SU784773A3 - Способ получени моноацетоксиэтиленкарбоната - Google Patents
Способ получени моноацетоксиэтиленкарбоната Download PDFInfo
- Publication number
- SU784773A3 SU784773A3 SU752134772A SU2134772A SU784773A3 SU 784773 A3 SU784773 A3 SU 784773A3 SU 752134772 A SU752134772 A SU 752134772A SU 2134772 A SU2134772 A SU 2134772A SU 784773 A3 SU784773 A3 SU 784773A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- carbonate
- acetic acid
- formula
- monoacetoxyethylenecarbonate
- preparing
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims abstract description 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 3
- 238000003786 synthesis reaction Methods 0.000 claims description 3
- 150000001242 acetic acid derivatives Chemical class 0.000 claims description 2
- 229910052783 alkali metal Inorganic materials 0.000 claims description 2
- 150000001340 alkali metals Chemical class 0.000 claims description 2
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 2
- 125000005843 halogen group Chemical group 0.000 claims description 2
- 239000012429 reaction media Substances 0.000 claims description 2
- UFLFSNVZQRNKOX-UHFFFAOYSA-N carbonic acid;ethenyl acetate Chemical compound OC(O)=O.CC(=O)OC=C UFLFSNVZQRNKOX-UHFFFAOYSA-N 0.000 claims 1
- 239000003814 drug Substances 0.000 claims 1
- 229940079593 drug Drugs 0.000 claims 1
- MFEJSXNGUWIDSO-UHFFFAOYSA-N (2-oxo-1,3-dioxolan-4-yl) acetate Chemical compound CC(=O)OC1COC(=O)O1 MFEJSXNGUWIDSO-UHFFFAOYSA-N 0.000 abstract description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract description 4
- 239000003513 alkali Substances 0.000 abstract description 2
- 229910052736 halogen Inorganic materials 0.000 abstract description 2
- 150000002367 halogens Chemical group 0.000 abstract description 2
- 239000002253 acid Substances 0.000 abstract 2
- -1 alkaline earth metal salt Chemical class 0.000 abstract 1
- 150000002431 hydrogen Chemical class 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- ORTFAQDWJHRMNX-UHFFFAOYSA-N hydroxidooxidocarbon(.) Chemical compound O[C]=O ORTFAQDWJHRMNX-UHFFFAOYSA-N 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 229960000583 acetic acid Drugs 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical compound [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 description 2
- QNXQLPUEZYZYFC-UHFFFAOYSA-N (4-nitrophenyl)methyl acetate Chemical compound CC(=O)OCC1=CC=C([N+]([O-])=O)C=C1 QNXQLPUEZYZYFC-UHFFFAOYSA-N 0.000 description 1
- OYOKPDLAMOMTEE-UHFFFAOYSA-N 4-chloro-1,3-dioxolan-2-one Chemical compound ClC1COC(=O)O1 OYOKPDLAMOMTEE-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical group CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- NDQKGYXNMLOECO-UHFFFAOYSA-N acetic acid;potassium Chemical compound [K].CC(O)=O NDQKGYXNMLOECO-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- MHDVGSVTJDSBDK-UHFFFAOYSA-N dibenzyl ether Chemical compound C=1C=CC=CC=1COCC1=CC=CC=C1 MHDVGSVTJDSBDK-UHFFFAOYSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- KGCNHWXDPDPSBV-UHFFFAOYSA-N p-nitrobenzyl chloride Chemical compound [O-][N+](=O)C1=CC=C(CCl)C=C1 KGCNHWXDPDPSBV-UHFFFAOYSA-N 0.000 description 1
- 235000011056 potassium acetate Nutrition 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D317/34—Oxygen atoms
- C07D317/36—Alkylene carbonates; Substituted alkylene carbonates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT22874/74A IT1012483B (it) | 1974-05-17 | 1974-05-17 | Processo per la preparazione di mo no acilossi od aroil ossi alchilen carbonati e prodotti ottenuti |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU784773A3 true SU784773A3 (ru) | 1980-11-30 |
Family
ID=11201415
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU752134772A SU784773A3 (ru) | 1974-05-17 | 1975-05-16 | Способ получени моноацетоксиэтиленкарбоната |
Country Status (19)
-
1974
- 1974-05-17 IT IT22874/74A patent/IT1012483B/it active
-
1975
- 1975-04-22 IL IL47142A patent/IL47142A0/xx unknown
- 1975-05-14 BE BE156326A patent/BE829048A/xx not_active IP Right Cessation
- 1975-05-14 NO NO751704A patent/NO751704L/no unknown
- 1975-05-14 DE DE19752521508 patent/DE2521508A1/de active Pending
- 1975-05-15 CS CS753400A patent/CS189592B2/cs unknown
- 1975-05-15 DD DD186067A patent/DD120876A5/xx unknown
- 1975-05-15 SE SE7505617A patent/SE418614B/xx unknown
- 1975-05-15 CH CH627275A patent/CH605901A5/xx not_active IP Right Cessation
- 1975-05-15 GB GB20709/75A patent/GB1503772A/en not_active Expired
- 1975-05-16 HU HU75SA00002792A patent/HU172188B/hu unknown
- 1975-05-16 SU SU752134772A patent/SU784773A3/ru active
- 1975-05-16 CA CA227,117A patent/CA1042906A/en not_active Expired
- 1975-05-16 ZA ZA00753165A patent/ZA753165B/xx unknown
- 1975-05-16 FR FR7515527A patent/FR2271223B1/fr not_active Expired
- 1975-05-16 DK DK216775A patent/DK216775A/da unknown
- 1975-05-16 JP JP50057495A patent/JPS51110568A/ja active Granted
- 1975-05-16 LU LU72494A patent/LU72494A1/xx unknown
- 1975-05-16 NL NL7505834A patent/NL7505834A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IT1012483B (it) | 1977-03-10 |
| ZA753165B (en) | 1976-04-28 |
| CS189592B2 (en) | 1979-04-30 |
| AU8104175A (en) | 1976-11-18 |
| BE829048A (fr) | 1975-09-01 |
| IL47142A0 (en) | 1975-07-28 |
| FR2271223A1 (enrdf_load_stackoverflow) | 1975-12-12 |
| DK216775A (da) | 1975-11-18 |
| LU72494A1 (enrdf_load_stackoverflow) | 1975-08-28 |
| GB1503772A (en) | 1978-03-15 |
| SE418614B (sv) | 1981-06-15 |
| JPS5519220B2 (enrdf_load_stackoverflow) | 1980-05-24 |
| DE2521508A1 (de) | 1975-11-20 |
| NO751704L (enrdf_load_stackoverflow) | 1975-11-18 |
| NL7505834A (nl) | 1975-11-19 |
| FR2271223B1 (enrdf_load_stackoverflow) | 1978-06-09 |
| JPS51110568A (en) | 1976-09-30 |
| CA1042906A (en) | 1978-11-21 |
| HU172188B (hu) | 1978-06-28 |
| DD120876A5 (enrdf_load_stackoverflow) | 1976-07-05 |
| CH605901A5 (enrdf_load_stackoverflow) | 1978-10-13 |
| SE7505617L (sv) | 1975-11-18 |
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