WO2010077039A2 - 유리 요오드 저감 폴리아릴렌 설파이드 제조 방법 - Google Patents

유리 요오드 저감 폴리아릴렌 설파이드 제조 방법 Download PDF

Info

Publication number
WO2010077039A2
WO2010077039A2 PCT/KR2009/007831 KR2009007831W WO2010077039A2 WO 2010077039 A2 WO2010077039 A2 WO 2010077039A2 KR 2009007831 W KR2009007831 W KR 2009007831W WO 2010077039 A2 WO2010077039 A2 WO 2010077039A2
Authority
WO
WIPO (PCT)
Prior art keywords
polyarylene sulphide
production method
free iodine
sulphide
polyarylene
Prior art date
Application number
PCT/KR2009/007831
Other languages
English (en)
French (fr)
Other versions
WO2010077039A3 (ko
Inventor
신용준
김성기
임재봉
조준상
차일훈
Original Assignee
에스케이케미칼주식회사
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 에스케이케미칼주식회사 filed Critical 에스케이케미칼주식회사
Priority to CN2009801577117A priority Critical patent/CN102341434A/zh
Priority to ES09836360.9T priority patent/ES2601363T3/es
Priority to US13/142,932 priority patent/US9163119B2/en
Priority to EP09836360.9A priority patent/EP2383308B1/en
Priority to JP2011543437A priority patent/JP5702731B2/ja
Publication of WO2010077039A2 publication Critical patent/WO2010077039A2/ko
Publication of WO2010077039A3 publication Critical patent/WO2010077039A3/ko
Priority to US14/831,360 priority patent/US20150353687A1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/14—Polysulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/14—Polysulfides
    • C08G75/16—Polysulfides by polycondensation of organic compounds with inorganic polysulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/0209—Polyarylenethioethers derived from monomers containing one aromatic ring
    • C08G75/0213—Polyarylenethioethers derived from monomers containing one aromatic ring containing elements other than carbon, hydrogen or sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C08G75/0263—Preparatory processes using elemental sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C08G75/0268—Preparatory processes using disulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/04—Polythioethers from mercapto compounds or metallic derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/06—Polythioethers from cyclic thioethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)

Abstract

본 발명은 유리 요오드 함량이 저감된 폴리아릴렌 설파이드(polyarylene sulfide)를 제조하는 방법에 관한 것으로서, 구체적으로 디요오드 방향족 화합물과 황 화합물을 포함하는 반응물을 중합 반응하여, 폴리아릴렌 설파이드를 중합하는 단계; 및 상기에서 중합된 폴리아릴렌 설파이드를 100 내지 260°C에서 히트-세팅(heat setting)하는 단계를 포함한다. 본 발명에 따른 제조방법은 폴리아릴렌 설파이드 내의 유리 요오드 함량을 효과적으로 낮추어 후공정 설비의 부식을 방지할 수 있고, 제조된 폴리아릴렌 설파이드의 열 안정성 등의 물성도 개선하여, 폴리아릴렌 설파이드의 제조에 관한 산업 분야에 유용하게 응용될 수 있다.
PCT/KR2009/007831 2008-12-31 2009-12-28 유리 요오드 저감 폴리아릴렌 설파이드 제조 방법 WO2010077039A2 (ko)

Priority Applications (6)

Application Number Priority Date Filing Date Title
CN2009801577117A CN102341434A (zh) 2008-12-31 2009-12-28 制备自由碘含量降低的聚芳撑硫醚的方法
ES09836360.9T ES2601363T3 (es) 2008-12-31 2009-12-28 Procedimiento para la preparación de sulfuros de poliarileno con un contenido reducido de yodo libre
US13/142,932 US9163119B2 (en) 2008-12-31 2009-12-28 Method for preparing polyarylene sulfide with reduced free iodine content
EP09836360.9A EP2383308B1 (en) 2008-12-31 2009-12-28 Method for preparing polyarylene sulfide with reduced free iodine content
JP2011543437A JP5702731B2 (ja) 2008-12-31 2009-12-28 遊離ヨウ素が低減されたポリアリーレンスルフィドの製造方法
US14/831,360 US20150353687A1 (en) 2008-12-31 2015-08-20 Method for preparing polyarylene sulfide with reduced free iodine content

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020080137680A KR101554010B1 (ko) 2008-12-31 2008-12-31 유리 요오드 저감 폴리아릴렌 설파이드의 제조 방법
KR10-2008-0137680 2008-12-31

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US13/142,932 A-371-Of-International US9163119B2 (en) 2008-12-31 2009-12-28 Method for preparing polyarylene sulfide with reduced free iodine content
US14/831,360 Division US20150353687A1 (en) 2008-12-31 2015-08-20 Method for preparing polyarylene sulfide with reduced free iodine content

Publications (2)

Publication Number Publication Date
WO2010077039A2 true WO2010077039A2 (ko) 2010-07-08
WO2010077039A3 WO2010077039A3 (ko) 2010-10-14

Family

ID=42310361

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2009/007831 WO2010077039A2 (ko) 2008-12-31 2009-12-28 유리 요오드 저감 폴리아릴렌 설파이드 제조 방법

Country Status (8)

Country Link
US (2) US9163119B2 (ko)
EP (1) EP2383308B1 (ko)
JP (1) JP5702731B2 (ko)
KR (1) KR101554010B1 (ko)
CN (2) CN104861163A (ko)
ES (1) ES2601363T3 (ko)
HK (1) HK1209144A1 (ko)
WO (1) WO2010077039A2 (ko)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109096761A (zh) * 2013-10-01 2018-12-28 Dic株式会社 聚芳硫醚树脂组合物及其成形品、以及电动汽车部件

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101554010B1 (ko) * 2008-12-31 2015-09-18 에스케이케미칼 주식회사 유리 요오드 저감 폴리아릴렌 설파이드의 제조 방법
KR101457745B1 (ko) * 2011-08-19 2014-11-03 주식회사 엘지화학 폴리페닐렌 설파이드 제조 방법 및 이로부터 제조된 폴리페닐렌 설파이드
WO2013147141A1 (ja) 2012-03-30 2013-10-03 株式会社クレハ 粒状ポリアリーレンスルフィド及びその製造方法
WO2014025190A1 (ko) * 2012-08-07 2014-02-13 에스케이케미칼주식회사 폴리아릴렌 설파이드 수지 및 그의 제조 방법
CN104640929B (zh) * 2012-09-19 2018-01-23 Sk化学株式会社 聚亚芳基硫醚树脂组合物及成形的物品
EP4029900A1 (en) * 2013-03-25 2022-07-20 DIC Corporation Method for producing polyarylene sulfide resin and polyarylene sulfide resin composition
KR20160042939A (ko) * 2013-08-09 2016-04-20 디아이씨 가부시끼가이샤 폴리아릴렌설피드 수지 조성물 및 그 성형품
JP6210341B2 (ja) * 2013-08-30 2017-10-11 Dic株式会社 多層成形体及びそれを用いた燃料用部品
JP6074105B2 (ja) * 2014-02-24 2017-02-01 帝人株式会社 樹脂組成物
CN108473766A (zh) * 2015-11-23 2018-08-31 Sk化学株式会社 聚亚芳基硫醚树脂组合物和模制物品
US10822457B2 (en) * 2015-11-23 2020-11-03 Sk Chemicals Co., Ltd. Polyarylene sulfide resin and preparation method thereof
KR102492258B1 (ko) * 2016-04-26 2023-01-26 에이치디씨폴리올 주식회사 내가수분해성이 우수한 폴리아릴렌 설파이드 수지 조성물
KR102503262B1 (ko) * 2016-05-19 2023-02-22 에이치디씨폴리올 주식회사 내화학성이 우수한 폴리아릴렌 설파이드 수지 조성물
JP2023519156A (ja) * 2020-03-26 2023-05-10 ディーエスエム アイピー アセッツ ビー．ブイ． 射出成形部品
KR20220007274A (ko) * 2020-07-10 2022-01-18 에이치디씨폴리올 주식회사 폴리아릴렌 설파이드 공중합체, 이의 제조방법, 및 이로부터 제조된 성형품

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2513188A (en) 1948-09-10 1950-06-27 Macallum Alexander Douglas Mixed phenylene sulfide resins
US2583941A (en) 1946-11-13 1952-01-29 Jr Thurlow M Gordon Device for detecting variations in fluid pressure
US4746758A (en) 1986-09-29 1988-05-24 Eastman Kodak Company Processes for preparing iodinated aromatic compounds
US4786713A (en) 1987-11-06 1988-11-22 Eastman Kodak Company Copoly(arylene sulfidex-disulfide)

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4952671A (en) 1988-07-15 1990-08-28 Eastman Kodak Company Terminated copoly(arylene sulfide)
US4857629A (en) * 1988-09-16 1989-08-15 Eastman Kodak Company Process for the preparation of copoly(arylene sulfide)
US4939236A (en) * 1989-03-10 1990-07-03 Eastman Kodak Company Process for preparation of copoly(arylene sulfide)
US4945155A (en) * 1989-05-11 1990-07-31 Eastman Kodak Company Preparation of low color copoly(arylene sulfide) by heating copoly(arylene sulfide)
US5256715A (en) 1991-09-19 1993-10-26 Phillips Petroleum Company Poly(arylene sulfide) resin composition
JPH10275577A (ja) 1997-03-31 1998-10-13 Canon Inc スペーサとその製法及び表示装置
KR101183780B1 (ko) * 2006-08-24 2012-09-17 에스케이케미칼주식회사 폴리아릴렌 설파이드의 제조방법
KR101196415B1 (ko) 2007-01-04 2012-11-02 에스케이케미칼주식회사 백색도가 높은 폴리아릴렌설파이드 수지 및 이의 제조방법
TWI466925B (zh) 2007-01-05 2015-01-01 Sk Chemicals Co Ltd 具有優良光度之聚芳硫醚樹脂的製造方法及其製成物
JP2009280794A (ja) 2008-04-22 2009-12-03 Toray Ind Inc ポリフェニレンスルフィド樹脂の処理方法
KR101549205B1 (ko) * 2008-12-23 2015-09-02 에스케이케미칼 주식회사 폴리아릴렌 설파이드의 제조 방법
KR101554010B1 (ko) * 2008-12-31 2015-09-18 에스케이케미칼 주식회사 유리 요오드 저감 폴리아릴렌 설파이드의 제조 방법

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2583941A (en) 1946-11-13 1952-01-29 Jr Thurlow M Gordon Device for detecting variations in fluid pressure
US2513188A (en) 1948-09-10 1950-06-27 Macallum Alexander Douglas Mixed phenylene sulfide resins
US4746758A (en) 1986-09-29 1988-05-24 Eastman Kodak Company Processes for preparing iodinated aromatic compounds
US4786713A (en) 1987-11-06 1988-11-22 Eastman Kodak Company Copoly(arylene sulfidex-disulfide)

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP2383308A4

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109096761A (zh) * 2013-10-01 2018-12-28 Dic株式会社 聚芳硫醚树脂组合物及其成形品、以及电动汽车部件
CN109096761B (zh) * 2013-10-01 2021-05-11 Dic株式会社 聚芳硫醚树脂组合物及其成形品、以及电动汽车部件

Also Published As

Publication number Publication date
ES2601363T3 (es) 2017-02-14
JP2012514068A (ja) 2012-06-21
US20110269935A1 (en) 2011-11-03
HK1209144A1 (en) 2016-03-24
CN104861163A (zh) 2015-08-26
CN102341434A (zh) 2012-02-01
US20150353687A1 (en) 2015-12-10
EP2383308A4 (en) 2015-08-12
JP5702731B2 (ja) 2015-04-15
EP2383308B1 (en) 2016-09-07
EP2383308A2 (en) 2011-11-02
KR20100079253A (ko) 2010-07-08
US9163119B2 (en) 2015-10-20
KR101554010B1 (ko) 2015-09-18
WO2010077039A3 (ko) 2010-10-14

Similar Documents

Publication Publication Date Title
WO2010077039A3 (ko) 유리 요오드 저감 폴리아릴렌 설파이드 제조 방법
GB201211010D0 (en) Stabilized lithium metal powder for lithium-ion applications, composition and production process
WO2010074482A2 (ko) 폴리아릴렌 설파이드의 제조 방법
EP2455408A4 (en) METHOD FOR MANUFACTURING FLUORINATED BLOCK COPOLYMER
WO2009016149A3 (en) Process for manufacturing glycidol
WO2012064102A3 (ko) 그래핀 피복 강판 및 이의 제조 방법
WO2008105189A1 (ja) ゴム状重合体粒子分散熱硬化性樹脂組成物、及びその製造方法
WO2008132314A3 (fr) Procede de synthese de nanoparticules metalliques cubiques en presence de deux reducteurs
WO2010029344A3 (en) Hyaluronic acid cryogel - compositions, uses, processes for manufacturing
BRPI0607836A2 (pt) produção de ferronìquel
TW200631963A (en) Process for preparing polymers
TW200642963A (en) Surface modified nanoparticle and method of preparing same
WO2008090870A1 (ja) 芳香族ポリエステル系樹脂成形体およびその製造方法
WO2009101947A3 (en) Process for producing carbon material
WO2010127087A8 (en) Pelletized low molecular weight brominated aromatic polymer compositions
WO2008105464A1 (ja) カルボン酸クロライドの製造方法
JP2010106179A5 (ko)
WO2008096723A1 (ja) 六フッ化リン酸塩の製造方法
EP2495215A3 (en) Process for producing monopersulfuric acid and monopersulfuric acid continuous production apparatus
EP2450361A4 (en) ORGANOMETALLIC COMPOUNDS AND METHOD FOR THE PRODUCTION THEREOF
MY146360A (en) Process for producing 1-(3,4-dichlorobenzyl)-5-octylbiguanide or a salt thereof
WO2010101448A3 (ko) 고온강도가 우수한 스테인레스 강재 및 그 제조방법
MX2014009002A (es) Nuevo proceso para la preparacion de silices precipitadas.
WO2011036387A3 (fr) Procédé de fonctionnalisation de structures carbonées, notamment de nanotubes de carbone
BR112012026631A2 (pt) processo para preparação de amidas do ácido pirazol carboxílico

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 200980157711.7

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 09836360

Country of ref document: EP

Kind code of ref document: A2

ENP Entry into the national phase

Ref document number: 2011543437

Country of ref document: JP

Kind code of ref document: A

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 13142932

Country of ref document: US

REEP Request for entry into the european phase

Ref document number: 2009836360

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 2009836360

Country of ref document: EP