TWI509035B

TWI509035B - Hard coating with a dispersion composition, a hard coat coating composition, and a hard coat coating

Hard coating with a dispersion composition, a hard coat coating composition, and a hard coat coating Download PDF

Info

Publication number: TWI509035B
Authority: TW; Taiwan
Prior art keywords: group; dispersion; hard coating; composition; coating
Prior art date: 2011-06-06

Application number

TW101118547A

Other languages

English (en)

Chinese (zh)

Other versions

TW201311835A (zh

Inventor

Masanori Omoto

Kazuyuki Kato

Original Assignee

Dai Ichi Kogyo Seiyaku Co Ltd

Priority date

2011-06-06

Filing date

2012-05-24

Publication date

2015-11-21

2012-05-24 Application filed by Dai Ichi Kogyo Seiyaku Co Ltd filed Critical Dai Ichi Kogyo Seiyaku Co Ltd

2013-03-16 Publication of TW201311835A publication Critical patent/TW201311835A/zh

2015-11-21 Application granted granted Critical

2015-11-21 Publication of TWI509035B publication Critical patent/TWI509035B/zh

Links

239000006185 dispersion Substances 0.000 title claims description 93
238000000576 coating method Methods 0.000 title claims description 89
239000011248 coating agent Substances 0.000 title claims description 88
239000000203 mixture Substances 0.000 title claims description 37
239000008199 coating composition Substances 0.000 title claims description 13
239000002270 dispersing agent Substances 0.000 claims description 94
239000002245 particle Substances 0.000 claims description 55
150000001875 compounds Chemical class 0.000 claims description 22
125000002947 alkylene group Chemical group 0.000 claims description 21
125000004432 carbon atom Chemical group C* 0.000 claims description 21
125000000217 alkyl group Chemical group 0.000 claims description 19
229910052799 carbon Inorganic materials 0.000 claims description 13
125000003342 alkenyl group Chemical group 0.000 claims description 12
239000002904 solvent Substances 0.000 claims description 9
125000005647 linker group Chemical group 0.000 claims description 8
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 6
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 6
239000000758 substrate Substances 0.000 claims description 6
238000009835 boiling Methods 0.000 claims description 5
125000000524 functional group Chemical group 0.000 claims description 4
239000010954 inorganic particle Substances 0.000 claims description 4
239000012752 auxiliary agent Substances 0.000 claims description 3
238000001704 evaporation Methods 0.000 claims description 3
125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 3
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238000000034 method Methods 0.000 description 39
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238000004519 manufacturing process Methods 0.000 description 24
239000002612 dispersion medium Substances 0.000 description 17
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230000015572 biosynthetic process Effects 0.000 description 14
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MFKRHJVUCZRDTF-UHFFFAOYSA-N 3-methoxy-3-methylbutan-1-ol Chemical compound COC(C)(C)CCO MFKRHJVUCZRDTF-UHFFFAOYSA-N 0.000 description 10
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238000006116 polymerization reaction Methods 0.000 description 5
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230000002776 aggregation Effects 0.000 description 4
125000003118 aryl group Chemical group 0.000 description 4
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HLZKNKRTKFSKGZ-UHFFFAOYSA-N tetradecan-1-ol Chemical compound CCCCCCCCCCCCCCO HLZKNKRTKFSKGZ-UHFFFAOYSA-N 0.000 description 4
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239000004593 Epoxy Substances 0.000 description 3
239000005057 Hexamethylene diisocyanate Substances 0.000 description 3
239000004440 Isodecyl alcohol Substances 0.000 description 3
229920003171 Poly (ethylene oxide) Polymers 0.000 description 3
239000002202 Polyethylene glycol Substances 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 3
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RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 description 3
239000012965 benzophenone Substances 0.000 description 3
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 3
BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 3
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239000012467 final product Substances 0.000 description 3
RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 description 3
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WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 3
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GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 3
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ALSTYHKOOCGGFT-KTKRTIGZSA-N (9Z)-octadecen-1-ol Chemical compound CCCCCCCC\C=C/CCCCCCCCO ALSTYHKOOCGGFT-KTKRTIGZSA-N 0.000 description 2
PMBXCGGQNSVESQ-UHFFFAOYSA-N 1-Hexanethiol Chemical compound CCCCCCS PMBXCGGQNSVESQ-UHFFFAOYSA-N 0.000 description 2
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125000000954 2-hydroxyethyl group Chemical group [H]C([*])([H])C([H])([H])O[H] 0.000 description 2
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229910052698 phosphorus Inorganic materials 0.000 description 2
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XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
238000000053 physical method Methods 0.000 description 2
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BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
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XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 2
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