TW341569B - Preparation process and purification process of dimeric cyclic ester of α-hydroxycarboxylic acid - Google Patents
Preparation process and purification process of dimeric cyclic ester of α-hydroxycarboxylic acidInfo
- Publication number
- TW341569B TW341569B TW086100909A TW86100909A TW341569B TW 341569 B TW341569 B TW 341569B TW 086100909 A TW086100909 A TW 086100909A TW 86100909 A TW86100909 A TW 86100909A TW 341569 B TW341569 B TW 341569B
- Authority
- TW
- Taiwan
- Prior art keywords
- oligomer
- hydroxycarboxylic acid
- cyclic ester
- dimeric cyclic
- depolymerization
- Prior art date
Links
- -1 cyclic ester Chemical class 0.000 title abstract 4
- 238000002360 preparation method Methods 0.000 title 1
- 238000000746 purification Methods 0.000 title 1
- 238000009835 boiling Methods 0.000 abstract 3
- 238000010438 heat treatment Methods 0.000 abstract 2
- 239000003495 polar organic solvent Substances 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000000155 melt Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D319/10—1,4-Dioxanes; Hydrogenated 1,4-dioxanes
- C07D319/12—1,4-Dioxanes; Hydrogenated 1,4-dioxanes not condensed with other rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyesters Or Polycarbonates (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP4800096 | 1996-02-09 | ||
| JP11313996 | 1996-04-10 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TW341569B true TW341569B (en) | 1998-10-01 |
Family
ID=26388215
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW086100909A TW341569B (en) | 1996-02-09 | 1997-01-28 | Preparation process and purification process of dimeric cyclic ester of α-hydroxycarboxylic acid |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US5830991A (index.php) |
| EP (1) | EP0789023A2 (index.php) |
| JP (1) | JP4871923B2 (index.php) |
| KR (1) | KR100218850B1 (index.php) |
| TW (1) | TW341569B (index.php) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100451402B1 (ko) | 1996-07-19 | 2004-10-06 | 구레하 가가쿠 고교 가부시키가이샤 | 가스 배리어성 복합필름 |
| DE69727304T2 (de) | 1996-09-13 | 2004-10-21 | Kureha Chemical Ind Co Ltd | Gasundurchlässiger mehrschichtiger hohler behälter |
| JP4565208B2 (ja) | 2000-03-31 | 2010-10-20 | 株式会社クレハ | グリコリドの精製方法 |
| US6916939B2 (en) * | 2000-08-11 | 2005-07-12 | Kureha Kagaku Kogyo K.K. | Process for the preparation of cyclic esters and method for purification of the same |
| ES2246385T3 (es) * | 2001-03-06 | 2006-02-16 | Kureha Kagaku Kogyo Kabushiki Kaisha | Procedimiento para la produccion de glicolido y composicion de acido glicolico. |
| JP4394352B2 (ja) * | 2001-04-12 | 2010-01-06 | 株式会社クレハ | グリコリドの製造方法 |
| JP2004043682A (ja) * | 2002-07-12 | 2004-02-12 | Nippon Shokubai Co Ltd | ポリグリコール酸の製造方法 |
| CA2511476A1 (en) * | 2002-12-23 | 2004-07-22 | Dow Global Technologies Inc. | Method of smc molding |
| US20040231845A1 (en) | 2003-05-15 | 2004-11-25 | Cooke Claude E. | Applications of degradable polymers in wells |
| US20090107684A1 (en) | 2007-10-31 | 2009-04-30 | Cooke Jr Claude E | Applications of degradable polymers for delayed mechanical changes in wells |
| EP1717236A1 (en) * | 2005-04-28 | 2006-11-02 | Purac Biochem B.V. | Method for purifying glycolide |
| JP5235311B2 (ja) * | 2007-02-20 | 2013-07-10 | 株式会社クレハ | 環状エステルの精製方法 |
| KR101274369B1 (ko) | 2008-06-20 | 2013-06-13 | 아사히 가세이 케미칼즈 가부시키가이샤 | α-히드록시산의 제조 방법 |
| EP2377858B1 (en) * | 2008-12-26 | 2014-04-30 | Kureha Corporation | Method for producing glycolide |
| CA2784995C (en) | 2009-12-21 | 2018-07-03 | Evonik Degussa Corporation | Process for preparing cyclic esters comprising unsaturated functional groups and polyesters prepared from same |
| CN102712617B (zh) | 2010-01-19 | 2015-06-24 | 株式会社吴羽 | 乙交酯的制造方法 |
| WO2012001003A1 (en) | 2010-07-02 | 2012-01-05 | Metabolic Explorer | Method for the preparation of hydroxy acids |
| JP2012097224A (ja) * | 2010-11-04 | 2012-05-24 | Hitachi Plant Technologies Ltd | ポリヒドロキシカルボン酸の製造装置および製造方法 |
| JP6326373B2 (ja) | 2012-11-22 | 2018-05-16 | 株式会社クレハ | 気液の向流接触による精留工程を備えるグリコリドの製造方法、及び、粗グリコリドの精製方法 |
| US9512100B2 (en) | 2013-03-26 | 2016-12-06 | Kureha Corporation | Method for producing glycolide |
| US9643949B2 (en) | 2013-03-27 | 2017-05-09 | Kureha Corporation | Method for producing glycolide |
| JP6144562B2 (ja) | 2013-07-22 | 2017-06-07 | 株式会社クレハ | 脂肪族ポリエステルの製造方法 |
| CN107286126A (zh) * | 2016-04-13 | 2017-10-24 | 中国石油化工股份有限公司 | 1,4-二氧杂环-2,5-己二酮的制备方法 |
| CN107286127A (zh) * | 2016-04-13 | 2017-10-24 | 中国石油化工股份有限公司 | 低酸含量1,4-二氧杂环-2,5-己二酮的制备方法 |
| CN107868076A (zh) * | 2016-09-26 | 2018-04-03 | 中国石油化工股份有限公司 | 低杂质含量乙交酯的制备 |
| CN110072856B (zh) * | 2017-01-24 | 2022-03-15 | 株式会社吴羽 | α-羟基羧酸二聚物环状酯的制造方法 |
| JP6785165B2 (ja) | 2017-01-27 | 2020-11-18 | 株式会社クレハ | 成形体の製造方法 |
| JP6751221B2 (ja) * | 2018-03-07 | 2020-09-02 | 株式会社クレハ | 環状エステルの製造方法 |
| WO2020087221A1 (en) * | 2018-10-29 | 2020-05-07 | Pujing Chemical Industry Co., Ltd | Controlled production of polyglycolic acid and glycolide |
| CN113603671A (zh) * | 2021-08-13 | 2021-11-05 | 山东谷雨春生物科技有限公司 | 一种提高交酯收率的方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2668162A (en) * | 1952-03-20 | 1954-02-02 | Du Pont | Preparation of high molecular weight polyhydroxyacetic ester |
| US4727163A (en) * | 1985-07-11 | 1988-02-23 | E. I. Du Pont De Nemours And Company | Process for preparing highly pure cyclic esters |
| US4835293A (en) * | 1987-02-24 | 1989-05-30 | E. I. Du Pont De Nemours And Company | Atmospheric pressure process for preparing pure cyclic esters |
| US5326887A (en) * | 1991-02-27 | 1994-07-05 | E. I. Du Pont De Nemours And Company | Process for the preparation of 1,4-dioxane-2,5-diones |
| TW211577B (index.php) * | 1991-07-24 | 1993-08-21 | Du Pont | |
| US5420304A (en) * | 1992-03-19 | 1995-05-30 | Biopak Technology, Ltd. | Method to produce cyclic esters |
| FR2692263B1 (fr) * | 1992-06-15 | 1994-09-23 | Flamel Tech Sa | Procédé de préparation d'esters cycliques d'acides-alpha-hydroxycarboxyliques. |
| US5342969A (en) * | 1993-03-03 | 1994-08-30 | E. I. Du Pont De Nemours And Company | Recovery of hydroxycarboxylic acid values from poly(hydroxycarboxylic acids) |
-
1997
- 1997-01-23 US US08/788,907 patent/US5830991A/en not_active Expired - Lifetime
- 1997-01-28 TW TW086100909A patent/TW341569B/zh not_active IP Right Cessation
- 1997-02-06 KR KR1019970003837A patent/KR100218850B1/ko not_active Expired - Fee Related
- 1997-02-07 EP EP97300823A patent/EP0789023A2/en not_active Withdrawn
-
2008
- 2008-07-08 JP JP2008178152A patent/JP4871923B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0789023A3 (index.php) | 1997-09-10 |
| JP4871923B2 (ja) | 2012-02-08 |
| KR970061886A (ko) | 1997-09-12 |
| JP2008297307A (ja) | 2008-12-11 |
| US5830991A (en) | 1998-11-03 |
| KR100218850B1 (ko) | 1999-09-01 |
| EP0789023A2 (en) | 1997-08-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Annulment or lapse of patent due to non-payment of fees |