TW316916B

TW316916B -

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Publication number: TW316916B
Authority: TW; Taiwan
Prior art keywords: integer; aromatic; alkyl; coating; item
Prior art date: 1994-04-29

Application number

TW83106161A

Other languages

English (en)

Chinese (zh)

Original Assignee

Rohm & Haas

Priority date

1994-04-29

Filing date

1994-07-06

Publication date

1997-10-01

1994-04-29 Priority claimed from US08/235,585 external-priority patent/US5574083A/en

1994-07-06 Application filed by Rohm & Haas filed Critical Rohm & Haas

1997-10-01 Application granted granted Critical

1997-10-01 Publication of TW316916B publication Critical patent/TW316916B/zh

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125000003118 aryl group Chemical group 0.000 claims description 79
238000000576 coating method Methods 0.000 claims description 59
239000011248 coating agent Substances 0.000 claims description 55
RAABOESOVLLHRU-UHFFFAOYSA-N diazene Chemical compound N=N RAABOESOVLLHRU-UHFFFAOYSA-N 0.000 claims description 43
239000002253 acid Substances 0.000 claims description 32
239000000203 mixture Substances 0.000 claims description 29
229910000071 diazene Inorganic materials 0.000 claims description 27
238000000034 method Methods 0.000 claims description 25
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
-1 aromatic isocyanate Chemical class 0.000 claims description 21
229920000642 polymer Polymers 0.000 claims description 21
125000000217 alkyl group Chemical group 0.000 claims description 15
238000004132 cross linking Methods 0.000 claims description 15
239000011230 binding agent Substances 0.000 claims description 14
239000001257 hydrogen Substances 0.000 claims description 10
229910052739 hydrogen Inorganic materials 0.000 claims description 10
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 8
150000001412 amines Chemical class 0.000 claims description 8
238000003763 carbonization Methods 0.000 claims description 8
125000002843 carboxylic acid group Chemical group 0.000 claims description 6
239000006185 dispersion Substances 0.000 claims description 6
238000002156 mixing Methods 0.000 claims description 6
239000003381 stabilizer Substances 0.000 claims description 6
125000000732 arylene group Chemical group 0.000 claims description 4
125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 4
125000006850 spacer group Chemical group 0.000 claims description 4
125000003107 substituted aryl group Chemical group 0.000 claims description 4
239000004721 Polyphenylene oxide Substances 0.000 claims description 3
229920002396 Polyurea Polymers 0.000 claims description 3
125000005418 aryl aryl group Chemical group 0.000 claims description 3
239000007788 liquid Substances 0.000 claims description 3
229920000570 polyether Polymers 0.000 claims description 3
125000005649 substituted arylene group Chemical group 0.000 claims description 3
239000012948 isocyanate Substances 0.000 claims description 2
125000002102 aryl alkyloxo group Chemical group 0.000 claims 2
VPKDCDLSJZCGKE-UHFFFAOYSA-N carbodiimide group Chemical group N=C=N VPKDCDLSJZCGKE-UHFFFAOYSA-N 0.000 claims 1
150000002823 nitrates Chemical class 0.000 claims 1
150000002989 phenols Chemical class 0.000 claims 1
230000002618 waking effect Effects 0.000 claims 1
238000012360 testing method Methods 0.000 description 56
239000010408 film Substances 0.000 description 33
NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 28
239000004642 Polyimide Substances 0.000 description 24
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 23
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229920001721 polyimide Polymers 0.000 description 23
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 21
239000003431 cross linking reagent Substances 0.000 description 19
238000011049 filling Methods 0.000 description 17
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YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 15
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 14
229920000058 polyacrylate Polymers 0.000 description 12
229920005989 resin Polymers 0.000 description 12
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KAPCRJOPWXUMSQ-UHFFFAOYSA-N [2,2-bis[3-(aziridin-1-yl)propanoyloxymethyl]-3-hydroxypropyl] 3-(aziridin-1-yl)propanoate Chemical compound C1CN1CCC(=O)OCC(COC(=O)CCN1CC1)(CO)COC(=O)CCN1CC1 KAPCRJOPWXUMSQ-UHFFFAOYSA-N 0.000 description 9
NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 9
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125000001931 aliphatic group Chemical group 0.000 description 8
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239000003054 catalyst Substances 0.000 description 8
239000008199 coating composition Substances 0.000 description 8
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IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 7
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 7
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 7
229910052782 aluminium Inorganic materials 0.000 description 7
230000000052 comparative effect Effects 0.000 description 7
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239000002904 solvent Substances 0.000 description 7
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150000001335 aliphatic alkanes Chemical class 0.000 description 5
238000006243 chemical reaction Methods 0.000 description 5
150000001875 compounds Chemical class 0.000 description 5
239000004745 nonwoven fabric Substances 0.000 description 5
239000007921 spray Substances 0.000 description 5
238000009736 wetting Methods 0.000 description 5
239000002023 wood Substances 0.000 description 5
239000008096 xylene Substances 0.000 description 5
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
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229920000178 Acrylic resin Polymers 0.000 description 4
239000004925 Acrylic resin Substances 0.000 description 4
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KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical class C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
229920002125 Sokalan® Polymers 0.000 description 4
229940072049 amyl acetate Drugs 0.000 description 4
PGMYKACGEOXYJE-UHFFFAOYSA-N anhydrous amyl acetate Natural products CCCCCOC(C)=O PGMYKACGEOXYJE-UHFFFAOYSA-N 0.000 description 4
125000005442 diisocyanate group Chemical group 0.000 description 4
239000000839 emulsion Substances 0.000 description 4
MNWFXJYAOYHMED-UHFFFAOYSA-M heptanoate Chemical compound CCCCCCC([O-])=O MNWFXJYAOYHMED-UHFFFAOYSA-M 0.000 description 4
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LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 description 4
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238000005406 washing Methods 0.000 description 4
POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 3
125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 3
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
229920000742 Cotton Polymers 0.000 description 3
229920004934 Dacron® Polymers 0.000 description 3
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 3
RWRDLPDLKQPQOW-UHFFFAOYSA-N Pyrrolidine Chemical compound C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 description 3
ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
239000000853 adhesive Substances 0.000 description 3
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 3
238000011109 contamination Methods 0.000 description 3
230000002079 cooperative effect Effects 0.000 description 3
238000004049 embossing Methods 0.000 description 3
125000001033 ether group Chemical group 0.000 description 3
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
238000011156 evaluation Methods 0.000 description 3
239000000835 fiber Substances 0.000 description 3
239000012467 final product Substances 0.000 description 3
238000002309 gasification Methods 0.000 description 3
239000011521 glass Substances 0.000 description 3
238000009434 installation Methods 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
239000005022 packaging material Substances 0.000 description 3
229920000768 polyamine Polymers 0.000 description 3
229920000728 polyester Polymers 0.000 description 3
229920000573 polyethylene Polymers 0.000 description 3
229920001223 polyethylene glycol Polymers 0.000 description 3
239000005020 polyethylene terephthalate Substances 0.000 description 3
229920001228 polyisocyanate Polymers 0.000 description 3
239000005056 polyisocyanate Substances 0.000 description 3
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 3
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 3
241000894007 species Species 0.000 description 3
238000003756 stirring Methods 0.000 description 3
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DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 3
DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 2
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
IUVCFHHAEHNCFT-INIZCTEOSA-N 2-[(1s)-1-[4-amino-3-(3-fluoro-4-propan-2-yloxyphenyl)pyrazolo[3,4-d]pyrimidin-1-yl]ethyl]-6-fluoro-3-(3-fluorophenyl)chromen-4-one Chemical compound C1=C(F)C(OC(C)C)=CC=C1C(C1=C(N)N=CN=C11)=NN1[C@@H](C)C1=C(C=2C=C(F)C=CC=2)C(=O)C2=CC(F)=CC=C2O1 IUVCFHHAEHNCFT-INIZCTEOSA-N 0.000 description 2
GJYCVCVHRSWLNY-UHFFFAOYSA-N 2-butylphenol Chemical compound CCCCC1=CC=CC=C1O GJYCVCVHRSWLNY-UHFFFAOYSA-N 0.000 description 2
NOWKCMXCCJGMRR-UHFFFAOYSA-N Aziridine Chemical compound C1CN1 NOWKCMXCCJGMRR-UHFFFAOYSA-N 0.000 description 2
FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 description 2
LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
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239000005977 Ethylene Substances 0.000 description 2
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OLLQYIBTJXUEEX-UHFFFAOYSA-N diethyl 3-hydroxypentanedioate Chemical compound CCOC(=O)CC(O)CC(=O)OCC OLLQYIBTJXUEEX-UHFFFAOYSA-N 0.000 description 2
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125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
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