2 (nl) * | 1995-12-22 | 1997-06-24 | Hoogovens Groep Bv | Werkwijze en inrichting voor het continu gieten van staal. |
ES2285148T3 (es) * | 2002-06-15 | 2007-11-16 | Solios Thermal Limited | Aparato de induccion electromagnetica y metodo de tratamiento de materiales fundidos. |
EP1913991A4 (de) * | 2005-08-10 | 2009-11-25 | Central Res Inst Elect | Reinigungsvorrichtung und reinigungsverfahren |
-
2013
- 2013-07-18 DE DE102013107685.8A patent/DE102013107685B3/de not_active Expired - Fee Related
-
2014
- 2014-07-17 WO PCT/EP2014/065429 patent/WO2015007861A1/de active Application Filing
- 2014-07-17 EP EP14741282.9A patent/EP3022325B1/de active Active
- 2014-07-17 PL PL14741282T patent/PL3022325T3/pl unknown
- 2014-07-17 CA CA2916477A patent/CA2916477A1/en not_active Abandoned
- 2014-07-17 JP JP2016526650A patent/JP2016530400A/ja active Pending
- 2014-07-17 CN CN201480040667.2A patent/CN105378120A/zh active Pending
- 2014-07-17 RU RU2016105398A patent/RU2639083C2/ru active
- 2014-07-17 US US14/903,725 patent/US20160160314A1/en not_active Abandoned
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4027722A (en) * | 1963-02-01 | 1977-06-07 | Airco, Inc. | Electron beam furnace |
DE1291760B (de) * | 1963-11-08 | 1969-04-03 | Suedwestfalen Ag Stahlwerke | Verfahren und Vorrichtung zum diskontinuierlichen und kontinuierlichen Vakuum-Schmelzen und -Giessen von Staehlen und stahlaehnlichen Legierungen (Superiegierungen) |
DE2118894A1 (de) * | 1970-04-21 | 1971-11-04 | Groupement Atomique Alsacienne Atiantique , Le Plessis Robinson (Frank reich) | Anordnung zum Behandeln und Fordern flussiger Metalle zum Zwecke ihres Ver gießens |
US5503655A (en) * | 1994-02-23 | 1996-04-02 | Orbit Technologies, Inc. | Low cost titanium production |
EP0796820A1 (de) * | 1996-03-19 | 1997-09-24 | Kawasaki Steel Corporation | Verfahren und Vorrichtung zur Raffinierung von Silicium |
Also Published As
Publication number | Publication date |
---|---|
RU2639083C2 (ru) | 2017-12-19 |
CN105378120A (zh) | 2016-03-02 |
DE102013107685B3 (de) | 2014-09-18 |
PL3022325T3 (pl) | 2018-04-30 |
EP3022325A1 (de) | 2016-05-25 |
RU2016105398A (ru) | 2017-08-23 |
EP3022325B1 (de) | 2017-10-04 |
JP2016530400A (ja) | 2016-09-29 |
CA2916477A1 (en) | 2015-01-22 |
US20160160314A1 (en) | 2016-06-09 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
DE69826940T2 (de) | Grader Herdofen zum Verfeinern von Titanium | |
DE1291760B (de) | Verfahren und Vorrichtung zum diskontinuierlichen und kontinuierlichen Vakuum-Schmelzen und -Giessen von Staehlen und stahlaehnlichen Legierungen (Superiegierungen) | |
DE3024697A1 (de) | Verfahren und vorrichtung zur herstellung legierter oder unlegierter reaktiver metalle | |
DE60024142T2 (de) | Giesssystem und giessverfahren für hochreinen und feinkörnigen metallguss | |
DE69704200T2 (de) | Weiterverarbeitung durch elektroschlackeumschmelzen gereinigter metalle | |
DE4207694A1 (de) | Vorrichtung fuer die herstellung von metallen und metall-legierungen hoher reinheit | |
EP3022325B1 (de) | Vorrichtung und verfahren zum sequentiellen schmelzen und raffinieren in einem kontinuierlichen verfahren | |
DE69003502T2 (de) | Vorrichtung zum Umschmelzen zur Gewinnung von Metallen. | |
DE112009001990T5 (de) | Verfahren zum Reinigen von Silizium | |
DE69015690T2 (de) | Verfahren zum Abtrennen von Einschlüssen in Metallen durch Umschmelzen. | |
EP0280765B1 (de) | Verfahren und Vorrichtung zur Herstellung von Gusskörpern aus druckbehandelten Schmelzen aus Stahllegierungen | |
DE3134429T1 (de) | Atmosphere controlled electric melting | |
EP3049543B1 (de) | Herstellung von hochwertigem mangan aus ferromangan mittels verdampfung in einer vakuuminduktionsanlage | |
DE1483647C3 (de) | Beheizung für einen Schmelzofen in einer Vorrichtung zum Herstellen von stickstofflegierten Gußblöcken | |
DE1433075A1 (de) | Vakuum-Schmelz- und-Giessverfahren und Vorrichtung zur Durchfuehrung desselben | |
EP0102479A2 (de) | Durchlauferhitzer für schmelzflüssige Metalle | |
DE205866C (de) | ||
EP3572539A1 (de) | Verfahren zur herstellung einer nbti-legierung | |
EP0512658B1 (de) | Anlage zur Behandlung flüssigen Stahls und Verfahren zum Betrieb einer derartigen Anlage | |
DE69004496T2 (de) | Verfahren und Anlage zur Trennung der Bestandteile einer Legierung. | |
DE3104003C2 (de) | ||
DE102014110251A1 (de) | Schmelzaggregat zum Einschmelzen von Gusswerkstoffen sowie ein Verfahren zur Herstellung einer Schmelze für das Gießen | |
AT230031B (de) | Vakuum-Schmelz- und -Gießverfahren und Vorrichtung zur Durchführung derselben | |
DE2501603B2 (de) | Einrichtung zur vakuumbehandlung fluessiger metalle | |
DE301959C (de) |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
121 | Ep: the epo has been informed by wipo that ep was designated in this application |
Ref document number: 14741282 Country of ref document: EP Kind code of ref document: A1 |
|
ENP | Entry into the national phase |
Ref document number: 2916477 Country of ref document: CA |
|
WWE | Wipo information: entry into national phase |
Ref document number: 14903725 Country of ref document: US |
|
ENP | Entry into the national phase |
Ref document number: 2016526650 Country of ref document: JP Kind code of ref document: A |
|
NENP | Non-entry into the national phase |
Ref country code: DE |
|
REEP | Request for entry into the european phase |
Ref document number: 2014741282 Country of ref document: EP |
|
WWE | Wipo information: entry into national phase |
Ref document number: 2014741282 Country of ref document: EP |
|
ENP | Entry into the national phase |
Ref document number: 2016105398 Country of ref document: RU Kind code of ref document: A |