WO2014035088A1 - 산성수 전해조 및 그 산성수의 이용방법 - Google Patents
산성수 전해조 및 그 산성수의 이용방법 Download PDFInfo
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- WO2014035088A1 WO2014035088A1 PCT/KR2013/007418 KR2013007418W WO2014035088A1 WO 2014035088 A1 WO2014035088 A1 WO 2014035088A1 KR 2013007418 W KR2013007418 W KR 2013007418W WO 2014035088 A1 WO2014035088 A1 WO 2014035088A1
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
- C25B9/17—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
- C25B9/19—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms
- C25B9/23—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms comprising ion-exchange membranes in or on which electrode material is embedded
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/46—Treatment of water, waste water, or sewage by electrochemical methods
- C02F1/461—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/46—Treatment of water, waste water, or sewage by electrochemical methods
- C02F1/461—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
- C02F1/46104—Devices therefor; Their operating or servicing
- C02F1/4618—Devices therefor; Their operating or servicing for producing "ionised" acidic or basic water
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/02—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form
- C25B11/03—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form perforated or foraminous
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/46—Treatment of water, waste water, or sewage by electrochemical methods
- C02F1/461—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
- C02F1/46104—Devices therefor; Their operating or servicing
- C02F1/46109—Electrodes
- C02F2001/46152—Electrodes characterised by the shape or form
- C02F2001/46157—Perforated or foraminous electrodes
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/46—Treatment of water, waste water, or sewage by electrochemical methods
- C02F1/461—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
- C02F1/46104—Devices therefor; Their operating or servicing
- C02F1/4618—Devices therefor; Their operating or servicing for producing "ionised" acidic or basic water
- C02F2001/46185—Devices therefor; Their operating or servicing for producing "ionised" acidic or basic water only anodic or acidic water, e.g. for oxidizing or sterilizing
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2201/00—Apparatus for treatment of water, waste water or sewage
- C02F2201/46—Apparatus for electrochemical processes
- C02F2201/461—Electrolysis apparatus
- C02F2201/46105—Details relating to the electrolytic devices
- C02F2201/46115—Electrolytic cell with membranes or diaphragms
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2201/00—Apparatus for treatment of water, waste water or sewage
- C02F2201/46—Apparatus for electrochemical processes
- C02F2201/461—Electrolysis apparatus
- C02F2201/46105—Details relating to the electrolytic devices
- C02F2201/4618—Supplying or removing reactants or electrolyte
Definitions
- FIG. 1 is a cross-sectional view schematically showing the configuration of an acidic electrolytic cell according to a first embodiment of the present invention.
- the acidic water obtained in the cathode side that is, the filling chamber 110b described above, was tested as follows to obtain a change in physical properties according to the change of the gap W2. Was performed.
- Raw water Water (conductivity 10uS / cm or less, pH7.0, ORP + 230mV, temperature 25.5 °C)
- the electrolyzed water obtained by the present invention is generally acidic, and in particular, the narrower the gap W2 is, the stronger the acidity becomes, and the redox potential difference (ORP) is also the gap (W2). It can be seen that as the size increases. As a result, it can be seen that the electrolytic water thus obtained is acidic reduced water.
- mice ingested with hydrogen water 1.0 ppm of hydrogen obtained from the cathode side of the acidic water electrolytic cell of the present invention.
- Plasma total antioxidant activity was measured using a kit for measuring total antioxdant status of Randox Inc. (U. K.). Immobility time was measured during 6 minutes of forced swimming to investigate the effects of stamina enhancement. This was done by filling a circular cylinder (height: 25cm, diameter: 10cm) with 10cm depth of water at 23 ⁇ 25 °C and measuring a floating time of 4 minutes before termination. It was made.
- the acidic water electrolytic cell according to the second embodiment of the present invention can generate a large potential difference proportionally by the amount of ions stored in the ion tank 400, thereby increasing the acidification and reducing power.
- the polarity of the electrode is changed and applied.
- the same components as those in the first embodiment are denoted by the same reference numerals, and detailed description thereof will be omitted.
- Example 1 acidic and cyclic acidic water can be obtained.
- Example 3 acidic and highly oxidizable acidic water can be obtained.
- the ion tank 400 is further configured in the housing 100 of the third embodiment.
- the same components as those in the third embodiment are denoted by the same reference numerals, and detailed description thereof will be omitted.
- the acidic water electrolytic cell according to the fourth embodiment of the present invention is capable of generating a potential difference proportionally larger by the amount of ions stored in the ion tank 400, so that acidic water having a high acidification can be obtained. .
- the acid reduced water obtained from the electrolytic cell according to the present invention is characterized in that it has an acidity (pH 4 to pH 6.9) and reducing power (ORP-100 kPa to -650 kPa) at the cathode side by electrolyzing raw water having conductivity of 50 uS / cm or less. . And, the acidic reduced water is characterized in that the dissolved hydrogen concentration (DH) is 200ppb ⁇ 1500ppb.
- the acidic reduced water according to the present invention can be used as raw material water, drinking water or beverage water, microbial growth and cell growth drinking water, growth promotion, and browning prevention water such as vegetables and fruits and cosmetic raw water.
- the acidic oxidized water obtained from the electrolytic cell according to the present invention electrolyzes raw water having a conductivity of 50 uS / cm or less and has an oxidizing power (ORP +700 kPa to +1,200 kPa) while being acidic (pH 3.5 to pH 6.0) at the anode side.
- Such acidic reduced water can be used as sterilized water, microbial growth and drinking water for cell proliferation, growth promotion, and browning prevention water such as vegetables or fruits or cosmetic raw water.
Abstract
Description
간극 / 물성 | pH1) | ORP2) | DH3) |
2㎜ | 4.82 | -653㎷ | 1.43ppm |
5㎜ | 5.05 | -620 ㎷ | 1.21ppm |
10㎜ | 5.37 | -586 ㎷ | 0.97ppm |
20㎜ | 5.83 | -534 ㎷ | 0.81ppm |
30㎜ | 6.20 | -508 ㎷ | 0.77ppm |
40㎜ | 6.42 | -472 ㎷ | 0.68ppm |
50㎜ | 6.75 | -426 ㎷ | 0.52ppm |
60㎜ | 6..81 | -398 ㎷ | 0.43ppm |
70㎜ | 6.98 | -327 ㎷ | 0.32ppm |
1) pH : 수소이온 농도 지수(Potential of Hydrogen)2) ORP : 산화환원 전위차(Oxidation Redution Potential)3) DH : 용존수소농도(Dissolved Hydrogen) |
전류(A) | 전압(V) | ORP1)(mV) | pH2) |
0,5 | 6.0 | +995 | 4.80 |
1.0 | 8.5 | +1041 | 4.46 |
1.5 | 10.5 | +1952 | 4.41 |
2.0 | 12.0 | +1060 | 4.39 |
2.5 | 12.9 | +1067 | 4.34 |
3.0 | 14.1 | +1073 | 4.28 |
1) ORP : 산화환원 전위차(Oxidation Redution Potential)2) pH : 수소이온 농도 지수(Potential of Hydrogen) |
구분 | 비교 트롤록스 (relative Trolox) 농도[nmol/ml 혈장(plasma)] |
대조군(비교예) | 1.24±0.06 |
수소수(실시예) | 1.46±0.13* |
[표 3] 수소수의 투여가 생쥐 혈장의 총 산화력에 미치는 영향1의 측정결과1평균치±SEM, n=10.2수용성(water-soluble) 비타민E 유사체(analogue).*P<0.05, 대조군과 비교 |
비교예 | 실시예(수소수군) | |
섭취 전 | 190±13 | 193±11 |
섭취 후 | 224±8 | 195±7* |
표4 수소수의 섭취가 생쥐의 강제 수영 시험에서 부동시간(초)에 미치는 영향1 1평균치±SEM, n=10.*P<0.05, 대조군과 비교. |
대조군 | 수소수군 | |
혈액 요소태 질소(blood urea nitrogen, mg/dl) | 22.0±0.9 | 18.8±0.6* |
크레아틴 카이네이즈(creatin kinase,mg/dl)) | 0.36±0.03 | 0.28±0.02* |
유산 탈수소효소(lactic dehydrogrnase, U/I) | 988±167 | 896±171 |
포도당(mg/dl) | 219±13 | 238±14 |
총 단백질(total protein, g/dl) | 4.3±0.1 | 5.1±0.1* |
[표 5]수소수의 섭취가 생쥐의 혈액 생화학 지표에 미치는 영향1 1평균치±SEM, n=10.*P<0.05, 대조군과비교 |
Claims (13)
- 적어도 하나의 이온 교환막(111)을 중심으로 분리된 적어도 2개의 충진실(110a,110b)이 구비되고, 각 충진실(110a,110b)에는 각각 입수구(112a,113a) 및 출수구(112b,113b)가 형성된 하우징(100); 상기 충진실(110a)에 설치되는 제1전극(200); 나머지 충진실(110b) 내에 이온 교환막(111)과 근접하게 설치되며 제1전극(200)과 다른 극성을 갖는 제2전극(300); 및 상기 각 충진실(110b)에, 제2전극(300)과 동일 극성을 가지면서 이 제2전극(300)과 미리 정해진 간격만큼 이격되게 설치되는 제3전극(300');을 포함하고,상기 제2전극(300) 및 제3전극(300')은 서로 연결되어 동시에 전원이 인가되도록 구성된 것을 특징으로 하는 산성수 전해조.
- 제 1 항에 있어서,상기 이온 교환막(111)과 상기 제1전극(200)은 0.1~2.0㎜의 간극(W1)만큼 이격되게 설치하여 원수가 통과할 수 있도록 그 사이를 충진공간으로 이용하는 것을 특징으로 하는 산성수 전해조.
- 제 1 항 또는 제 2 항에 있어서,상기 제2전극(300)과 상기 제3전극(300')은 0.1~100.0㎜의 간극(W2)만큼 이격되게 설치하여 원수가 통과할 수 있도록 그 사이를 충진공간으로 이용하는 것을 특징으로 하는 산성수 전해조.
- 제 3 항에 있어서,제1전극(200)이 설치된 충진실(110a)의 입수구(112a)와 출수구(112b) 사이에는,이온탱크(400)가 구비된 것을 특징으로 하는 산성수 전해조.
- 제 4 항에 있어서,상기 이온 교환막(111)은 불소계 캐치온 교환막인 것을 특징으로 하는 산성수 전해조.
- 제 5 항에 있어서,상기 제1 내지 제3전극(200,300,300')은 타공성 백금전극 또는 메쉬 백금 전극인 것을 특징으로 하는 산성수 전해조.
- 제 1 항에 있어서,상기 이온 교환막(111)에는 제1전극(200)과 마주보는 면의 일부 면적에 대하여 이 제1전극(200)과 동일 극성을 갖는 메쉬 전극(114)이 더 구비되어 있는 것을 특징으로 하는 산성수 전해조.
- 제 7 항에 있어서,상기 메쉬 전극(114)은 이온 교환막(111)의 한쪽 표면의 전체 크기에 대하여 30~80% 크기로 형성된 것을 특징으로 하는 산성수 전해조.
- 제 6 항에 있어서,상기 전해조로부터 전해된 물은 용존수소농도(DH)가 200ppb~1,500ppb인 것을 특징으로 하는 산성수 전해조.
- 제 9 항에 의한 전해조에 전도도가 50uS/cm 이하인 원수를 전해하여 음극측에서 산성(pH4~pH6.9)이면서 환원력(ORP -100㎷~-650㎷)을 갖은 산성의 환원수를 얻는 것을 특징으로 하는 산성수 전해조.
- 제 10 항에 있어서,상기 산성의 환원수는 황산화제 원료수·음용수나 음료수의 원료수·미생물증식 및 세포증식용 식용수·성장촉진 및 야채나 과일 등의 갈변방지수 또는 화장품 원료수로 이용하는 이용방법.
- 제 9 항에 의한 전해조에 전도도가 50uS/cm이하인 원수을 전해하여 양극측에서 산성(pH3.5~pH6.0)이면서 산화력(ORP +700㎷~+1,200㎷)을 갖은 산성의 산화수를 얻는 것을 특징으로 하는 산성수 전해조.
- 제 12 항에 있어서,상기 산성의 산화수는 살균수·미생물증식 및 세포증식용 식용수·성장촉진 및 야채나 과일 등의 갈변방지수 또는 화장품 원료수로 이용하는 이용방법.
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
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US14/382,841 US9624117B2 (en) | 2012-08-27 | 2013-08-19 | Electrolysis bath for acidic water and method for using the acidic water |
RU2014130407/04A RU2602234C2 (ru) | 2012-08-27 | 2013-08-19 | Электролизная ванна для кислой воды и способ использования кислой воды |
JP2014540987A JP5835599B2 (ja) | 2012-08-27 | 2013-08-19 | 酸性水電解槽及びその酸性水の利用方法 |
CN201380003623.8A CN104024480B (zh) | 2012-08-27 | 2013-08-19 | 酸性水电解槽及其酸性水的利用方法 |
SG11201404539PA SG11201404539PA (en) | 2012-08-27 | 2013-08-19 | Electrolytic bath for manufacturing acidic water and use of the acidic water |
DE112013000327.9T DE112013000327B4 (de) | 2012-08-27 | 2013-08-19 | Elektrolysebad zur Herstellung von saurem Wasser und dessen Verwendung |
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KR20120093589 | 2012-08-27 | ||
KR10-2012-0093589 | 2012-08-27 | ||
KR10-2013-0062744 | 2013-05-31 | ||
KR1020130062744A KR20140027866A (ko) | 2012-08-27 | 2013-05-31 | 산성수 전해조 및 그 산성수의 이용방법 |
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JP (1) | JP5835599B2 (ko) |
KR (1) | KR20140027866A (ko) |
CN (1) | CN104024480B (ko) |
DE (1) | DE112013000327B4 (ko) |
RU (1) | RU2602234C2 (ko) |
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CN105198045A (zh) * | 2014-06-18 | 2015-12-30 | Mag技术株式会社 | 酸性水电解槽及其酸性水的使用方法 |
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KR101663126B1 (ko) * | 2015-03-31 | 2016-10-10 | 주식회사 심스바이오닉스 | 산성수 전해조 |
KR20170024618A (ko) | 2015-08-25 | 2017-03-08 | 주식회사 심스바이오닉스 | 산성수 전해 장치 |
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JP2017070920A (ja) * | 2015-10-08 | 2017-04-13 | モレックス エルエルシー | 電解水の製造装置 |
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JP7103626B2 (ja) * | 2018-02-22 | 2022-07-20 | 国立大学法人弘前大学 | リチウム回収装置およびリチウム回収方法 |
KR102195894B1 (ko) | 2018-08-30 | 2020-12-29 | 한양대학교 산학협력단 | 하이브리드 아이템 추천 방법 및 장치 |
JP2021079315A (ja) * | 2019-11-15 | 2021-05-27 | 株式会社東芝 | 水処理装置及び水処理方法 |
CN116969554B (zh) * | 2023-09-22 | 2024-01-12 | 康亦健(集团)有限公司 | 一种电解还原制水机 |
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- 2013-08-19 DE DE112013000327.9T patent/DE112013000327B4/de active Active
- 2013-08-19 WO PCT/KR2013/007418 patent/WO2014035088A1/ko active Application Filing
- 2013-08-19 CN CN201380003623.8A patent/CN104024480B/zh active Active
- 2013-08-19 JP JP2014540987A patent/JP5835599B2/ja active Active
- 2013-08-19 US US14/382,841 patent/US9624117B2/en active Active
- 2013-08-19 RU RU2014130407/04A patent/RU2602234C2/ru active
- 2013-08-19 SG SG11201404539PA patent/SG11201404539PA/en unknown
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CN104024480A (zh) | 2014-09-03 |
RU2014130407A (ru) | 2016-10-20 |
US9624117B2 (en) | 2017-04-18 |
US20150021171A1 (en) | 2015-01-22 |
SG11201404539PA (en) | 2014-10-30 |
KR20140027866A (ko) | 2014-03-07 |
JP5835599B2 (ja) | 2015-12-24 |
CN104024480B (zh) | 2017-08-04 |
RU2602234C2 (ru) | 2016-11-10 |
JP2014532561A (ja) | 2014-12-08 |
DE112013000327B4 (de) | 2023-12-07 |
DE112013000327T5 (de) | 2014-08-21 |
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