SU562190A3 - Способ получени фосфороксигалогенидов из реакционных смесей - Google Patents
Способ получени фосфороксигалогенидов из реакционных смесейInfo
- Publication number
- SU562190A3 SU562190A3 SU1835484A SU1835484A SU562190A3 SU 562190 A3 SU562190 A3 SU 562190A3 SU 1835484 A SU1835484 A SU 1835484A SU 1835484 A SU1835484 A SU 1835484A SU 562190 A3 SU562190 A3 SU 562190A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- phosphorus
- reaction mixtures
- parts
- carried out
- halide
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 13
- 239000011541 reaction mixture Substances 0.000 title claims description 6
- 229910001392 phosphorus oxide Inorganic materials 0.000 title claims 2
- LFGREXWGYUGZLY-UHFFFAOYSA-N phosphoryl Chemical class [P]=O LFGREXWGYUGZLY-UHFFFAOYSA-N 0.000 title claims 2
- 229910052698 phosphorus Inorganic materials 0.000 claims description 13
- 239000011574 phosphorus Substances 0.000 claims description 13
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 229910052736 halogen Inorganic materials 0.000 claims description 5
- 150000002367 halogens Chemical class 0.000 claims description 5
- -1 phosphorus halide Chemical class 0.000 claims description 5
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- 238000004821 distillation Methods 0.000 claims description 3
- RFFLAFLAYFXFSW-UHFFFAOYSA-N 1,2-dichlorobenzene Chemical compound ClC1=CC=CC=C1Cl RFFLAFLAYFXFSW-UHFFFAOYSA-N 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- 150000004820 halides Chemical class 0.000 claims 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- 239000003208 petroleum Substances 0.000 claims 1
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 description 10
- 239000000203 mixture Substances 0.000 description 4
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 2
- CNTIXUGILVWVHR-UHFFFAOYSA-N diphosphoryl chloride Chemical compound ClP(Cl)(=O)OP(Cl)(Cl)=O CNTIXUGILVWVHR-UHFFFAOYSA-N 0.000 description 2
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- NFHKZAUDRWRXMZ-UHFFFAOYSA-N 2-chloro-2,2-diphenylacetyl chloride Chemical compound C=1C=CC=CC=1C(Cl)(C(=O)Cl)C1=CC=CC=C1 NFHKZAUDRWRXMZ-UHFFFAOYSA-N 0.000 description 1
- ZESWUEBPRPGMTP-UHFFFAOYSA-N 4-nitrobenzamide Chemical compound NC(=O)C1=CC=C([N+]([O-])=O)C=C1 ZESWUEBPRPGMTP-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- PHSPJQZRQAJPPF-UHFFFAOYSA-N N-alpha-Methylhistamine Chemical compound CNCCC1=CN=CN1 PHSPJQZRQAJPPF-UHFFFAOYSA-N 0.000 description 1
- 239000000010 aprotic solvent Substances 0.000 description 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical group BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Chemical group 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/10—Halides or oxyhalides of phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1471471A CH567434A5 (https=) | 1971-10-08 | 1971-10-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU562190A3 true SU562190A3 (ru) | 1977-06-15 |
Family
ID=4403236
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1835484A SU562190A3 (ru) | 1971-10-08 | 1972-10-06 | Способ получени фосфороксигалогенидов из реакционных смесей |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US3845194A (https=) |
| JP (1) | JPS4845496A (https=) |
| BE (1) | BE789763A (https=) |
| CH (1) | CH567434A5 (https=) |
| DE (1) | DE2248747A1 (https=) |
| FR (1) | FR2156649B1 (https=) |
| GB (1) | GB1373312A (https=) |
| IT (1) | IT966220B (https=) |
| SU (1) | SU562190A3 (https=) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5198697A (ja) * | 1975-02-27 | 1976-08-31 | Okishenkarinnoseizohoho | |
| US4678612A (en) * | 1986-01-31 | 1987-07-07 | Stauffer Chemical Company | Process for the production of arylsulfonyl halides |
| DE4408404A1 (de) * | 1994-03-12 | 1995-09-14 | Huels Chemische Werke Ag | Verfahren zur Herstellung von Chlorpyrimidinen |
| CN1137099C (zh) * | 1995-01-30 | 2004-02-04 | 曾尼卡有限公司 | 4,6-二氯嘧啶的制法 |
| DE19730224A1 (de) * | 1997-07-15 | 1999-01-21 | Bayer Ag | Verfahren zur Reinigung Phosphoroxychlorid |
| AT405738B (de) * | 1997-09-03 | 1999-11-25 | Chemie Linz Gmbh | Verfahren zur reinigung von phosphoroxychlorid |
| JP2001526272A (ja) * | 1997-12-19 | 2001-12-18 | ダウ・アグロサイエンス・エル・エル・シー | クロロピリミジン法 |
| CN107324300A (zh) * | 2013-09-13 | 2017-11-07 | 重庆紫光化工股份有限公司 | 一种含磷废液的体系 |
| CN103539747B (zh) * | 2013-09-24 | 2016-08-10 | 重庆紫光化工股份有限公司 | 4,6-二氯嘧啶的制备方法 |
| CN104447569A (zh) * | 2014-11-05 | 2015-03-25 | 定陶县友帮化工有限公司 | 一种3,6-二氯哒嗪的合成方法 |
| CN107935933A (zh) * | 2017-12-12 | 2018-04-20 | 江西开元生物医药科技有限公司 | 一种5‑哌嗪基‑3‑甲基‑1‑苯基吡唑的制备方法 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1367751A (fr) * | 1962-07-12 | 1964-07-24 | Knapsack Ag | Procédé et appareil pour la préparation de l'oxychlorure de phosphore et des composés supérieurs oxygénés et chlorés du phosphore |
-
0
- BE BE789763D patent/BE789763A/xx unknown
-
1971
- 1971-10-08 CH CH1471471A patent/CH567434A5/xx not_active IP Right Cessation
-
1972
- 1972-09-27 US US00292562A patent/US3845194A/en not_active Expired - Lifetime
- 1972-09-27 GB GB4467772A patent/GB1373312A/en not_active Expired
- 1972-09-29 FR FR7234486A patent/FR2156649B1/fr not_active Expired
- 1972-10-05 DE DE19722248747 patent/DE2248747A1/de active Pending
- 1972-10-06 SU SU1835484A patent/SU562190A3/ru active
- 1972-10-06 IT IT53212/72A patent/IT966220B/it active
- 1972-10-07 JP JP47101047A patent/JPS4845496A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| BE789763A (fr) | 1973-04-06 |
| IT966220B (it) | 1974-02-11 |
| DE2248747A1 (de) | 1973-04-12 |
| CH567434A5 (https=) | 1975-10-15 |
| FR2156649B1 (https=) | 1975-01-03 |
| GB1373312A (en) | 1974-11-06 |
| FR2156649A1 (https=) | 1973-06-01 |
| US3845194A (en) | 1974-10-29 |
| JPS4845496A (https=) | 1973-06-29 |
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