WO2014065553A1 - Procédé de purification de 1,4-diaminobutane, 1,4-diaminobutane purifié selon ledit procédé et polyamide préparé à partir de celui-ci - Google Patents

Procédé de purification de 1,4-diaminobutane, 1,4-diaminobutane purifié selon ledit procédé et polyamide préparé à partir de celui-ci Download PDF

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Publication number
WO2014065553A1
WO2014065553A1 PCT/KR2013/009399 KR2013009399W WO2014065553A1 WO 2014065553 A1 WO2014065553 A1 WO 2014065553A1 KR 2013009399 W KR2013009399 W KR 2013009399W WO 2014065553 A1 WO2014065553 A1 WO 2014065553A1
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WO
WIPO (PCT)
Prior art keywords
diaminobutane
fermentation broth
composition
distillation
concentrating
Prior art date
Application number
PCT/KR2013/009399
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English (en)
Korean (ko)
Inventor
곽원식
서용범
이종호
이인성
무라타히데키
Original Assignee
씨제이제일제당 (주)
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by 씨제이제일제당 (주) filed Critical 씨제이제일제당 (주)
Priority to US14/437,172 priority Critical patent/US9376370B2/en
Priority to RU2015114079A priority patent/RU2616002C2/ru
Priority to AU2013335491A priority patent/AU2013335491B2/en
Priority to ES13849534T priority patent/ES2797379T3/es
Priority to EP13849534.6A priority patent/EP2910543B1/fr
Priority to BR112015009055-9A priority patent/BR112015009055B1/pt
Priority to CN201380062423.XA priority patent/CN104822652B/zh
Priority to JP2015536723A priority patent/JP6050895B2/ja
Priority to IN3205DEN2015 priority patent/IN2015DN03205A/en
Publication of WO2014065553A1 publication Critical patent/WO2014065553A1/fr

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/84—Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C211/09—Diamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/04—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/26—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00—Preparation of nitrogen-containing organic compounds
    • C12P13/001—Amines; Imines
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00—Preparation of nitrogen-containing organic compounds

Definitions

  • the residue adjusted to pH 13.5 was introduced into a 5L double jacket reactor.
  • the upper part of the double jacket reactor is connected to the 10-stage part from the bottom of a total of 30-stage distillation column (manufactured by Aceglass) in the form of a tray.
  • the double jacketed reactor further concentrated the residue at a vapor temperature of 50-90 ° C. and a pressure of 80 mmHg.
  • the double jacket reactor was initially maintained at a vapor temperature of 47 ° C. due to evaporation of water, and then the vapor temperature was increased to 90 ° C. as 1,4-diaminobutane was evaporated. Steam containing 1,4-diaminobutane as a main component was introduced into a 30 stage distillation column.
  • the residue adjusted to pH 13.5 was introduced into a 5L double jacket reactor.
  • the upper portion of the double jacket reactor is connected to the 10-stage portion at the bottom of a total of 30 stages of distillation tower (manufactured by Aceglass) in the form of a tray.
  • the double jacketed reactor further concentrated the residue at a vapor temperature of 50-90 ° C. and a pressure of 80 mmHg.
  • the double jacket reactor was initially maintained at a vapor temperature of 47 ° C. due to evaporation of water, and then the vapor temperature was increased to 90 ° C. as 1,4-diaminobutane was evaporated. Steam containing 1,4-diaminobutane as a main component was introduced into a 30 stage distillation column.

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyamides (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

La présente invention concerne un procédé de purification du 1,4-diaminobutane, du 1,4-diaminobutane purifié selon ledit procédé, et un polyamide préparé en utilisant le 1,4-diaminobutane, le procédé de purification du 1,4-diaminobutane comprenant les étapes consistant à : concentrer une solution de fermentation contenant au moins l'un parmi le 1,4-diaminobutane et l'un de ses sels ; préparer une composition basique de pH supérieur ou égal à 12 par addition d'une base au produit concentré de la solution de fermentation ; et collecter le 1,4-diaminobutane à partir de la composition basique.
PCT/KR2013/009399 2012-10-22 2013-10-22 Procédé de purification de 1,4-diaminobutane, 1,4-diaminobutane purifié selon ledit procédé et polyamide préparé à partir de celui-ci WO2014065553A1 (fr)

Priority Applications (9)

Application Number Priority Date Filing Date Title
US14/437,172 US9376370B2 (en) 2012-10-22 2013-10-22 Method for purifying 1,4-diaminobutane, 1,4-diaminobutane purified by said method, and polyamide prepared therefrom
RU2015114079A RU2616002C2 (ru) 2012-10-22 2013-10-22 Способ очистки 1,4-диаминобутана, очищенный указанным способом 1,4-диаминобутан и полученный из него полиамид
AU2013335491A AU2013335491B2 (en) 2012-10-22 2013-10-22 Method for purifying 1,4-diaminobutane, 1,4-diaminobutane purified by said method, and polyamide prepared therefrom
ES13849534T ES2797379T3 (es) 2012-10-22 2013-10-22 Procedimiento de purificación de 1,4-diaminobutano, 1,4-diaminobutano purificado por dicho procedimiento, y poliamida preparada a partir de este
EP13849534.6A EP2910543B1 (fr) 2012-10-22 2013-10-22 Procédé de purification de 1,4-diaminobutane, 1,4-diaminobutane purifié selon ledit procédé et polyamide préparé à partir de celui-ci
BR112015009055-9A BR112015009055B1 (pt) 2012-10-22 2013-10-22 método para purificar 1,4-diaminobutano, e 1,4-diaminobutano
CN201380062423.XA CN104822652B (zh) 2012-10-22 2013-10-22 纯化1,4‑二氨基丁烷的方法、由所述方法纯化的1,4‑二氨基丁烷和由其制备的聚酰胺
JP2015536723A JP6050895B2 (ja) 2012-10-22 2013-10-22 １，４−ジアミノブタンの精製方法、該方法によって精製された１，４−ジアミノブタン、及びそれから製造されるポリアミド
IN3205DEN2015 IN2015DN03205A (fr) 2012-10-22 2013-10-22

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020120117501A KR20140052189A (ko) 2012-10-22 2012-10-22 1,4-디아미노부탄의 정제방법, 상기 방법으로 정제된 1,4-디아미노부탄 및 이로부터 제조되는 폴리아미드
KR10-2012-0117501 2012-10-22

Publications (1)

Publication Number Publication Date
WO2014065553A1 true WO2014065553A1 (fr) 2014-05-01

Family

ID=50544882

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2013/009399 WO2014065553A1 (fr) 2012-10-22 2013-10-22 Procédé de purification de 1,4-diaminobutane, 1,4-diaminobutane purifié selon ledit procédé et polyamide préparé à partir de celui-ci

Country Status (12)

Country Link
US (1) US9376370B2 (fr)
EP (1) EP2910543B1 (fr)
JP (1) JP6050895B2 (fr)
KR (1) KR20140052189A (fr)
CN (1) CN104822652B (fr)
AU (1) AU2013335491B2 (fr)
BR (1) BR112015009055B1 (fr)
ES (1) ES2797379T3 (fr)
IN (1) IN2015DN03205A (fr)
MY (1) MY175861A (fr)
RU (1) RU2616002C2 (fr)
WO (1) WO2014065553A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10450262B2 (en) 2015-05-08 2019-10-22 Cj Cheiljedang Corporation Method for purifying 1,4-diaminobutane

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020011725A1 (fr) * 2018-07-10 2020-01-16 Givaudan Sa Améliorations dans ou relatives à des composés organiques
KR102352784B1 (ko) * 2020-03-19 2022-01-18 씨제이제일제당 주식회사 탄산 함유 디아미노알칸 용액의 분리막 분리 공정
EP4151619A1 (fr) * 2021-09-20 2023-03-22 Covestro Deutschland AG Procédé pour l'élimination de l'eau et le transport de diamines aliphatiques

Citations (4)

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Publication number Priority date Publication date Assignee Title
KR20080108082A (ko) * 2006-01-11 2008-12-11 디에스엠 아이피 어셋츠 비.브이. 유기 아민의 단리 방법
KR20090107920A (ko) 2008-04-10 2009-10-14 한국과학기술원 퓨트레신 고생성능을 가지는 변이 미생물 및 이를 이용한 퓨트레신의 제조방법
KR20100117084A (ko) * 2008-01-23 2010-11-02 바스프 에스이 발효에 의한 1,5-디아미노펜탄의 제조 방법
KR20100133366A (ko) * 2008-03-12 2010-12-21 도레이 카부시키가이샤 디아민 및 폴리아미드의 제조 방법

Family Cites Families (4)

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Publication number Priority date Publication date Assignee Title
EP2949755B1 (fr) * 2004-07-15 2018-03-28 DSM IP Assets B.V. Synthèse biochimique de 1,4-butanediamine
AU2009234625B2 (en) * 2008-04-10 2012-07-19 Korea Advanced Institute Of Science And Technology Mutant microorganisms having high ability to produce putrescine and method for producing putrescine using the same
KR101286158B1 (ko) * 2011-08-24 2013-07-15 씨제이제일제당 (주) 발효액에서 1,4-디아미노부탄의 분리 및 정제하는 방법
MY170936A (en) * 2011-10-14 2019-09-19 Toray Industries Process for producing 2,3-butanediol

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20080108082A (ko) * 2006-01-11 2008-12-11 디에스엠 아이피 어셋츠 비.브이. 유기 아민의 단리 방법
KR20100117084A (ko) * 2008-01-23 2010-11-02 바스프 에스이 발효에 의한 1,5-디아미노펜탄의 제조 방법
KR20100133366A (ko) * 2008-03-12 2010-12-21 도레이 카부시키가이샤 디아민 및 폴리아미드의 제조 방법
KR20090107920A (ko) 2008-04-10 2009-10-14 한국과학기술원 퓨트레신 고생성능을 가지는 변이 미생물 및 이를 이용한 퓨트레신의 제조방법

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10450262B2 (en) 2015-05-08 2019-10-22 Cj Cheiljedang Corporation Method for purifying 1,4-diaminobutane

Also Published As

Publication number Publication date
AU2013335491B2 (en) 2016-04-28
BR112015009055B1 (pt) 2020-12-08
RU2616002C2 (ru) 2017-04-12
MY175861A (en) 2020-07-14
KR20140052189A (ko) 2014-05-07
JP6050895B2 (ja) 2016-12-21
IN2015DN03205A (fr) 2015-10-02
RU2015114079A (ru) 2016-12-10
AU2013335491A1 (en) 2015-04-30
US20150284315A1 (en) 2015-10-08
EP2910543A1 (fr) 2015-08-26
US9376370B2 (en) 2016-06-28
EP2910543B1 (fr) 2020-04-15
EP2910543A4 (fr) 2016-06-08
ES2797379T3 (es) 2020-12-02
CN104822652A (zh) 2015-08-05
JP2015533830A (ja) 2015-11-26
CN104822652B (zh) 2017-07-14
BR112015009055A2 (pt) 2017-07-04

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