WO2010059000A3 - 고분자 입자의 제조 장치 및 제조 방법 - Google Patents

고분자 입자의 제조 장치 및 제조 방법 Download PDF

Info

Publication number
WO2010059000A3
WO2010059000A3 PCT/KR2009/006881 KR2009006881W WO2010059000A3 WO 2010059000 A3 WO2010059000 A3 WO 2010059000A3 KR 2009006881 W KR2009006881 W KR 2009006881W WO 2010059000 A3 WO2010059000 A3 WO 2010059000A3
Authority
WO
WIPO (PCT)
Prior art keywords
present
degree
crosslinking
enables
polymer particles
Prior art date
Application number
PCT/KR2009/006881
Other languages
English (en)
French (fr)
Other versions
WO2010059000A2 (ko
WO2010059000A9 (ko
Inventor
최재훈
이창훈
서정현
김유석
송인협
최정욱
송광호
Original Assignee
(주)Lg화학
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by (주)Lg화학 filed Critical (주)Lg화학
Priority to CN2009801461676A priority Critical patent/CN102215951A/zh
Priority to JP2011537368A priority patent/JP5448004B2/ja
Priority to US13/127,012 priority patent/US8378039B2/en
Priority to EP09827765.0A priority patent/EP2357036B1/en
Publication of WO2010059000A2 publication Critical patent/WO2010059000A2/ko
Publication of WO2010059000A9 publication Critical patent/WO2010059000A9/ko
Publication of WO2010059000A3 publication Critical patent/WO2010059000A3/ko

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/12—Powdering or granulating
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/12—Powdering or granulating
    • C08J3/126—Polymer particles coated by polymer, e.g. core shell structures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00788—Three-dimensional assemblies, i.e. the reactor comprising a form other than a stack of plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00889—Mixing
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2325/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Derivatives of such polymers
    • C08J2325/02—Homopolymers or copolymers of hydrocarbons
    • C08J2325/04—Homopolymers or copolymers of styrene
    • C08J2325/06—Polystyrene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
    • C08J2333/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters
    • C08J2333/06—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters of esters containing only carbon, hydrogen, and oxygen, the oxygen atom being present only as part of the carboxyl radical

Abstract

본 발명은 고분자 입자의 제조 장치 및 제조 방법에 관한 것이다. 본 발명은, 단분산성이 우수하며, 가교도 및 중합도 등의 물성이 균일한 고분자 입자를 효율적으로 제조할 수 있는 장치 및 방법을 제공한다. 본 발명에서는 또한, 높은 가교도를 가지거나, 코어셀 또는 코어-더블셀 구조를 가지면서도 목적하는 입경 내에서 탁월한 단분산성을 나타내는 입자를 효과적으로 제조할 수 있다. 또한, 본 발명에서는, 상기 고분자 입자 제조 공정의 재현성을 탁월하게 유지할 수 있다. 추가로, 본 발명은, 입경, 형상, 가교도, 중합도 또는 구조 등과 중합액의 고형분 농도 등을 목적에 따라 효과적으로 제어할 수 있는 장치 및 방법을 제공한다.
PCT/KR2009/006881 2008-11-21 2009-11-23 고분자 입자의 제조 장치 및 제조 방법 WO2010059000A2 (ko)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN2009801461676A CN102215951A (zh) 2008-11-21 2009-11-23 制备聚合物粒子的装置和制备聚合物粒子的方法
JP2011537368A JP5448004B2 (ja) 2008-11-21 2009-11-23 高分子粒子の製造装置及び製造方法
US13/127,012 US8378039B2 (en) 2008-11-21 2009-11-23 Method and apparatus for manufacturing polymer particle
EP09827765.0A EP2357036B1 (en) 2008-11-21 2009-11-23 Method and apparatus for manufacturing polymer particle

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR20080116497 2008-11-21
KR10-2008-0116497 2008-11-21

Publications (3)

Publication Number Publication Date
WO2010059000A2 WO2010059000A2 (ko) 2010-05-27
WO2010059000A9 WO2010059000A9 (ko) 2010-07-15
WO2010059000A3 true WO2010059000A3 (ko) 2010-09-02

Family

ID=42198691

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2009/006881 WO2010059000A2 (ko) 2008-11-21 2009-11-23 고분자 입자의 제조 장치 및 제조 방법

Country Status (7)

Country Link
US (1) US8378039B2 (ko)
EP (1) EP2357036B1 (ko)
JP (1) JP5448004B2 (ko)
KR (1) KR101211856B1 (ko)
CN (1) CN102215951A (ko)
TW (1) TWI432457B (ko)
WO (1) WO2010059000A2 (ko)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012092249A (ja) * 2010-10-28 2012-05-17 Osaka Prefecture Univ 粒子状重合体及びその製造方法
EP2655439B1 (en) * 2010-12-21 2018-09-19 Dow Global Technologies LLC Polymerization process and raman analysis for olefin-based polymers
JP6331718B2 (ja) * 2014-06-03 2018-05-30 デクセリアルズ株式会社 光学活性化合物の製造方法
KR20170048464A (ko) * 2014-09-02 2017-05-08 쓰리엠 이노베이티브 프로퍼티즈 캄파니 비닐실란 가교결합제를 갖는 아크릴레이트 접착제
JP6471481B2 (ja) * 2014-12-03 2019-02-20 デクセリアルズ株式会社 光学活性β−アミノカルボニル化合物の製造方法
CN104549585B (zh) * 2014-12-31 2017-01-18 国家纳米科学中心 一种微流控芯片及使用其制备纳米胶囊的方法
US9481764B1 (en) 2015-10-13 2016-11-01 The Boeing Company Flow reactor synthesis of polymers
GB201521670D0 (en) * 2015-12-09 2016-01-20 Blacktrace Holdings Ltd A reactor device for reaction fluid
CN108380150B (zh) * 2018-03-21 2020-05-05 上海交通大学 制备低分子量聚苯乙烯的多通道微反应器系统及方法
CN111434753B (zh) * 2019-01-11 2021-11-12 中国石油化工股份有限公司 一种合成聚α烯烃基础油的方法
CN114505017B (zh) * 2020-10-28 2022-11-11 中国石油化工股份有限公司 一种烯烃水合反应装置及烯烃水合方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2504452B2 (ja) * 1987-03-13 1996-06-05 チッソ株式会社 横型反応器
WO1998007764A1 (en) * 1996-08-20 1998-02-26 Amoco Corporation Transfer of polymer particles between vapor phase polymerization reactors
US6082891A (en) * 1995-10-28 2000-07-04 Forschungszentrum Karlsruhe Gmbh Static micromixer
US20060089474A1 (en) * 2004-10-04 2006-04-27 Sumitomo Chemical Company, Limited Apparatus for continuous polymerization and method for continuous polymerizing using the same
WO2006071515A2 (en) * 2004-12-29 2006-07-06 Exxonmobil Chemical Patents Inc. Tubular polymerization reactors and polymers made therein

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS57145101A (en) 1980-12-30 1982-09-08 Nat Res Dev Polymerization
DE3222002A1 (de) * 1982-06-11 1983-12-15 Röhm GmbH, 6100 Darmstadt Kontinuierliches emulsionspolymerisationsverfahren
GB8710332D0 (en) 1987-04-30 1987-06-03 Daton Lovett A J Extensible elements
IT1230085B (it) * 1989-05-24 1991-10-05 Montedipe Spa Processo per la produzione in massa e in continuo di (co) polimeri vinil aromatici antiurto.
DE19634450A1 (de) * 1996-08-26 1998-03-05 Basf Ag Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen
DE19717877A1 (de) * 1997-04-28 1998-10-29 Basf Ag Verfahren zur Herstellung von partikelförmigen Homo- und Copolymerisaten aus Mikrosuspensionen in einem Rohrreaktor
DE19816886C2 (de) 1998-04-17 2001-06-07 Axiva Gmbh Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymerisaten
JP2003140386A (ja) * 2001-10-31 2003-05-14 Canon Inc 重合法トナーの製造方法
US7276565B2 (en) * 2003-06-20 2007-10-02 Xerox Corporation Continuous miniemulsion polymerization process
JP4417811B2 (ja) * 2004-02-27 2010-02-17 出光興産株式会社 カチオン重合による重合体の製造方法
EP1829920B9 (en) * 2004-11-09 2017-01-04 Sumitomo Bakelite Company, Limited Apparatus and method for producing raw material for recycled resin composition
BRPI0614392A2 (pt) * 2005-08-05 2011-03-22 Exxonmobil Chemical Patentes Inc processo e aparelho para fabricação de polìmeros e copolìmeros de etileno
KR100718302B1 (ko) 2006-03-16 2007-05-15 한국화학연구원 가교된 고분자비드 제조 장치
JP2008081639A (ja) * 2006-09-28 2008-04-10 Konica Minolta Business Technologies Inc 静電荷像現像用トナー、樹脂粒子、及び、樹脂微粒子重合装置

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2504452B2 (ja) * 1987-03-13 1996-06-05 チッソ株式会社 横型反応器
US6082891A (en) * 1995-10-28 2000-07-04 Forschungszentrum Karlsruhe Gmbh Static micromixer
WO1998007764A1 (en) * 1996-08-20 1998-02-26 Amoco Corporation Transfer of polymer particles between vapor phase polymerization reactors
US20060089474A1 (en) * 2004-10-04 2006-04-27 Sumitomo Chemical Company, Limited Apparatus for continuous polymerization and method for continuous polymerizing using the same
WO2006071515A2 (en) * 2004-12-29 2006-07-06 Exxonmobil Chemical Patents Inc. Tubular polymerization reactors and polymers made therein

Also Published As

Publication number Publication date
KR20100057524A (ko) 2010-05-31
EP2357036A4 (en) 2012-08-29
JP2012509386A (ja) 2012-04-19
US8378039B2 (en) 2013-02-19
JP5448004B2 (ja) 2014-03-19
TWI432457B (zh) 2014-04-01
US20110263800A1 (en) 2011-10-27
EP2357036B1 (en) 2017-09-27
CN102215951A (zh) 2011-10-12
WO2010059000A2 (ko) 2010-05-27
TW201035117A (en) 2010-10-01
EP2357036A2 (en) 2011-08-17
WO2010059000A9 (ko) 2010-07-15
KR101211856B1 (ko) 2012-12-12

Similar Documents

Publication Publication Date Title
WO2010059000A3 (ko) 고분자 입자의 제조 장치 및 제조 방법
WO2011065368A8 (ja) 吸水性樹脂粒子の製造方法、吸水性樹脂粒子、止水材及び吸収性物品
TWI646049B (zh) 多孔質碳材料、多孔質碳材料的製造方法、電極材料及吸附材料
WO2011007974A3 (ko) 고흡수성 수지의 제조방법
Yang et al. Synthesis of novel sunflower-like silica/polypyrrole nanocomposites via self-assembly polymerization
Lai et al. Surface characterization of TEMPO‐oxidized bacterial cellulose
Zhao et al. Preparation, characterization and photocatalytic degradation properties of a TiO 2/calcium alginate composite film and the recovery of TiO 2 nanoparticles
WO2010114632A3 (en) Metal nanoparticles functionalized with rationally designed coatings and uses thereof
WO2009001905A1 (ja) 球状有機ポリマー－シリコン化合物複合粒子、中空粒子およびそれらの製造方法
MX2009001242A (es) Proceso para producir particulas finas de polimero.
EP2770012A3 (en) Tetrafluoroethylene/hexafluoropropylene copolymer and the production method thereof, and electrical wire
TW201613686A (en) Composition mainly composed of ptfe, mixed powder, molding material, filtering medium for filter, air filter unit, and porous membrane manufacturing method
WO2012124934A3 (ko) 그라핀 섬유 및 이의 제조 방법
WO2009131910A3 (en) Process for the surface modification of particles
WO2011068697A3 (en) Functionalized zirconia nanoparticles and high index films made therefrom
JP2016102063A (ja) 複合材料
EP1911772A4 (en) PROCESS FOR PRODUCING AQUEOUS DISPERSION OF COMPOSITE FLUOROPOLYMER PARTICLES, AQUEOUS DISPERSION, AND COMPOSITE POLYMER PARTICLE
WO2009150367A3 (fr) Procede de preparation d'une dispersion de particules polymeriques en milieu aqueux
ATE501178T1 (de) Verfahren zur herstellung wasserabsorbierender polymerpartikel durch polymerisation von tropfen einer monomerlösung
CN104888626B (zh) 一种可降解聚乳酸微孔膜的制备方法
WO2009069973A3 (en) Catalytic composition for producing 1-alkene and acrylates copolymer and method for producing 1-alkene and acrylates copolymer
CN104629098A (zh) 一种多孔壳聚糖微球制备方法
WO2014079745A3 (en) Benefit delivery particle, compositions comprising said particles and a method for treating substrates
CN102040394B (zh) SiOC微介孔陶瓷及其制备方法
WO2008106381A3 (en) Electrospinning polymer fibers and fiber arrays using dc biased ac potential

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 200980146167.6

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 09827765

Country of ref document: EP

Kind code of ref document: A2

REEP Request for entry into the european phase

Ref document number: 2009827765

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 2009827765

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 2011537368

Country of ref document: JP

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 13127012

Country of ref document: US