TW201235291A - Nanowire preparation methods, compositions, and articles - Google Patents
Nanowire preparation methods, compositions, and articles Download PDFInfo
- Publication number
- TW201235291A TW201235291A TW101100504A TW101100504A TW201235291A TW 201235291 A TW201235291 A TW 201235291A TW 101100504 A TW101100504 A TW 101100504A TW 101100504 A TW101100504 A TW 101100504A TW 201235291 A TW201235291 A TW 201235291A
- Authority
- TW
- Taiwan
- Prior art keywords
- product
- amount
- metal
- ratio
- silver
- Prior art date
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- 239000002070 nanowire Substances 0.000 title claims abstract description 37
- 239000000203 mixture Substances 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title description 5
- 238000000034 method Methods 0.000 claims abstract description 50
- 229910021645 metal ion Inorganic materials 0.000 claims description 42
- 229910052751 metal Inorganic materials 0.000 claims description 33
- 239000002184 metal Substances 0.000 claims description 33
- 229910052709 silver Inorganic materials 0.000 claims description 33
- 239000004332 silver Substances 0.000 claims description 33
- -1 silver ions Chemical class 0.000 claims description 6
- 230000015572 biosynthetic process Effects 0.000 abstract description 8
- 238000003786 synthesis reaction Methods 0.000 abstract description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 48
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 39
- 239000000047 product Substances 0.000 description 38
- 239000002245 particle Substances 0.000 description 19
- 239000013078 crystal Substances 0.000 description 18
- 239000000243 solution Substances 0.000 description 17
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 12
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 10
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 10
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 9
- 229920005862 polyol Polymers 0.000 description 9
- 150000003077 polyols Chemical class 0.000 description 9
- 239000006185 dispersion Substances 0.000 description 7
- 239000003223 protective agent Substances 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 229910001961 silver nitrate Inorganic materials 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 238000012886 linear function Methods 0.000 description 4
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000002042 Silver nanowire Substances 0.000 description 2
- 238000003917 TEM image Methods 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 238000007872 degassing Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002923 metal particle Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000002073 nanorod Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 239000002798 polar solvent Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- YBCAZPLXEGKKFM-UHFFFAOYSA-K ruthenium(iii) chloride Chemical compound [Cl-].[Cl-].[Cl-].[Ru+3] YBCAZPLXEGKKFM-UHFFFAOYSA-K 0.000 description 2
- 235000000346 sugar Nutrition 0.000 description 2
- 150000008163 sugars Chemical class 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- GBECUEIQVRDUKB-UHFFFAOYSA-M thallium monochloride Chemical compound [Tl]Cl GBECUEIQVRDUKB-UHFFFAOYSA-M 0.000 description 2
- BWLBGMIXKSTLSX-UHFFFAOYSA-N 2-hydroxyisobutyric acid Chemical compound CC(C)(O)C(O)=O BWLBGMIXKSTLSX-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 241000219112 Cucumis Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- 229910021577 Iron(II) chloride Inorganic materials 0.000 description 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 210000005069 ears Anatomy 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000010109 expendable mold casting Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000002110 nanocone Substances 0.000 description 1
- 239000002071 nanotube Substances 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 238000000879 optical micrograph Methods 0.000 description 1
- 238000000399 optical microscopy Methods 0.000 description 1
- 150000004714 phosphonium salts Chemical class 0.000 description 1
- 229920006316 polyvinylpyrrolidine Polymers 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- CQLFBEKRDQMJLZ-UHFFFAOYSA-M silver acetate Chemical compound [Ag+].CC([O-])=O CQLFBEKRDQMJLZ-UHFFFAOYSA-M 0.000 description 1
- 229940071536 silver acetate Drugs 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/06—Metallic powder characterised by the shape of the particles
- B22F1/062—Fibrous particles
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Powder Metallurgy (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161429853P | 2011-01-05 | 2011-01-05 | |
| US13/314,232 US20120171072A1 (en) | 2011-01-05 | 2011-12-08 | Nanowire preparation methods, compositions, and articles |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TW201235291A true TW201235291A (en) | 2012-09-01 |
Family
ID=46380918
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW101100504A TW201235291A (en) | 2011-01-05 | 2012-01-05 | Nanowire preparation methods, compositions, and articles |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20120171072A1 (enExample) |
| EP (1) | EP2661333A1 (enExample) |
| JP (1) | JP2014507562A (enExample) |
| KR (1) | KR20130132890A (enExample) |
| CN (1) | CN103313813A (enExample) |
| TW (1) | TW201235291A (enExample) |
| WO (1) | WO2012094096A1 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104889383B (zh) * | 2015-05-21 | 2017-12-12 | 桂林理工大学 | 一种含银无水甘油悬浮液及其制备方法 |
| CN108746662A (zh) * | 2018-06-27 | 2018-11-06 | 苏州向心力纳米科技有限公司 | 一种制备银纳米线前驱液的制备方法 |
| CN112705721B (zh) * | 2019-10-25 | 2022-08-19 | 深圳市善柔科技有限公司 | 银纳米线的制备方法 |
| CN114029499B (zh) | 2021-11-08 | 2022-08-19 | 西北有色金属研究院 | 一种超长纳米银线材料的制备方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100342064C (zh) * | 2005-09-23 | 2007-10-10 | 浙江大学 | 一种银纳米线的合成方法 |
| JP2008013798A (ja) * | 2006-07-04 | 2008-01-24 | Sumitomo Osaka Cement Co Ltd | ナノワイヤ状金属物質の製造方法及びナノワイヤ状金属物質並びにナノワイヤ状金属物質含有組成物 |
| WO2009063744A1 (ja) * | 2007-11-16 | 2009-05-22 | Konica Minolta Holdings, Inc. | 金属ナノワイヤの製造方法、金属ナノワイヤ及び透明導電体 |
| JP2009215573A (ja) * | 2008-03-07 | 2009-09-24 | Fujifilm Corp | 棒状金属粒子及びその製造方法、並びに棒状金属粒子含有組成物、及び帯電防止材料 |
| JP5683256B2 (ja) * | 2010-12-24 | 2015-03-11 | 三菱製紙株式会社 | 銀ナノワイヤの製造方法 |
-
2011
- 2011-12-08 US US13/314,232 patent/US20120171072A1/en not_active Abandoned
- 2011-12-09 CN CN2011800640178A patent/CN103313813A/zh active Pending
- 2011-12-09 EP EP11808028.2A patent/EP2661333A1/en not_active Withdrawn
- 2011-12-09 JP JP2013548404A patent/JP2014507562A/ja active Pending
- 2011-12-09 WO PCT/US2011/064048 patent/WO2012094096A1/en not_active Ceased
- 2011-12-09 KR KR1020137016947A patent/KR20130132890A/ko not_active Withdrawn
-
2012
- 2012-01-05 TW TW101100504A patent/TW201235291A/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP2661333A1 (en) | 2013-11-13 |
| JP2014507562A (ja) | 2014-03-27 |
| US20120171072A1 (en) | 2012-07-05 |
| KR20130132890A (ko) | 2013-12-05 |
| CN103313813A (zh) | 2013-09-18 |
| WO2012094096A1 (en) | 2012-07-12 |
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