WO2009051076A1 - フッ素化ナノダイヤモンド分散液の作製方法 - Google Patents

フッ素化ナノダイヤモンド分散液の作製方法 Download PDF

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Publication number
WO2009051076A1
WO2009051076A1 PCT/JP2008/068461 JP2008068461W WO2009051076A1 WO 2009051076 A1 WO2009051076 A1 WO 2009051076A1 JP 2008068461 W JP2008068461 W JP 2008068461W WO 2009051076 A1 WO2009051076 A1 WO 2009051076A1
Authority
WO
WIPO (PCT)
Prior art keywords
dispersion
fluorinated nanodiamond
production
subjecting
fluorinated
Prior art date
Application number
PCT/JP2008/068461
Other languages
English (en)
French (fr)
Inventor
Akifumi Yao
Original Assignee
Central Glass Company, Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Central Glass Company, Limited filed Critical Central Glass Company, Limited
Priority to CN2008801075135A priority Critical patent/CN101801846B/zh
Priority to KR1020107009951A priority patent/KR101167622B1/ko
Priority to US12/738,027 priority patent/US8961631B2/en
Priority to EP08839719.5A priority patent/EP2218684B1/en
Publication of WO2009051076A1 publication Critical patent/WO2009051076A1/ja

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/25—Diamond
    • C01B32/28—After-treatment, e.g. purification, irradiation, separation or recovery
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00—Materials not provided for elsewhere
    • C09K3/14—Anti-slip materials; Abrasives
    • C09K3/1454—Abrasive powders, suspensions and pastes for polishing
    • C09K3/1472—Non-aqueous liquid suspensions

Abstract

フッ素化ナノダイヤモンドと炭素数４以下のアルコールを混合し、超音波処理することにより懸濁液を作製し、得られる懸濁液を遠心分離による分級処理によりフッ素化ナノダイヤモンドの分散液を作製する精製工程、該精製工程で得られるフッ素化ナノダイヤモンドの分散液から前記アルコールを除去することにより乾燥フッ素化ナノダイヤモンドを作製する乾燥工程、該乾燥工程で得られる乾燥フッ素化ナノダイヤモンドと非プロトン性極性溶媒を混合し、超音波処理によりフッ素化ナノダイヤモンド分散液を作製する再分散工程を含む、フッ素化ナノダイヤモンド分散液の作製方法が提供される。
PCT/JP2008/068461 2007-10-15 2008-10-10 フッ素化ナノダイヤモンド分散液の作製方法 WO2009051076A1 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN2008801075135A CN101801846B (zh) 2007-10-15 2008-10-10 氟化纳米金刚石分散液的制作方法
KR1020107009951A KR101167622B1 (ko) 2007-10-15 2008-10-10 불소화 나노 다이아몬드 분산액의 제작방법
US12/738,027 US8961631B2 (en) 2007-10-15 2008-10-10 Process for production of dispersion of fluorinated nano diamond
EP08839719.5A EP2218684B1 (en) 2007-10-15 2008-10-10 Process for production of dispersion of fluorinated nano diamond

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2007-267655 2007-10-15
JP2007267655 2007-10-15
JP2008260649A JP5359166B2 (ja) 2007-10-15 2008-10-07 フッ素化ナノダイヤモンド分散液の作製方法
JP2008-260649 2008-10-07

Publications (1)

Publication Number Publication Date
WO2009051076A1 true WO2009051076A1 (ja) 2009-04-23

Family

ID=40567343

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/068461 WO2009051076A1 (ja) 2007-10-15 2008-10-10 フッ素化ナノダイヤモンド分散液の作製方法

Country Status (6)

Country Link
US (1) US8961631B2 (ja)
EP (1) EP2218684B1 (ja)
JP (1) JP5359166B2 (ja)
KR (1) KR101167622B1 (ja)
CN (1) CN101801846B (ja)
WO (1) WO2009051076A1 (ja)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011084444A (ja) * 2009-10-17 2011-04-28 Univ Of Fukui フッ素化炭素微粒子分散液

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5326381B2 (ja) * 2008-06-30 2013-10-30 セントラル硝子株式会社 フッ素化ナノダイヤモンドとその分散液および、その作製方法
US9745197B2 (en) 2012-03-16 2017-08-29 Carbodeon Ltd Oy Detonation nanodiamond material purification method and product thereof
GB2503643A (en) * 2012-04-27 2014-01-08 Univ Newcastle Method for separation of diamond particle clusters
US20160096967A1 (en) 2014-10-03 2016-04-07 C3Nano Inc. Property enhancing fillers for transparent coatings and transparent conductive films
JP6800445B2 (ja) * 2017-02-28 2020-12-16 株式会社ダイセル 表面修飾ナノダイヤモンド、前記表面修飾ナノダイヤモンドを含む分散液、及び複合材料
CN106737256A (zh) * 2017-03-17 2017-05-31 衢州学院 一种采用湿混法的纳米金刚石磨具丸片制备方法
CN111117723A (zh) * 2019-12-30 2020-05-08 国网河南省电力公司电力科学研究院 一种含纳米粉体的天然酯绝缘油的制备方法及制备装置

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005001983A (ja) 2003-05-20 2005-01-06 Futaba Corp 超分散状態ナノ炭素およびその製造方法
JP2005097375A (ja) 2003-09-24 2005-04-14 Okamoto Machine Tool Works Ltd ナノダイヤモンド非水分散液およびその調製方法
US20050158549A1 (en) 2003-11-26 2005-07-21 William Marsh Rice University Functionalization of nanodiamond powder through fluorination and subsequent derivatization reactions
JP2007238411A (ja) * 2006-03-10 2007-09-20 Naoki Komatsu ナノダイヤモンド
JP2007308351A (ja) * 2006-05-22 2007-11-29 Central Glass Co Ltd フッ素含有ナノダイヤモンド分散液、およびその作製方法
WO2007142213A1 (ja) * 2006-06-05 2007-12-13 Central Glass Co., Ltd. フッ素化ナノダイヤモンド分散液の調製方法

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CN1203915C (zh) * 2002-11-18 2005-06-01 长沙矿冶研究院 纳米金刚石的解团聚及分级方法
US7491554B2 (en) 2003-04-23 2009-02-17 Tadamasa Fujimura Carrier of a diamond fine particle for immobilizing virus
JP2004339412A (ja) * 2003-05-16 2004-12-02 Ishizuka Kenkyusho:Kk 研磨材用サブミクロンダイヤモンド粉及びその製造方法
US7300958B2 (en) 2003-05-20 2007-11-27 Futaba Corporation Ultra-dispersed nanocarbon and method for preparing the same
US20050015849A1 (en) 2003-07-10 2005-01-27 Norment Vincent Edward D-band

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005001983A (ja) 2003-05-20 2005-01-06 Futaba Corp 超分散状態ナノ炭素およびその製造方法
JP2005097375A (ja) 2003-09-24 2005-04-14 Okamoto Machine Tool Works Ltd ナノダイヤモンド非水分散液およびその調製方法
US20050158549A1 (en) 2003-11-26 2005-07-21 William Marsh Rice University Functionalization of nanodiamond powder through fluorination and subsequent derivatization reactions
JP2007238411A (ja) * 2006-03-10 2007-09-20 Naoki Komatsu ナノダイヤモンド
JP2007308351A (ja) * 2006-05-22 2007-11-29 Central Glass Co Ltd フッ素含有ナノダイヤモンド分散液、およびその作製方法
WO2007142213A1 (ja) * 2006-06-05 2007-12-13 Central Glass Co., Ltd. フッ素化ナノダイヤモンド分散液の調製方法

Non-Patent Citations (7)

* Cited by examiner, † Cited by third party
Title
AKIKO YONEMOTO; TATUMI OHI; SHINJI KAWASAKI; FUJIO OKINO; FUMIAKI KATAOKA; EIJI OSAWA; HIDEKAZU TOUHARA, ABSTRACT OF THE 83RD SPRING ANNUAL MEETING OF THE CHEMICAL SOCIETY OF JAPAN, March 2003 (2003-03-01), pages 101
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See also references of EP2218684A4 *
TATSUMI OHI; AKIKO YONEMOTO; SHINJI KAWASAKI; FUJIO OKINO; HIDEKAZU TOUHARA, ABSTRACT OF THE 26TH FLUORINE CONFERENCE OF JAPAN, November 2002 (2002-11-01), pages 24 - 25
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011084444A (ja) * 2009-10-17 2011-04-28 Univ Of Fukui フッ素化炭素微粒子分散液

Also Published As

Publication number Publication date
CN101801846B (zh) 2013-02-13
JP5359166B2 (ja) 2013-12-04
US20110232199A1 (en) 2011-09-29
KR20100074253A (ko) 2010-07-01
US8961631B2 (en) 2015-02-24
EP2218684B1 (en) 2013-08-07
KR101167622B1 (ko) 2012-07-20
EP2218684A1 (en) 2010-08-18
CN101801846A (zh) 2010-08-11
EP2218684A4 (en) 2012-04-18
JP2009114052A (ja) 2009-05-28

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