TW341569B - Preparation process and purification process of dimeric cyclic ester of α-hydroxycarboxylic acid - Google Patents
Preparation process and purification process of dimeric cyclic ester of α-hydroxycarboxylic acidInfo
- Publication number
- TW341569B TW341569B TW086100909A TW86100909A TW341569B TW 341569 B TW341569 B TW 341569B TW 086100909 A TW086100909 A TW 086100909A TW 86100909 A TW86100909 A TW 86100909A TW 341569 B TW341569 B TW 341569B
- Authority
- TW
- Taiwan
- Prior art keywords
- oligomer
- hydroxycarboxylic acid
- cyclic ester
- dimeric cyclic
- depolymerization
- Prior art date
Links
- -1 cyclic ester Chemical class 0.000 title abstract 4
- 238000002360 preparation method Methods 0.000 title 1
- 238000000746 purification Methods 0.000 title 1
- 238000009835 boiling Methods 0.000 abstract 3
- 238000010438 heat treatment Methods 0.000 abstract 2
- 239000003495 polar organic solvent Substances 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000000155 melt Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D319/10—1,4-Dioxanes; Hydrogenated 1,4-dioxanes
- C07D319/12—1,4-Dioxanes; Hydrogenated 1,4-dioxanes not condensed with other rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyesters Or Polycarbonates (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP4800096 | 1996-02-09 | ||
| JP11313996 | 1996-04-10 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TW341569B true TW341569B (en) | 1998-10-01 |
Family
ID=26388215
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW086100909A TW341569B (en) | 1996-02-09 | 1997-01-28 | Preparation process and purification process of dimeric cyclic ester of α-hydroxycarboxylic acid |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US5830991A (cg-RX-API-DMAC7.html) |
| EP (1) | EP0789023A2 (cg-RX-API-DMAC7.html) |
| JP (1) | JP4871923B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR100218850B1 (cg-RX-API-DMAC7.html) |
| TW (1) | TW341569B (cg-RX-API-DMAC7.html) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6245437B1 (en) | 1996-07-19 | 2001-06-12 | Kureha Kagaku Kogyo K.K. | Gas-barrier composite film |
| KR100451403B1 (ko) | 1996-09-13 | 2004-10-06 | 구레하 가가쿠 고교 가부시키가이샤 | 가스 배리어성 다층 중공 용기 |
| JP4565208B2 (ja) * | 2000-03-31 | 2010-10-20 | 株式会社クレハ | グリコリドの精製方法 |
| DE60125045T2 (de) * | 2000-08-11 | 2007-07-05 | Kureha Corporation | Verfahren zur Herstellung eines cyclischen Esters durch Depolymerisation eines aliphatischen Polyesters und Verfahren zur Reinigung eines rohen cyclischen Esters |
| JP4317690B2 (ja) * | 2001-03-06 | 2009-08-19 | 株式会社クレハ | グリコリドの製造方法 |
| CN1266146C (zh) * | 2001-04-12 | 2006-07-26 | 株式会社吴羽 | 乙交酯生产方法以及用于生产乙交酯的乙醇酸低聚物 |
| JP2004043682A (ja) * | 2002-07-12 | 2004-02-12 | Nippon Shokubai Co Ltd | ポリグリコール酸の製造方法 |
| AU2003293148A1 (en) * | 2002-12-23 | 2004-07-29 | Dow Global Technologies Inc. | Method of smc molding |
| US20090107684A1 (en) | 2007-10-31 | 2009-04-30 | Cooke Jr Claude E | Applications of degradable polymers for delayed mechanical changes in wells |
| US20040231845A1 (en) | 2003-05-15 | 2004-11-25 | Cooke Claude E. | Applications of degradable polymers in wells |
| EP1717236A1 (en) * | 2005-04-28 | 2006-11-02 | Purac Biochem B.V. | Method for purifying glycolide |
| JP5235311B2 (ja) * | 2007-02-20 | 2013-07-10 | 株式会社クレハ | 環状エステルの精製方法 |
| CN102066305B (zh) | 2008-06-20 | 2015-11-25 | 旭化成化学株式会社 | α-羟酸的制造方法 |
| EP2377858B1 (en) * | 2008-12-26 | 2014-04-30 | Kureha Corporation | Method for producing glycolide |
| JP6150522B2 (ja) | 2009-12-21 | 2017-06-21 | エボニック コーポレイションEvonik Corporation | 不飽和官能基を含む環状エステルを調製するための方法及びこれから調製されるポリエステル |
| JP5813516B2 (ja) | 2010-01-19 | 2015-11-17 | 株式会社クレハ | グリコリドの製造方法 |
| WO2012001003A1 (en) | 2010-07-02 | 2012-01-05 | Metabolic Explorer | Method for the preparation of hydroxy acids |
| JP2012097224A (ja) * | 2010-11-04 | 2012-05-24 | Hitachi Plant Technologies Ltd | ポリヒドロキシカルボン酸の製造装置および製造方法 |
| WO2014080876A1 (ja) | 2012-11-22 | 2014-05-30 | 株式会社クレハ | 気液の向流接触による精留工程を備えるグリコリドの製造方法、及び、粗グリコリドの精製方法 |
| WO2014157140A1 (ja) | 2013-03-26 | 2014-10-02 | 株式会社クレハ | グリコリドの製造方法 |
| US9643949B2 (en) | 2013-03-27 | 2017-05-09 | Kureha Corporation | Method for producing glycolide |
| JP6144562B2 (ja) | 2013-07-22 | 2017-06-07 | 株式会社クレハ | 脂肪族ポリエステルの製造方法 |
| CN107286127A (zh) * | 2016-04-13 | 2017-10-24 | 中国石油化工股份有限公司 | 低酸含量1,4-二氧杂环-2,5-己二酮的制备方法 |
| CN107286126A (zh) * | 2016-04-13 | 2017-10-24 | 中国石油化工股份有限公司 | 1,4-二氧杂环-2,5-己二酮的制备方法 |
| CN107868076A (zh) * | 2016-09-26 | 2018-04-03 | 中国石油化工股份有限公司 | 低杂质含量乙交酯的制备 |
| US11046665B2 (en) | 2017-01-24 | 2021-06-29 | Kureha Corporation | Method for producing α-hydroxycarboxylic acid dimeric cyclic ester |
| JP6785165B2 (ja) | 2017-01-27 | 2020-11-18 | 株式会社クレハ | 成形体の製造方法 |
| WO2019172361A1 (ja) * | 2018-03-07 | 2019-09-12 | 株式会社クレハ | 環状エステルの製造方法 |
| WO2020087221A1 (en) * | 2018-10-29 | 2020-05-07 | Pujing Chemical Industry Co., Ltd | Controlled production of polyglycolic acid and glycolide |
| CN113603671A (zh) * | 2021-08-13 | 2021-11-05 | 山东谷雨春生物科技有限公司 | 一种提高交酯收率的方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2668162A (en) * | 1952-03-20 | 1954-02-02 | Du Pont | Preparation of high molecular weight polyhydroxyacetic ester |
| US4727163A (en) * | 1985-07-11 | 1988-02-23 | E. I. Du Pont De Nemours And Company | Process for preparing highly pure cyclic esters |
| US4835293A (en) * | 1987-02-24 | 1989-05-30 | E. I. Du Pont De Nemours And Company | Atmospheric pressure process for preparing pure cyclic esters |
| US5326887A (en) * | 1991-02-27 | 1994-07-05 | E. I. Du Pont De Nemours And Company | Process for the preparation of 1,4-dioxane-2,5-diones |
| TW211577B (cg-RX-API-DMAC7.html) * | 1991-07-24 | 1993-08-21 | Du Pont | |
| US5420304A (en) * | 1992-03-19 | 1995-05-30 | Biopak Technology, Ltd. | Method to produce cyclic esters |
| FR2692263B1 (fr) * | 1992-06-15 | 1994-09-23 | Flamel Tech Sa | Procédé de préparation d'esters cycliques d'acides-alpha-hydroxycarboxyliques. |
| US5342969A (en) * | 1993-03-03 | 1994-08-30 | E. I. Du Pont De Nemours And Company | Recovery of hydroxycarboxylic acid values from poly(hydroxycarboxylic acids) |
-
1997
- 1997-01-23 US US08/788,907 patent/US5830991A/en not_active Expired - Lifetime
- 1997-01-28 TW TW086100909A patent/TW341569B/zh not_active IP Right Cessation
- 1997-02-06 KR KR1019970003837A patent/KR100218850B1/ko not_active Expired - Fee Related
- 1997-02-07 EP EP97300823A patent/EP0789023A2/en not_active Withdrawn
-
2008
- 2008-07-08 JP JP2008178152A patent/JP4871923B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0789023A3 (cg-RX-API-DMAC7.html) | 1997-09-10 |
| JP4871923B2 (ja) | 2012-02-08 |
| EP0789023A2 (en) | 1997-08-13 |
| KR970061886A (ko) | 1997-09-12 |
| US5830991A (en) | 1998-11-03 |
| JP2008297307A (ja) | 2008-12-11 |
| KR100218850B1 (ko) | 1999-09-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Annulment or lapse of patent due to non-payment of fees |