WO2014074558A2 - Releasable polyester metal transfer film - Google Patents

Releasable polyester metal transfer film Download PDF

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Publication number
WO2014074558A2
WO2014074558A2 PCT/US2013/068655 US2013068655W WO2014074558A2 WO 2014074558 A2 WO2014074558 A2 WO 2014074558A2 US 2013068655 W US2013068655 W US 2013068655W WO 2014074558 A2 WO2014074558 A2 WO 2014074558A2
Authority
WO
WIPO (PCT)
Prior art keywords
layer
film
metal
polyester
release agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2013/068655
Other languages
English (en)
French (fr)
Other versions
WO2014074558A3 (en
WO2014074558A4 (en
Inventor
Jan Moritz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toray Plastics America Inc
Original Assignee
Toray Plastics America Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toray Plastics America Inc filed Critical Toray Plastics America Inc
Priority to EP13852454.1A priority Critical patent/EP2917910B1/en
Priority to JP2015541873A priority patent/JP6498122B2/ja
Priority to CA2891082A priority patent/CA2891082C/en
Publication of WO2014074558A2 publication Critical patent/WO2014074558A2/en
Publication of WO2014074558A3 publication Critical patent/WO2014074558A3/en
Publication of WO2014074558A4 publication Critical patent/WO2014074558A4/en
Priority to US14/586,785 priority patent/US10099462B2/en
Anticipated expiration legal-status Critical
Priority to US15/874,949 priority patent/US10596794B2/en
Ceased legal-status Critical Current

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Classifications

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    • B32B37/02—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by a sequence of laminating steps, e.g. by adding new layers at consecutive laminating stations
    • B32B37/025—Transfer laminating
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    • C08L67/03—Polyesters derived from dicarboxylic acids and dihydroxy compounds the dicarboxylic acids and dihydroxy compounds having the carboxyl- and the hydroxy groups directly linked to aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
    • C08L91/06—Waxes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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    • C09J7/22—Plastics; Metallised plastics
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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    • C09J7/25—Plastics; Metallised plastics based on macromolecular compounds obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds
    • C09J7/255—Polyesters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J7/00—Adhesives in the form of films or foils
    • C09J7/20—Adhesives in the form of films or foils characterised by their carriers
    • C09J7/29—Laminated material
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y10T428/24355—Continuous and nonuniform or irregular surface on layer or component [e.g., roofing, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/26—Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
    • Y10T428/263—Coating layer not in excess of 5 mils thick or equivalent
    • Y10T428/264—Up to 3 mils
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31678—Of metal
    • Y10T428/31681—Next to polyester, polyamide or polyimide [e.g., alkyd, glue, or nylon, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31786—Of polyester [e.g., alkyd, etc.]

Definitions

  • the present invention provides a single or multi-layered thermoplastic polyester carrier film for metal transfer that is free of a non-polyester release layer.
  • the composition of the thermoplastic polyester carrier film is preferably polyethylene terephthalate ("PET").
  • PET polyethylene terephthalate
  • At least one surface of the novel carrier film is intended for receiving, carrying and releasing a metal layer in the process of transferring the metal layer to a substrate, such as paperboard.
  • the metal receiving surface of the polyester carrier film has suitable metal adhesion and release properties that result from the incorporation of one or more release agents into the polyester carrier film metal-bearing layer.
  • this invention relates to biaxially oriented coextruded multilayer polyester films that can be readily fabricated, have ease of handling, and metal release properties on at least one outer layer surface, for use in metal transfer processes.
  • any standard method to fabricate co-extruded biaxially oriented multilayer films may be employed.
  • the term "polyester carrier film” refers to a film of polyester and release agent according to this invention prior to deposition of a layer of metal thereon.
  • transfer film refers to a composite of the polyester carrier film with a metal layer of metal deposited on an outer surface of the polyester carrier film. The primary intended use of the novel polyester carrier film is to receive, carry and transfer some or all of the metal from the metal layer onto a surface of a substrate.
  • metal adhesion can be controlled to a preselected value within a narrow range by adjusting the concentration of release agent in the polyester carrier film.
  • the metal adhesion can be controlled to within a range of ⁇ 10 g/in (3.9 g/cm) of a target metal adhesion value.
  • the actual amount of surfactant will be adjusted depending upon the thickness of the skin layer to provide a suitable metal adhesion value and should be determined by one of ordinary skill in the art without undue experimentation.
  • all or any selected parts of the metal deposited onto the surface of the base layer may be readily transferred to the substrate utilizing well known techniques.
  • the concentration of surfactant and optional wax release agent incorporated into the polymeric base layer can modify the metal adhesion of the carrier film to match the different specifications for diverse metal tranfer end use applications of metal transfer converters.
  • This invention further can provide metal adhesion with precision of narrow tolerance limits of the metal transfer converters' target.
  • a three layer PET film carrier film is prepared by coextruding an A/B/C composition and structure. Both skin layers A and C have the same calcium carbonate/aluminum oxide particle package for modifying the surface texture and a release agent of mixed
  • A/B/C A Layer Composition B Layer Composition C Layer Layer CompoThickness sition

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Laminated Bodies (AREA)
  • Decoration By Transfer Pictures (AREA)
  • Shaping By String And By Release Of Stress In Plastics And The Like (AREA)
  • Mechanical Engineering (AREA)
PCT/US2013/068655 2012-11-08 2013-11-06 Releasable polyester metal transfer film Ceased WO2014074558A2 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP13852454.1A EP2917910B1 (en) 2012-11-08 2013-11-06 Releasable polyester metal transfer film
JP2015541873A JP6498122B2 (ja) 2012-11-08 2013-11-06 ポリエステル製の剥離可能な金属の転写フィルム
CA2891082A CA2891082C (en) 2012-11-08 2013-11-06 Releasable polyester metal transfer film
US14/586,785 US10099462B2 (en) 2013-06-28 2014-12-30 Releasable polyester high gloss metal transfer film
US15/874,949 US10596794B2 (en) 2012-11-08 2018-01-19 Releasable polyester high gloss metal transfer film method

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201261723967P 2012-11-08 2012-11-08
US61/723,967 2012-11-08
US13/930,395 US9630385B2 (en) 2012-11-08 2013-06-28 Releasable polyester metal transfer film
US13/930,395 2013-06-28

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
US13/930,395 Continuation-In-Part US9630385B2 (en) 2012-11-08 2013-06-28 Releasable polyester metal transfer film

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US14/586,785 Continuation US10099462B2 (en) 2012-11-08 2014-12-30 Releasable polyester high gloss metal transfer film

Publications (3)

Publication Number Publication Date
WO2014074558A2 true WO2014074558A2 (en) 2014-05-15
WO2014074558A3 WO2014074558A3 (en) 2014-07-17
WO2014074558A4 WO2014074558A4 (en) 2014-08-28

Family

ID=50621271

Family Applications (1)

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PCT/US2013/068655 Ceased WO2014074558A2 (en) 2012-11-08 2013-11-06 Releasable polyester metal transfer film

Country Status (5)

Country Link
US (2) US9630385B2 (cg-RX-API-DMAC7.html)
EP (2) EP3332963A1 (cg-RX-API-DMAC7.html)
JP (1) JP6498122B2 (cg-RX-API-DMAC7.html)
CA (1) CA2891082C (cg-RX-API-DMAC7.html)
WO (1) WO2014074558A2 (cg-RX-API-DMAC7.html)

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US10183471B2 (en) * 2016-02-22 2019-01-22 Toray Plastics (America), Inc. Metal transfer film and method of using same
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WO2014074558A4 (en) 2014-08-28
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EP3332963A1 (en) 2018-06-13
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EP2917910A2 (en) 2015-09-16
EP2917910B1 (en) 2019-10-30
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US10596794B2 (en) 2020-03-24

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