TWI659935B - 熔融可成形鋰鋁矽酸鹽玻璃陶瓷 - Google Patents
熔融可成形鋰鋁矽酸鹽玻璃陶瓷 Download PDFInfo
- Publication number
- TWI659935B TWI659935B TW106137134A TW106137134A TWI659935B TW I659935 B TWI659935 B TW I659935B TW 106137134 A TW106137134 A TW 106137134A TW 106137134 A TW106137134 A TW 106137134A TW I659935 B TWI659935 B TW I659935B
- Authority
- TW
- Taiwan
- Prior art keywords
- glass
- weight
- sio
- viscosity
- glass ceramic
- Prior art date
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- 230000004927 fusion Effects 0.000 title 1
- 239000005398 lithium aluminium silicate glass-ceramic Substances 0.000 title 1
- 239000011521 glass Substances 0.000 claims abstract description 112
- 239000007791 liquid phase Substances 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 14
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 24
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 20
- 230000005496 eutectics Effects 0.000 claims description 20
- 229910018068 Li 2 O Inorganic materials 0.000 claims description 15
- 239000010453 quartz Substances 0.000 claims description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 9
- 239000010970 precious metal Substances 0.000 claims description 5
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 4
- 229910052709 silver Inorganic materials 0.000 claims description 4
- 229910006404 SnO 2 Inorganic materials 0.000 claims description 3
- 229910052737 gold Inorganic materials 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 229910052697 platinum Inorganic materials 0.000 claims description 3
- 229910000506 β-spodumene-lithium Inorganic materials 0.000 claims description 3
- 229910052763 palladium Inorganic materials 0.000 claims description 2
- 229910052703 rhodium Inorganic materials 0.000 claims description 2
- 239000002241 glass-ceramic Substances 0.000 abstract description 56
- 238000000034 method Methods 0.000 abstract description 35
- 239000000155 melt Substances 0.000 abstract description 7
- 238000002844 melting Methods 0.000 abstract description 5
- 238000010438 heat treatment Methods 0.000 description 10
- 239000011734 sodium Substances 0.000 description 10
- 239000006112 glass ceramic composition Substances 0.000 description 7
- 239000012071 phase Substances 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 7
- 229910052783 alkali metal Inorganic materials 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- 229910000502 Li-aluminosilicate Inorganic materials 0.000 description 5
- 150000001340 alkali metals Chemical class 0.000 description 5
- 239000005354 aluminosilicate glass Substances 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- PAZHGORSDKKUPI-UHFFFAOYSA-N lithium metasilicate Chemical compound [Li+].[Li+].[O-][Si]([O-])=O PAZHGORSDKKUPI-UHFFFAOYSA-N 0.000 description 4
- 229910052912 lithium silicate Inorganic materials 0.000 description 4
- 239000006060 molten glass Substances 0.000 description 4
- 229910052700 potassium Inorganic materials 0.000 description 4
- 239000011591 potassium Substances 0.000 description 4
- 230000007704 transition Effects 0.000 description 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 3
- 238000000137 annealing Methods 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- WVMPCBWWBLZKPD-UHFFFAOYSA-N dilithium oxido-[oxido(oxo)silyl]oxy-oxosilane Chemical compound [Li+].[Li+].[O-][Si](=O)O[Si]([O-])=O WVMPCBWWBLZKPD-UHFFFAOYSA-N 0.000 description 3
- 239000010433 feldspar Substances 0.000 description 3
- 229910052744 lithium Inorganic materials 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 239000002667 nucleating agent Substances 0.000 description 3
- 229910000500 β-quartz Inorganic materials 0.000 description 3
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000003103 lithium disilicate glass Substances 0.000 description 2
- 238000010309 melting process Methods 0.000 description 2
- 239000006064 precursor glass Substances 0.000 description 2
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- -1 alkali metal aluminosilicate Chemical class 0.000 description 1
- SXQXMCWCWVCFPC-UHFFFAOYSA-N aluminum;potassium;dioxido(oxo)silane Chemical compound [Al+3].[K+].[O-][Si]([O-])=O.[O-][Si]([O-])=O SXQXMCWCWVCFPC-UHFFFAOYSA-N 0.000 description 1
- 238000003279 ceramming Methods 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000007496 glass forming Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012768 molten material Substances 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000003504 photosensitizing agent Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000003303 reheating Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 238000003283 slot draw process Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
- C03C10/0018—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and monovalent metal oxide as main constituents
- C03C10/0027—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and monovalent metal oxide as main constituents containing SiO2, Al2O3, Li2O as main constituents
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B17/00—Forming molten glass by flowing-out, pushing-out, extruding or drawing downwardly or laterally from forming slits or by overflowing over lips
- C03B17/06—Forming glass sheets
- C03B17/064—Forming glass sheets by the overflow downdraw fusion process; Isopipes therefor
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B17/00—Forming molten glass by flowing-out, pushing-out, extruding or drawing downwardly or laterally from forming slits or by overflowing over lips
- C03B17/06—Forming glass sheets
- C03B17/067—Forming glass sheets combined with thermal conditioning of the sheets
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
- C03C10/0009—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing silica as main constituent
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
- C03C10/0018—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and monovalent metal oxide as main constituents
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C14/00—Glass compositions containing a non-glass component, e.g. compositions containing fibres, filaments, whiskers, platelets, or the like, dispersed in a glass matrix
- C03C14/004—Glass compositions containing a non-glass component, e.g. compositions containing fibres, filaments, whiskers, platelets, or the like, dispersed in a glass matrix the non-glass component being in the form of particles or flakes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/095—Glass compositions containing silica with 40% to 90% silica, by weight containing rare earths
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/097—Glass compositions containing silica with 40% to 90% silica, by weight containing phosphorus, niobium or tantalum
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2214/00—Nature of the non-vitreous component
- C03C2214/08—Metals
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Ceramic Engineering (AREA)
- Dispersion Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Glass Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361770376P | 2013-02-28 | 2013-02-28 | |
| US61/770,376 | 2013-02-28 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW201803823A TW201803823A (zh) | 2018-02-01 |
| TWI659935B true TWI659935B (zh) | 2019-05-21 |
Family
ID=50238513
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW106137134A TWI659935B (zh) | 2013-02-28 | 2014-02-26 | 熔融可成形鋰鋁矽酸鹽玻璃陶瓷 |
| TW103106576A TWI606985B (zh) | 2013-02-28 | 2014-02-26 | 熔融可成形鋰鋁矽酸鹽玻璃陶瓷 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW103106576A TWI606985B (zh) | 2013-02-28 | 2014-02-26 | 熔融可成形鋰鋁矽酸鹽玻璃陶瓷 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US9440878B2 (enExample) |
| EP (2) | EP2961702B1 (enExample) |
| JP (2) | JP6334572B2 (enExample) |
| KR (2) | KR102263681B1 (enExample) |
| CN (2) | CN105228964B (enExample) |
| TW (2) | TWI659935B (enExample) |
| WO (1) | WO2014134100A2 (enExample) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10752536B2 (en) * | 2014-10-30 | 2020-08-25 | Corning Incorporated | Glass-ceramic compositions and laminated glass articles incorporating the same |
| US10703671B2 (en) * | 2016-01-26 | 2020-07-07 | Corning Incorporated | Photosensitive glasses and glass ceramics and composite glass materials made therefrom |
| DE102016119108A1 (de) * | 2016-10-07 | 2018-04-12 | Degudent Gmbh | Lithiumsilikat-Glaskeramik |
| US10626046B2 (en) | 2016-10-12 | 2020-04-21 | Corning Incorporated | Glass ceramics |
| WO2019191480A1 (en) | 2018-03-29 | 2019-10-03 | Corning Incorporated | Glasses having high fracture toughness |
| NL2020914B1 (en) * | 2018-05-11 | 2019-11-18 | Corning Inc | Glasses having high fracture toughness |
| DE102018221827B4 (de) * | 2018-12-14 | 2023-12-28 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Verfahren zur Herstellung einer Glaskeramik und Glaskeramik |
| TW202120449A (zh) | 2019-11-20 | 2021-06-01 | 美商康寧公司 | 具有高斷裂韌性的含硼玻璃組成 |
| US11584681B2 (en) | 2019-11-26 | 2023-02-21 | Corning Incorporated | Ion exchangeable alkali aluminosilicate glass compositions having improved mechanical durability |
| US12454479B2 (en) | 2021-06-18 | 2025-10-28 | Corning Incorporated | Gold containing silicate glass |
| US11802072B2 (en) | 2021-06-18 | 2023-10-31 | Corning Incorporated | Gold containing silicate glass |
| KR20240023516A (ko) | 2021-06-18 | 2024-02-22 | 코닝 인코포레이티드 | 향상된 기계적 내구성을 갖는 착색 유리 물품 |
| US11634354B2 (en) | 2021-06-18 | 2023-04-25 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| US12054422B2 (en) | 2021-06-18 | 2024-08-06 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| WO2022266273A1 (en) | 2021-06-18 | 2022-12-22 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| US11597674B2 (en) | 2021-06-18 | 2023-03-07 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| US12378152B2 (en) | 2021-06-18 | 2025-08-05 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| US11560329B1 (en) | 2021-10-04 | 2023-01-24 | Corning Incorporated | Colored glass articles having improved mechanical durability |
| JP2023072220A (ja) * | 2021-11-12 | 2023-05-24 | 日本電気硝子株式会社 | Ｌｉ２Ｏ－Ａｌ２Ｏ３－ＳｉＯ２系結晶化ガラス |
| US12240782B2 (en) | 2022-05-31 | 2025-03-04 | Corning Incorporated | Ion exchangeable yellow glass articles |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101233086A (zh) * | 2005-07-29 | 2008-07-30 | 日本电气硝子株式会社 | 图案化结晶玻璃制品及其制造方法 |
| CN102089252A (zh) * | 2008-07-03 | 2011-06-08 | 康宁股份有限公司 | 用于电子设备的耐用玻璃陶瓷机壳/封罩 |
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-
2014
- 2014-02-20 US US14/185,202 patent/US9440878B2/en active Active
- 2014-02-26 CN CN201480011255.6A patent/CN105228964B/zh active Active
- 2014-02-26 EP EP14708776.1A patent/EP2961702B1/en active Active
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| CN101233086A (zh) * | 2005-07-29 | 2008-07-30 | 日本电气硝子株式会社 | 图案化结晶玻璃制品及其制造方法 |
| CN102089252A (zh) * | 2008-07-03 | 2011-06-08 | 康宁股份有限公司 | 用于电子设备的耐用玻璃陶瓷机壳/封罩 |
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| JP6648188B2 (ja) | 2020-02-14 |
| JP6334572B2 (ja) | 2018-05-30 |
| EP3553037A1 (en) | 2019-10-16 |
| WO2014134100A2 (en) | 2014-09-04 |
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| CN110078369B (zh) | 2023-01-10 |
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| CN110078369A (zh) | 2019-08-02 |
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| EP2961702A2 (en) | 2016-01-06 |
| KR102538051B1 (ko) | 2023-05-30 |
| US9919953B2 (en) | 2018-03-20 |
| US9440878B2 (en) | 2016-09-13 |
| JP2018111647A (ja) | 2018-07-19 |
| TW201439021A (zh) | 2014-10-16 |
| TWI606985B (zh) | 2017-12-01 |
| EP2961702B1 (en) | 2019-04-10 |
| US20140243183A1 (en) | 2014-08-28 |
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