JP2014507562A - ナノワイヤの調製方法、組成物および物品 - Google Patents
ナノワイヤの調製方法、組成物および物品 Download PDFInfo
- Publication number
- JP2014507562A JP2014507562A JP2013548404A JP2013548404A JP2014507562A JP 2014507562 A JP2014507562 A JP 2014507562A JP 2013548404 A JP2013548404 A JP 2013548404A JP 2013548404 A JP2013548404 A JP 2013548404A JP 2014507562 A JP2014507562 A JP 2014507562A
- Authority
- JP
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- Prior art keywords
- product
- silver
- metal
- ratio
- metal ion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002070 nanowire Substances 0.000 title claims abstract description 50
- 239000000203 mixture Substances 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title description 11
- 238000000034 method Methods 0.000 claims abstract description 52
- 229910021645 metal ion Inorganic materials 0.000 claims description 41
- 239000002184 metal Substances 0.000 claims description 32
- 229910052751 metal Inorganic materials 0.000 claims description 32
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 abstract description 9
- 238000003786 synthesis reaction Methods 0.000 abstract description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 51
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 35
- 239000000047 product Substances 0.000 description 31
- 229910052709 silver Inorganic materials 0.000 description 27
- 239000004332 silver Substances 0.000 description 27
- 239000002245 particle Substances 0.000 description 21
- 239000000243 solution Substances 0.000 description 19
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 16
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 12
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 12
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 12
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 9
- 229920005862 polyol Polymers 0.000 description 9
- 150000003077 polyols Chemical class 0.000 description 9
- -1 iron ions Chemical class 0.000 description 8
- 229910001961 silver nitrate Inorganic materials 0.000 description 8
- 239000002904 solvent Substances 0.000 description 8
- 239000003223 protective agent Substances 0.000 description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 239000006185 dispersion Substances 0.000 description 6
- 150000002500 ions Chemical class 0.000 description 6
- 229910052742 iron Inorganic materials 0.000 description 4
- 238000012886 linear function Methods 0.000 description 4
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 101710134784 Agnoprotein Proteins 0.000 description 2
- 229910021577 Iron(II) chloride Inorganic materials 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- 239000002042 Silver nanowire Substances 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 238000003917 TEM image Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 150000003841 chloride salts Chemical class 0.000 description 2
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002923 metal particle Substances 0.000 description 2
- 239000002073 nanorod Substances 0.000 description 2
- 239000002071 nanotube Substances 0.000 description 2
- 239000002798 polar solvent Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 238000004626 scanning electron microscopy Methods 0.000 description 2
- 235000000346 sugar Nutrition 0.000 description 2
- 150000008163 sugars Chemical class 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 230000008685 targeting Effects 0.000 description 2
- 238000004627 transmission electron microscopy Methods 0.000 description 2
- 238000013019 agitation Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000002505 iron Chemical class 0.000 description 1
- 159000000014 iron salts Chemical class 0.000 description 1
- FXNJQPDKIOMNLN-UHFFFAOYSA-N iron;2-oxopropyl acetate Chemical compound [Fe].CC(=O)COC(C)=O FXNJQPDKIOMNLN-UHFFFAOYSA-N 0.000 description 1
- 238000000386 microscopy Methods 0.000 description 1
- 230000000877 morphologic effect Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000000879 optical micrograph Methods 0.000 description 1
- 238000000399 optical microscopy Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000010963 scalable process Methods 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/06—Metallic powder characterised by the shape of the particles
- B22F1/062—Fibrous particles
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Powder Metallurgy (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161429853P | 2011-01-05 | 2011-01-05 | |
| US61/429,853 | 2011-01-05 | ||
| US13/314,232 | 2011-12-08 | ||
| US13/314,232 US20120171072A1 (en) | 2011-01-05 | 2011-12-08 | Nanowire preparation methods, compositions, and articles |
| PCT/US2011/064048 WO2012094096A1 (en) | 2011-01-05 | 2011-12-09 | Nanowire preparation methods, compositions, and articles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2014507562A true JP2014507562A (ja) | 2014-03-27 |
| JP2014507562A5 JP2014507562A5 (enExample) | 2014-08-21 |
Family
ID=46380918
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013548404A Pending JP2014507562A (ja) | 2011-01-05 | 2011-12-09 | ナノワイヤの調製方法、組成物および物品 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20120171072A1 (enExample) |
| EP (1) | EP2661333A1 (enExample) |
| JP (1) | JP2014507562A (enExample) |
| KR (1) | KR20130132890A (enExample) |
| CN (1) | CN103313813A (enExample) |
| TW (1) | TW201235291A (enExample) |
| WO (1) | WO2012094096A1 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104889383B (zh) * | 2015-05-21 | 2017-12-12 | 桂林理工大学 | 一种含银无水甘油悬浮液及其制备方法 |
| CN108746662A (zh) * | 2018-06-27 | 2018-11-06 | 苏州向心力纳米科技有限公司 | 一种制备银纳米线前驱液的制备方法 |
| CN112705721B (zh) * | 2019-10-25 | 2022-08-19 | 深圳市善柔科技有限公司 | 银纳米线的制备方法 |
| CN114029499B (zh) * | 2021-11-08 | 2022-08-19 | 西北有色金属研究院 | 一种超长纳米银线材料的制备方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008013798A (ja) * | 2006-07-04 | 2008-01-24 | Sumitomo Osaka Cement Co Ltd | ナノワイヤ状金属物質の製造方法及びナノワイヤ状金属物質並びにナノワイヤ状金属物質含有組成物 |
| WO2009063744A1 (ja) * | 2007-11-16 | 2009-05-22 | Konica Minolta Holdings, Inc. | 金属ナノワイヤの製造方法、金属ナノワイヤ及び透明導電体 |
| JP2009215573A (ja) * | 2008-03-07 | 2009-09-24 | Fujifilm Corp | 棒状金属粒子及びその製造方法、並びに棒状金属粒子含有組成物、及び帯電防止材料 |
| JP2012132082A (ja) * | 2010-12-24 | 2012-07-12 | Mitsubishi Paper Mills Ltd | 銀ナノワイヤの製造方法およびそれを用いた透明導電膜 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100342064C (zh) * | 2005-09-23 | 2007-10-10 | 浙江大学 | 一种银纳米线的合成方法 |
-
2011
- 2011-12-08 US US13/314,232 patent/US20120171072A1/en not_active Abandoned
- 2011-12-09 CN CN2011800640178A patent/CN103313813A/zh active Pending
- 2011-12-09 EP EP11808028.2A patent/EP2661333A1/en not_active Withdrawn
- 2011-12-09 JP JP2013548404A patent/JP2014507562A/ja active Pending
- 2011-12-09 KR KR1020137016947A patent/KR20130132890A/ko not_active Withdrawn
- 2011-12-09 WO PCT/US2011/064048 patent/WO2012094096A1/en not_active Ceased
-
2012
- 2012-01-05 TW TW101100504A patent/TW201235291A/zh unknown
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008013798A (ja) * | 2006-07-04 | 2008-01-24 | Sumitomo Osaka Cement Co Ltd | ナノワイヤ状金属物質の製造方法及びナノワイヤ状金属物質並びにナノワイヤ状金属物質含有組成物 |
| WO2009063744A1 (ja) * | 2007-11-16 | 2009-05-22 | Konica Minolta Holdings, Inc. | 金属ナノワイヤの製造方法、金属ナノワイヤ及び透明導電体 |
| JP2009215573A (ja) * | 2008-03-07 | 2009-09-24 | Fujifilm Corp | 棒状金属粒子及びその製造方法、並びに棒状金属粒子含有組成物、及び帯電防止材料 |
| JP2012132082A (ja) * | 2010-12-24 | 2012-07-12 | Mitsubishi Paper Mills Ltd | 銀ナノワイヤの製造方法およびそれを用いた透明導電膜 |
Non-Patent Citations (1)
| Title |
|---|
| JPN5014003078; ＹＵＧＡＮＧ ＳＵＮ: 'ＵＮＩＦＯＲＭ ＳＩＬＶＥＲ ＮＡＮＯＷＩＲＥＳ ＳＹＮＴＨＥＳＩＳ ＢＹ ＲＥＤＵＣＩＮＧ ＡＧＮＯ３ ＷＩＴＨ ＥＴＨＹＬＥＮＥ ＧＬＹＣＯＬ ＩＮ ＴＨＥ ＰＲＥＳＥＮＣＥ ＯＦ ＳＥＥＤＳ Ａ' ＣＨＥＭＩＳＴＲＹ ＯＦ ＭＡＴＥＲＩＡＬＳ Ｖ１４ Ｎ１１, 20021108, Ｐ４７３６-４７４５, ＡＭＥＲＩＣＡＮ ＣＨＥＭＩＣＡＬ ＳＯＣＩＥＴＹ * |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20130132890A (ko) | 2013-12-05 |
| WO2012094096A1 (en) | 2012-07-12 |
| US20120171072A1 (en) | 2012-07-05 |
| CN103313813A (zh) | 2013-09-18 |
| TW201235291A (en) | 2012-09-01 |
| EP2661333A1 (en) | 2013-11-13 |
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