RU2707136C1 - Vodka "vodka a" production method - Google Patents

Abstract

FIELD: alcohol industry.

SUBSTANCE: method includes sorting ethyl rectified "Lux" produced from selected corn from alcohol and drinking water corrected from artesian well. Sorting is mixed, filtered, passing through coal-cleaning battery and/or sorption-filtering elements of cartridge type of mari EPSF.UA_ag0.4, filled with activated carbon impregnated with silver, with filtration rate through one element with height of 1,000 mm from 3 to 21 dal/h. Vodka is delivered into a rendering tub. Honey natural is diluted with water with temperature of 70 °C in ratio of 1:5, thoroughly mixed, brought to a boiling point, stirred for 15–25 minutes, filtered in hot form and self-cooling to 10–20 °C. One pours 0.3–0.5 kg per 1,000 dal of corn vodka with a water-and-alcohol liquid with 50 % vol. at ratio of 1:10, stays in during 4.5–5.5 days while stirring, drained with infusion and filtered. In the rendering trough honey and infusion are successively introduced during 1.0–1.5 h stirring; vodka is delivered for rest for 1–3 months and subjected to control filtration. For production of 1,000 dal of vodka 3.8–4.2 kg of natural honey, 3.0–3.5 l of infusion of fortified grains of maize of the first drainage and the rest – rectified ethyl alcohol "Lux" and water as per calculation for 40 % vol. proof are used.

EFFECT: invention allows to enhance the ready product quality.

1 cl, 3 ex

Description

The invention relates to the distillery industry. A known method for the production of vodka, characterized in that they prepare an alcoholized infusion of corn grits by pouring them with a water-alcohol liquid with a strength of 45% in a ratio of 1:10, infusing for 5 days with periodic stirring, draining the infusion, thorough filtering, prepare sorting by mixing ethyl alcohol rectified "Lux" and corrected drinking water based on the receipt of finished vodka with a strength of 40% vol., thoroughly mixed, filtered on a coal-cleaning battery, sent vodka to a refined minutes vat, succinic acid are dissolved in demineralized water, with constant stirring, sodium bicarbonate, contribute sugar syrup, and solution infusion in dovodnoy vat with stirring, the blend was stirred, filtered and sent to bottling (patent RU 2252955, 2005). The disadvantage of this method is that the multicomponent leads to labor costs for their preparation for the process, the resulting vodka has not enough organoleptic characteristics, its tasting score is 9.36 points. A known method of producing vodka, characterized in that it is prepared from rectified ethyl alcohol and sorting water, purifying it with activated carbon, introducing ingredients into the vodka, including honey, purifying vodka with activated carbon, impregnated silver, followed by cooling (patent RU 2275421, 2006 )

The disadvantage of this method is, despite its high organoleptic characteristics, the use of uncharacteristic for vodka ingredients that are not related to crops.

The production of rectified ethyl alcohol from corn is known from the prior art (patent RU 2663723, 2018).

Known use in the production of vodka drinking corrected water from an artesian well (patent RU 2159280, 2000, BY 6240, 2004).

A known method of producing vodka, characterized in that it is prepared from rectified ethyl alcohol “Extra” and drinking water of corrected sorting, introducing sugar syrup, cleaning it with activated carbon, preparing a water-alcohol infusion of the first discharge from corn grits, filtering the infusion, maintain the filtrate, introducing in vodka filtrate, filtration of vodka and bottling (application RU 96114398, 1999).

The disadvantage of this method is that in the preparation of vodka is used alcohol "Extra", which does not provide it with high organoleptic characteristics.

The closest method to the invention is the method of producing vodka, characterized in that they prepare a sorting (water-alcohol solution) of rectified ethyl alcohol “Lux” and drinking water corrected in an amount that provides vodka with a 40% strength, mix the sorting carefully, and adjust the strength pass through a coal-cleaning battery, prepare the alcoholized infusions of the first discharge of the germ of corn and kelp dried by pouring water-alcohol liquid, respectively, with a strength of 50% in At a ratio of 1:20 and 1:15, infusion for 5 days with periodic stirring, draining the infusions and thoroughly filtering them, add the Bonavit complex food supplement and filtered glycine dissolved in corrected water and filtered into the vat to the filtered vodka. vodka or sorting granulated sugar in the form of 65.8% sugar syrup with constant stirring, the contents of the vat are mixed, if necessary, the condition of vodka is adjusted for strength, sent for bottling with a mandatory control filtration Iey (patent RU 2288261, 2006).

The disadvantage of this method is the use along with bread raw materials that are not characteristic of vodka, which distorts the organoleptic characteristics inherent in vodka. The tasting score of vodka is 9.69 points.

The technical result of the invention is to improve the quality of vodka. The technical result is achieved by the fact that the method of producing vodka is characterized in that a water-alcohol solution (sorting) is prepared from rectified ethyl alcohol from food raw materials “Lux” produced from selected corn and drinking water corrected from an artesian well so as to obtain vodka strength of 40 vol.%, mixed thoroughly sorting, it was filtered by passing through charcoal cleansing battery, and / or a sorption-type cartridge filter elements Mari EPSF.UA _ag0,4, filled activate with charcoal from a coconut shell impregnated with silver, with a filtering speed through one element 1000 mm high from 3 to 21 dal / h, filtered vodka is sent to a finishing vat, diluted honey with natural drinking water corrected from an artesian well with a temperature of 70 ° C in the ratio 1: 5, mix thoroughly until smooth, bring to a boil, mix for 15-25 minutes, filter while hot, and perform self-cooling to a temperature of 10-20 ° C, prepare an alcohol-infused infusion by pouring 0.3-0.5 kg per 1000 dal vodka corn kernels with an aqueous-alcoholic liquid with a strength of 50% vol. in a ratio of 1:10, infusion for 4.5-5.5 days with periodic stirring, draining the infusion and thorough filtering, add diluted chilled honey and infusion with continuous stirring of the blend for 1.0-1.5 to the vat, hours, they direct vodka to rest for 1-3 months and are subjected to control filtration when vodka is supplied to the pressure vessel and when it is supplied from the pressure vessel to the bottling, the following ingredients are used to obtain 1000 gave vodka:

natural honey - 3.8-4.2 kg the infusion of spirit grains of corn of the first plum - 3.0-3.5 L rectified ethyl alcohol from food raw materials "Lux" produced from selected corn and water drinking corrected from an artesian well - the rest is calculated on the strength of 40% vol.

The production method of vodka "Vodka A" ("Vodka A") is as follows.

For the production of vodka "Vodka A" ("Vodka A") are used:

- rectified ethyl alcohol from food raw materials "Lux", produced from selected corn, according to GOST 5962-2013;

- drinking water from an artesian well according to SanPiN 2.1.4.1074-01 with a hardness of up to 1 ° W for natural water and up to 0.2 ° W for corrected water;

- natural honey (light varieties) according to GOST 19792-2017 or approved for use in the prescribed manner;

- corn (grain) according to GOST 13634-2017;

- crushed active wood charcoal grade BAU-A according to GOST 6217-74 and other coal grades approved for use in the alcoholic beverage industry;

- carbon sorption-filtering cartridge elements impregnated with silver of EPSF.UA ag0.4 _grade in _accordance with TU 5131-018-10471723-2006 or other appropriate quality, approved for use in the established manner.

In the production of vodka use auxiliary materials that are approved for use in the distillery industry in the prescribed manner.

Prepare a water-alcohol solution (sorting) of rectified ethyl alcohol from food raw materials produced from selected corn and drinking water corrected from an artesian well so as to obtain vodka with a strength of 40% vol. Drinking artesian water is prepared by a method generally accepted in the industry. The technological process of its correction consists of the following stages of cleaning: filtering from mechanical impurities; deferrization of water on the deferrization filter; deodorization and sorption on a carbon filter; Na-cationite softening; demineralization in a reverse osmosis unit. Sorting is carried out batchwise. First, the calculated amount of alcohol is poured into the sorting vat from the alcohol storage via a measuring device, and then the corrected water with a hardness of up to 0.2 ° W, taking into account the receipt of a water-alcohol mixture of the required strength. After this, thorough sorting is done by sorting with a propeller stirrer, rotating at a frequency of 960 rpm for 1.0-1.5 hours. After adjusting the strength, the sorting is pumped to a pressure tank, and then it is filtered by passing through a coal-cleaning battery and / or installation "Silver filtration." The Silver Filtration unit consists of a preliminary filtration unit and two coal filtration units. The pre-filtering unit consists of cartridge-type filter elements based on wound textured polypropylene filament, which delays mechanical particles in sorting, thereby protecting carbon elements from mechanical impurities. Coal filtration unit

represents two filter holders in which there are sorption and filtering elements of the cartridge type of EPSF.UA _{ag0,4 brand} , filled with activated carbon from a coconut shell impregnated with silver. Filtering speed through one element with a height of 1000 mm from 3 to 21 dal / h. The filtering speed of sorting on a coal-cleaning battery for BAU-A brand coal is up to 40 dal / h for fresh coal and up to 30 dal / h for regenerated coal. Filtered vodka is sent to a clean-up vat. Natural honey is heated in hot water for 4 hours (in a water bath) and diluted with drinking water corrected from an artesian well with a temperature of 70 ° C in a ratio of 1: 5, mix thoroughly until smooth, bring to a boil, mix for 15-25 minutes, filtered hot and conduct self-cooling to a temperature of 10-20 ° C. Prepare an infusion of alcohol by pouring 0.3-0.5 kg per 1000 gave vodka dry corn kernels with an aqueous-alcoholic liquid with a strength of 50% vol. in a ratio of 1:10, infusion for 4.5-5.5 days with periodic stirring for 20-30 minutes 2 times per shift, draining the infusion and thorough filtering. Diluted chilled honey and infusion are successively added to the finishing vat with continuous mixing of the blend for 1.0-1.5 hours, vodka is sent to rest for 1-3 months and subjected to control filtration. The first filtration is carried out when vodka is supplied to the pressure vessel through filter elements of the cartridge type, which are located in the filter holder of the brand DF-NS (L) -08-750-AO. The second filtration is carried out directly during filling when vodka is supplied from the pressure vessel to the filling through the cartridge-type filter elements that are in the filter holder of the grade 8-A-750 P.

The following ingredients are used to produce 1000 dal vodka:

natural honey - 3.8-4.2 kg the infusion of spirit grains of corn of the first plum - 3.0-3.5 L rectified ethyl alcohol from food raw materials "Lux" produced from selected corn and water drinking corrected from an artesian well - the rest is calculated on the strength of 40% vol.

Example 1

Prepare a water-alcohol solution (sorting) of rectified ethyl alcohol from food raw materials produced from selected corn and drinking water corrected from an artesian well so as to obtain vodka with a strength of 40% vol. Sorting is carried out batchwise. First, the calculated amount of alcohol is poured into the sorting vat from the alcohol storage via a measuring device, and then the corrected water with a hardness of up to 0.2 ° F, taking into account the receipt of a water-alcohol mixture of the required strength. After this, the sorting is thoroughly mixed with a propeller stirrer, rotating at a frequency of 960 rpm for 1.0 hour. After adjusting the strength, the sorting is pumped into a pressure tank, and then it is filtered by passing through a coal-cleaning battery and the Silver Filtration unit. The Silver Filtration unit consists of a preliminary filtration unit and two coal filtration units. The pre-filtering unit consists of cartridge-type filter elements based on wound textured polypropylene filament, which delays mechanical particles in sorting, thereby protecting carbon elements from mechanical impurities. The coal filtration unit consists of two filter holders, in which there are sorption-filtering elements of the cartridge type of EPSF.UA _{ag0,4 brand} , filled with activated carbon from coconut shell impregnated with silver. The filtration rate through one element with a height of 1000 mm 21 dal / h. The filtering speed of sorting on a coal-cleaning battery for BAU-A brand coal is up to 40 dal / h for fresh coal and up to 30 dal / h for regenerated coal. Filtered vodka is sent to a clean-up vat. Natural honey is heated in a water bath in hot water for 4 hours and diluted with drinking water corrected from an artesian well with a temperature of 70 ° C in a ratio of 1: 5, thoroughly mixed to a homogeneous state, brought to a boil, stirred for 15 minutes, filtered hot and conduct self-cooling to a temperature of 10 ° C. Prepare an infusion of alcoholized by pouring 0.3 kg per 1000 gave vodka dried corn kernels with an aqueous-alcoholic liquid with a strength of 50% vol. in a ratio of 1:10, infusion for 4.5 days with periodic stirring for 20 minutes, 2 times per shift, draining the infusion and thorough filtering. Diluted chilled honey and infusion are successively added to the finishing vat with continuous mixing of the blend for 1.0 hour, vodka is sent to rest for 1 month and subjected to control filtration. The first filtration is carried out when vodka is supplied to the pressure vessel through filter elements of the cartridge type, which are located in the filter holder of the brand DF-NS (L) -08-750-AO. The second filtration is carried out directly during filling when vodka is supplied from the pressure vessel to the filling through the cartridge-type filter elements that are in the filter holder of the grade 8-A-750 P.

The following ingredients are used to produce 1000 dal vodka:

natural honey - 3.8 kg the infusion of spirit grains of corn of the first plum - 3.0 L rectified ethyl alcohol from food raw materials "Lux" produced from selected corn and water drinking corrected from an artesian well - the rest is calculated on the strength of 40% vol.

Example 2

Prepare a water-alcohol solution (sorting) of rectified ethyl alcohol from food raw materials produced from selected corn and drinking water corrected from an artesian well so as to obtain vodka with a strength of 40% vol. Sorting is carried out batchwise. First, the calculated amount of alcohol is poured into the sorting vat from the alcohol storage via a measuring device, and then the corrected water with a hardness of up to 0.2 ° F, taking into account the receipt of a water-alcohol mixture of the required strength. Then, thorough sorting is carried out by sorting with a propeller stirrer, rotating at a frequency of 960 rpm for 1 h 10 min. After adjusting the fortress, the sorting is pumped into a pressure tank, and then it is filtered by passing through the Silver Filtration unit. The Silver Filtration unit consists of a preliminary filtration unit and two coal filtration units. The pre-filtering unit consists of cartridge-type filter elements based on wound textured polypropylene filament, which delays mechanical particles in sorting, thereby protecting carbon elements from mechanical impurities. The coal filtration unit consists of two filter holders, in which there are sorption-filtering elements of the cartridge type of EPSF.UA _{ag0,4 brand} , filled with activated carbon from coconut shell impregnated with silver. The filtration rate through one element with a height of 1000 mm 3 dal / h. Filtered vodka is sent to a clean-up vat. Natural honey is heated in hot water for 4 hours (in a water bath) and diluted with drinking water corrected from an artesian well with a temperature of 70 ° C in a ratio of 1: 5, mix thoroughly until smooth, bring to a boil, mix for 20 minutes, filter in hot and carry out self-cooling to a temperature of 15 ° C. Prepare an infusion of alcoholized by the gulf of 0.4 kg per 1000 gave vodka dry corn kernels with an aqueous-alcoholic liquid with a strength of 50% vol. in a ratio of 1:10, infusion for 5.0 days with periodic stirring for 25 minutes, 2 times per shift, draining the infusion and thorough filtering. Diluted chilled honey and infusion are successively added to the finishing vat with continuous mixing of the blend for 1.5 hours, vodka is sent to rest for 3 months and subjected to control filtration. The first filtration is carried out when vodka is supplied to the pressure vessel through filter elements of the cartridge type, which are located in the filter holder of the brand DF-NS (L) -08-750-AO. The second filtration is carried out directly during filling when vodka is supplied from the pressure vessel to the filling through the cartridge-type filter elements that are in the filter holder of the grade 8-A-750 P.

The following ingredients are used to produce 1000 dal vodka:

natural honey - 4.0 kg the infusion of spirit grains of corn of the first plum - 3,2 l rectified ethyl alcohol from food raw materials "Lux" produced from selected corn and water drinking corrected from an artesian well - the rest is calculated on the strength of 40% vol.

Example 3

Prepare a water-alcohol solution (sorting) of rectified ethyl alcohol from food raw materials produced from selected corn and drinking water corrected from an artesian well so as to obtain vodka with a strength of 40% vol. Sorting is carried out batchwise. First, the calculated amount of alcohol is poured into the sorting vat from the alcohol storage via a measuring device, and then the corrected water with a hardness of up to 0.2 ° F, taking into account the receipt of a water-alcohol mixture of the required strength. After that, thorough sorting is done by sorting with a propeller stirrer, rotating at a frequency of 960 rpm for 1.5 hours. After adjusting the strength, the sorting is pumped to a pressure tank, and then it is filtered by passing through the Silver Filtration unit. The Silver Filtration unit consists of a preliminary filtration unit and two coal filtration units. The pre-filtering unit consists of cartridge-type filter elements based on wound textured polypropylene filament, which delays mechanical particles in sorting, thereby protecting carbon elements from mechanical impurities. Carbon filtration unit comprises two filter holder, in which there are sorption filter elements cartridge Mari EPSF.UA _ag0,4, filled with activated carbon of coconut shell impregnated silver. The filtration rate through one element with a height of 1000 mm is 15 dal / h. Filtered vodka is sent to a clean-up vat. Natural honey is heated in hot water for 4 hours (in a water bath) and diluted with drinking water corrected from an artesian well with a temperature of 70 ° C in a ratio of 1: 5, mix thoroughly until smooth, bring to a boil, mix for 25 minutes, filter in hot and carry out self-cooling to a temperature of 20 ° C. Prepare the infusion of alcoholized by pouring 0.5 kg per 1000 gave vodka dry corn kernels with an aqueous-alcoholic liquid with a strength of 50% vol. in a ratio of 1:10, infusion for 5.5 days with periodic stirring for 30 minutes, 2 times per shift, draining the infusion and thorough filtering. Diluted chilled honey and infusion are successively added to the vat with continuous blending for 1.5 hours, vodka is sent to rest for 2 months and subjected to control filtration. The first filtration is carried out when vodka is supplied to the pressure vessel through filter elements of the cartridge type, which are located in the filter holder of the brand DF-NS (L) -08-750-AO. The second filtration is carried out directly during filling when vodka is supplied from the pressure vessel to the filling through the cartridge-type filter elements that are in the filter holder of the grade 8-A-750 P.

The following ingredients are used to produce 1000 dal vodka:

natural honey - 4.2 kg the infusion of spirit grains of corn of the first plum - 3,5 l rectified ethyl alcohol from food raw materials "Lux" produced from selected corn and water drinking corrected from an artesian well - the rest is calculated on the strength of 40% vol.

Vodka "Vodka A" ("Vodka A"), produced from raw materials that do not contain gluten, has the following indicators.

Physicochemical.

Fortress,% 40,0 Alkalinity - volume of hydrochloric acid concentration s (HCL) = 0.1 mol / dm ³ consumed in titration 100 cm ³ vodka, cm ³ , no more 2.0 Mass concentration of acetic aldehyde in 1 DM ³ Anhydrous alcohol, g, not more than 3.0 Mass concentration of fusel oil (1-propanol, 2-propanol, isobutyl alcohol, 1-butanol, isoamyl alcohol) in 1 dm ³ anhydrous alcohol, mg, no more 5,0 Mass concentration of esters (methyl acetate, ethyl acetate) in 1 dm ^{3 of} anhydrous alcohol, mg, no more 5,0 The volume fraction of methyl alcohol in terms of anhydrous alcohol, 5, no more 0.02 Gluten free 0

Organoleptic.

Appearance - transparent liquid without impurities and sediment Colour - colorless, without additional shades Taste - soft, balanced, slightly sweet, with a pleasant enveloping finish Scent - characteristic vodka, harmonious, rounded.

According to the conclusion of the Tasting Commission, vodka has a tasting score of 9.72.

The invention improves the quality of the finished product, to obtain high-quality gluten-free vodka.

Claims (2)

A method of producing vodka, characterized in that a water-alcohol solution (sorting) is prepared from rectified ethyl alcohol from food raw materials “Lux”, produced from selected corn, and drinking water corrected from an artesian well so as to obtain vodka with a strength of 40 vol. %, thoroughly mix the sorting, filter it, passing through a coal-cleaning battery and / or sorption-filtering elements of the cartridge type marie EPSF. _{UA ag0,4} , filled with activated carbon from a coconut shell, impregnated with silver, with a filtering speed through one element with a height of 1000 mm from 3 to 21 dal / h, filtered vodka is sent to a finishing vat, natural honey is diluted with drinking water corrected from an artesian well with a temperature of 70 ° C in a ratio of 1: 5, mix thoroughly to homogeneous state, bring to a boil, mix for 15-25 minutes, filter hot and conduct self-cooling to a temperature of 10-20 ° C, prepare an alcohol-infused infusion by pouring 0.3-0.5 kg per 1000 dal of vodka of corn kernels water-alcohol Jew bone strength 50% vol. in a ratio of 1:10, infusion for 4.5-5.5 days with periodic stirring, draining the infusion and thorough filtering, add diluted chilled honey and infusion with continuous stirring of the blend for 1.0-1.5 to the vat, hours, they direct vodka to rest for 1-3 months and are subjected to control filtration when vodka is supplied to the pressure vessel and when it is supplied from the pressure vessel to the bottling, while using the following ingredients to obtain 1000 gave vodka: natural honey 3.8-4.2 kg the infusion of spirit grains of corn of the first plum 3.0-3.5 L rectified ethyl alcohol from food raw materials "Lux" produced from selected corn and drinking water corrected from an artesian well  the rest is calculated on the strength of 40 vol.%.