US4970072A - Bath preparation - Google Patents

Bath preparation Download PDF

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Publication number
US4970072A
US4970072A US07/148,120 US14812088A US4970072A US 4970072 A US4970072 A US 4970072A US 14812088 A US14812088 A US 14812088A US 4970072 A US4970072 A US 4970072A
Authority
US
United States
Prior art keywords
concentrate
bath
bath preparation
whey concentrate
whey
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
US07/148,120
Other languages
English (en)
Inventor
Tsuneo Honda
Toru Asakoshi
Hiroshi Ishido
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
KYODO MILK INDUSTRY Corp Ltd
Chugai Pharmaceutical Co Ltd
Kyodo Milk Industry Co Ltd
Original Assignee
Chugai Pharmaceutical Co Ltd
Kyodo Milk Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chugai Pharmaceutical Co Ltd, Kyodo Milk Industry Co Ltd filed Critical Chugai Pharmaceutical Co Ltd
Assigned to KYODO MILK INDUSTRY CORPORATION LTD., CHUGAI SEIYAKU KABUSHIKI KAISHA reassignment KYODO MILK INDUSTRY CORPORATION LTD. ASSIGNMENT OF ASSIGNORS INTEREST. Assignors: ASAKOSHI, TORU, HONDA, TSUNEO, ISHIDO, HIROSHI
Application granted granted Critical
Publication of US4970072A publication Critical patent/US4970072A/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • A61K8/986Milk; Derivatives thereof, e.g. butter
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S530/00Chemistry: natural resins or derivatives; peptides or proteins; lignins or reaction products thereof
    • Y10S530/827Proteins from mammals or birds
    • Y10S530/833Whey; cheese

Definitions

  • the present invention relates to a novel bath preparation. More particularly, the present invention relates to a bath preparation that contains as an effective ingredient a whey concentrate of high mineral content and which has good health promoting and beautifying effects.
  • inorganic salts such as sodium chloride, sodium hydrogencarbonate, sodium carbonate, sodium phosphate, calcium oxide and magnesium carbonate
  • inorganic acids such as boric acid and silicic anhydride
  • organic acids such as benzoic acid, citric acid and succinic acid
  • medicinal herbs such as fennel (Foeniculi fructus), phellodendron bark (Pheiodendri cortex), Japanese Angelica root (Angelicae radix) and cinnamon bark (Cinnamomi cortex); together with common additives such as a variety of natural essential oils, dyestuffs, perfumes, fats and oils, and alcohols.
  • bath preparations are said to have some ability to clean and sterilize the skin,.
  • bath preparations are even claimed to provide some psychological effects which can have a favourable influence on psychosomatic diseases by virtue of their colors and flavors.
  • a prior art technique related to milk-treated baths is a bath preparation in which a dairy ingredient selected from among cow's milk, milk components, powdered milk, unsweetened condensed milk, unsweetened condensed milk components, cream, and cream components is coated with cyclodextrin so as to improve the storage stability of the dairy ingredient (Unexamined Published Japanese Patent Application No. 181013/1985).
  • Japanese Patent Publication No. 5382/1978 An improvement directed to providing better warming and beautifying effects than those attained by natural mineral springs has been proposed (Japanese Patent Publication No. 5382/1978).
  • This is a bath preparation for use in an artificial mineral spring that has improved warming and beautifying effects and which contains a water-soluble salt of sodium or potassium (e.g. sodium carbonate or sodium sesquicarbonate), a chelate-forming water-soluble metal salt present in an amount sufficient to form a chelate through exchange with sodium or potassium bound to skin protein (e.g., a water-soluble salt of an alkaline earth metal such as calcium or magnesium), and a nonionic or anionic surfactant.
  • a water-soluble salt of sodium or potassium e.g. sodium carbonate or sodium sesquicarbonate
  • a chelate-forming water-soluble metal salt present in an amount sufficient to form a chelate through exchange with sodium or potassium bound to skin protein
  • a nonionic or anionic surfactant e.g. sodium
  • the bath preparation proposed in Unexamined Published Japanese Patent Application No. 181013/1985 which contains a coated compound in which a dairy ingredient (e.g., cow's milk, powdered milk or cream) is coated with cyclodextrin, successfully improved the keeping quality of the inherently labile dairy ingredient.
  • a dairy ingredient e.g., cow's milk, powdered milk or cream
  • cyclodextrin coat dissolves in the bath water and the dairy ingredient becomes directly exposed to the heat of the water, whereupon it deteriorates through accelerated oxidation, causing such troubles as the occurrence of a rancid smell.
  • the bath preparation proposed in Japanese Patent Publication No. 5382/1978 is chiefly intended to provide better warming and beautifying effects by incorporating the two principal ingredients, a water-soluble salt such as sodium carbonate or sodium hydrogencarbonate, and a chelateforming water-soluble salt of an alkaline earth metal such as calcium or magnesium. Therefore, not much can be expected from this bath preparation as regards the curative effects for dermal and other diseases such as rheumatism and neuralgia.
  • Bathing in milk-treated water has long been considered to be beneficial for beautifying and health-promoting purposes but it has the disadvantage of making the bath water cloudy and leaving a sticky effect on the skin after bathing.
  • the present inventors Under the circumstances described above, the present inventors undertook investigations to develop a new type of bath preparation that is stable, provides health-promoting and beautifying effects and which has curative effects with respect to various diseases.
  • the present inventors paid special attention to the tradition of bathing in milk-treated water that has long been known to have superior health-promoting and beautifying effects and in whey-treated water that has also been known to have curative effects for neuralgia and rheumatism.
  • the specific objective of the present inventors was to make efficient use of the vitamins and minerals present in these two kinds of bath water.
  • An object, therefore, of the present invention is to provide a novel type of clear bath preparation that has a whey concentrate of high mineral content as its active ingredient and which remains stable while exhibiting the intended health-promoting and beautifying effects.
  • the bath preparation of the present invention is characterized by containing a whey concentrate as the effective ingredient, with one or more known additives for bath preparations being incorporated as required.
  • the whey concentrate used as the effective ingredient in the bath preparation of the present invention has an increased mineral content. It may be prepared by the following procedures.
  • Skimmed milk obtained by centrifugation of cow's milk, or whey obtained as a by-product in cheese production is passed through an ultrafiltration membrane so that it is separated into a protein portion and a permeate.
  • Preparation of the whey concentrate starts with the permeate, which is first concentrated under vacuum to increase the solids content to at least about 40%, preferably at least about 60%. Thereafter, the concentrated solution is cooled, for example, to about 20°-30° C., and mixed with ground lactose in an amount of, for example, about 0.01-0.1%. The mixture is continuously cooled with stirring so as to accelerate the crystallization of the lactose. The mixture is cooled to about 7° C. and below and stirred for a period of at least about 2 hours.
  • the lactose After the lactose has completely crystallized, it is separated by a suitable technique such as filtration or with a centrifuge, preferably a decantertype centrifuge.
  • the resulting whey solution may be decolored, if necessary, with a suitable decoloring agent such as activated carbon, and subsequently dried by a suitable drying method such as spray drying, so as to produce a whey concentrate in powder form.
  • a suitable decoloring agent such as activated carbon
  • a suitable drying method such as spray drying
  • the thus prepared whey concentrate in powder form has a very high mineral content, say, in the range of from about 40% to about 70%.
  • a whey concentrate having such a high mineral content has not been known in the prior art.
  • the bath preparation of the present invention which contains the above-described whey concentrate as the effective ingredient may incorporate one or more of the common additives as required, such as inorganic salts, inorganic acids, organic acids, medicinal herbs, fats and oils, dyestuffs, perfumes, alcohols, and polyhydric alcohols.
  • the common additives such as inorganic salts, inorganic acids, organic acids, medicinal herbs, fats and oils, dyestuffs, perfumes, alcohols, and polyhydric alcohols.
  • inorganic salts such as sodium chloride, sodium hydrogencarbonate, sodium carbonate, sodium sulfate, sodium thiosulfate, calcium carbonate, magnesium carbonate, potassium sulfide, potassium bromide, calcium oxide, aluminum sulfate and iron sulfate
  • inorganic acids such as boric acid, silicic anhydride and metasilicic acid
  • organic acids such as benzoic acid, citric acid, fumaric acid, tartaric acid and pyrrolidone carboxylic acid
  • medicinal herbs such as fennel (Foeniculi fructus), phellodendron bark (Pheliodendri cortex), german chamomile (Matricaria chamomillae flos), cinnamon bark (Cinnamomi cortex), Japanese Angelica root (Angelicae radix), mentha herb (Menthae herba), Japanese iris, peony root (Paeoniae radix), bitter orange peel (Aurantii
  • inorganic acids
  • the additives for bath preparation illustrated above may be selected as appropriate for the specific use of the bath preparation. They may be used in any desired form such as a powder, granules, tablets, paste or, if they are herbs, in the form of an extract or shreds of a suitable size. The amount in which these additives are used also depends on the specific use of the bath preparation.
  • the bath preparation of the present invention may be formulated in a desired dosage form such as a powder, granules, a solution or tablets.
  • the amount in which the whey concentrate is incorporated in the bath preparation of the present invention is in no way limited and can be appropriately selected according to the specific objective of using this bath preparation.
  • the whey concentrate may be incorporated in an amount ranging from about 2 to about 80 wt % of the bath preparation.
  • the method of producing the bath preparation of the present invention depends upon its dosage form (whether of the powder type, granule type, solution type or tablet type) or on the kind and dosage form of the additives described above.
  • the bath preparation can be readily produced by merely mixing the whey concentrate with one or more of the additives that are illustrated above and which match a specific type of bath preparation.
  • such additives may be formulated in a variety of dosage forms before they are mixed with the whey concentrate to make a specific type of bath preparation.
  • the bath preparation made according to the present invention has a very high content of milk-derived minerals such as sodium, potassium, calcium and magnesium. Because of such high mineral content, the preparation has the great potential to serve as a curative in the treatment of various diseases such as shoulder stiffness, neuralgia, lumbago, rheumatism, oversensitiveness to cold, chapped hand, frostbite, miliaria, common acne, eczema and athlete's foot. It also contributes to beautification.
  • a further advantage is that unlike milk-treated bath water, the bath preparation of the present invention leaves no stickiness on the skin after bathing and instead will give a highly refreshing effect while keeping the body warm for an extended period of time.
  • Skimmed milk (1,000 g) was passed through an ultrafiltration membrane (average pore size, 0.01-0.05 ⁇ m) to separate it into a protein portion and a permeate.
  • the permeate was concentrated at 50°-60° C. at 600-700 mmHg to obtain a solids content of ca. 60%. Thereafter, the concentrated solution was cooled to about 25° C. and charged into a tank equipped with a cooler and a stirrer. When the temperature had decreased to about 25° C., ground lactose was added to the concentrated solution in an amount of about 0.1% of that solution and the cooling was continued with stirring to accelerate the crystallization of lactose. The stirred solution was cooled to about 5° C. and below with the stirring continued for about 4 hours.
  • One tablet (5.0 g) was added to the bath water (200 liters) and its ability to warm the human body was evaluated by 30 panelists.
  • Example 1 the ability of the solution to warm the human body was evaluated by 30 panelists, who answered unanimously that they felt much warmer after bathing in the treated bath water than in the untreated bath water.

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dermatology (AREA)
  • Zoology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
US07/148,120 1987-01-20 1988-01-19 Bath preparation Expired - Fee Related US4970072A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP62010203A JPS63179818A (ja) 1987-01-20 1987-01-20 浴剤組成物
JP62-10203 1987-01-20

Publications (1)

Publication Number Publication Date
US4970072A true US4970072A (en) 1990-11-13

Family

ID=11743715

Family Applications (1)

Application Number Title Priority Date Filing Date
US07/148,120 Expired - Fee Related US4970072A (en) 1987-01-20 1988-01-19 Bath preparation

Country Status (5)

Country Link
US (1) US4970072A (da)
EP (1) EP0275981A3 (da)
JP (1) JPS63179818A (da)
KR (1) KR880008799A (da)
DK (1) DK21788A (da)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5296472A (en) * 1991-12-05 1994-03-22 Vyrex Corporation Methods for delipidation of skin and cerumen removal
DE4427705A1 (de) * 1994-08-04 1996-02-08 Herbert Van Lier Pharmazeutisch wirksames, hautschonendes Milchserumbad
US5750149A (en) * 1993-01-26 1998-05-12 Horse Vitality Ltd Pharmaceutical and dermocosmetic compositions containing equine colostrum
US20040241197A1 (en) * 2001-07-25 2004-12-02 Beiersdorf Ag Cosmetic or dermatological preparations including creatinine or a derivative thereof and creatine or a derivative thereof and methods of applying the preparations to the skin
US20050123651A1 (en) * 2003-12-05 2005-06-09 Young-Ho Hahn Mineral water composition
US20060083708A1 (en) * 1998-01-26 2006-04-20 Sam Schwartz Composition using mineral salts for cosmetic or therapeutic treatment
CN104546648A (zh) * 2014-12-29 2015-04-29 腾冲县艾爱摩拉牛乳业有限责任公司 一种水牛乳清洗浴液制法

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0537737A1 (en) * 1991-10-17 1993-04-21 Kao Corporation Bath composition
DE19529773A1 (de) * 1995-08-12 1997-02-13 Beiersdorf Ag Hautpflegemittel und pflegendes Hautreinigungsmittel
JP5236415B2 (ja) * 2008-10-02 2013-07-17 オーム乳業株式会社 機能性生体水

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4851235A (en) * 1986-12-12 1989-07-25 National Starch And Chemical Corporation Production of fermented whey products containing an emulsifier

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE659567C (de) * 1936-08-13 1938-05-06 Wilhelm Loehr Seifenfreies Waschmittel
AT363193B (de) * 1979-08-24 1981-07-10 Eberle M & Co Doris Cosmetic Verfahren zur herstellung eines kosmetischen praeparates
SU1342503A1 (ru) * 1985-01-02 1987-10-07 Всесоюзный научно-исследовательский и проектный институт химической промышленности Моющее средство личной гигиены

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4851235A (en) * 1986-12-12 1989-07-25 National Starch And Chemical Corporation Production of fermented whey products containing an emulsifier

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
Koehler, cited in Chem. Abstracts, vol. 75 (1971), 25244u. *
Obata et al., cited in Chem. Abstracts, vol. 104 (1986), 128654z. *
Saut , in Cosmetics: Science and Technology, Second Ed., vol. 2, 1972, pp. 505 506. *
Saute, in Cosmetics: Science and Technology, Second Ed., vol. 2, 1972, pp. 505-506.
Soviet Inventions Illustrated, Section Chemical, week 8819, May 12, 1988, Derwent Publications Ltd., GB, Abstract No. D21E16 & Su A 1 342 503 (Cement Ind. Res. Inst.), (UMEA), 07 10 1987. *
Soviet Inventions Illustrated, Section Chemical, week 8819, May 12, 1988, Derwent Publications Ltd., GB, Abstract No. D21E16 & Su-A-1 342 503 (Cement Ind. Res. Inst.), (UMEA), 07-10-1987.

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5296472A (en) * 1991-12-05 1994-03-22 Vyrex Corporation Methods for delipidation of skin and cerumen removal
US5750149A (en) * 1993-01-26 1998-05-12 Horse Vitality Ltd Pharmaceutical and dermocosmetic compositions containing equine colostrum
DE4427705A1 (de) * 1994-08-04 1996-02-08 Herbert Van Lier Pharmazeutisch wirksames, hautschonendes Milchserumbad
US20060083708A1 (en) * 1998-01-26 2006-04-20 Sam Schwartz Composition using mineral salts for cosmetic or therapeutic treatment
US20040241197A1 (en) * 2001-07-25 2004-12-02 Beiersdorf Ag Cosmetic or dermatological preparations including creatinine or a derivative thereof and creatine or a derivative thereof and methods of applying the preparations to the skin
US20050123651A1 (en) * 2003-12-05 2005-06-09 Young-Ho Hahn Mineral water composition
CN104546648A (zh) * 2014-12-29 2015-04-29 腾冲县艾爱摩拉牛乳业有限责任公司 一种水牛乳清洗浴液制法

Also Published As

Publication number Publication date
JPH0427206B2 (da) 1992-05-11
JPS63179818A (ja) 1988-07-23
EP0275981A2 (en) 1988-07-27
EP0275981A3 (en) 1989-03-08
KR880008799A (ko) 1988-09-13
DK21788D0 (da) 1988-01-19
DK21788A (da) 1988-07-21

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AS Assignment

Owner name: CHUGAI SEIYAKU KABUSHIKI KAISHA, NO. 5-1, 5-CHOME,

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST.;ASSIGNORS:HONDA, TSUNEO;ASAKOSHI, TORU;ISHIDO, HIROSHI;REEL/FRAME:004840/0921

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Owner name: KYODO MILK INDUSTRY CORPORATION LTD., 17-2, KOAMI-

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST.;ASSIGNORS:HONDA, TSUNEO;ASAKOSHI, TORU;ISHIDO, HIROSHI;REEL/FRAME:004840/0921

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Owner name: CHUGAI SEIYAKU KABUSHIKI KAISHA,JAPAN

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:HONDA, TSUNEO;ASAKOSHI, TORU;ISHIDO, HIROSHI;REEL/FRAME:004840/0921

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Owner name: KYODO MILK INDUSTRY CORPORATION LTD.,JAPAN

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:HONDA, TSUNEO;ASAKOSHI, TORU;ISHIDO, HIROSHI;REEL/FRAME:004840/0921

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Effective date: 19941116

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Free format text: PATENT EXPIRED DUE TO NONPAYMENT OF MAINTENANCE FEES UNDER 37 CFR 1.362