RU2615811C2 - Способ гранулирования мочевины с применением системы очистки газа - Google Patents

Способ гранулирования мочевины с применением системы очистки газа Download PDF

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RU2615811C2
RU2615811C2 RU2014146274A RU2014146274A RU2615811C2 RU 2615811 C2 RU2615811 C2 RU 2615811C2 RU 2014146274 A RU2014146274 A RU 2014146274A RU 2014146274 A RU2014146274 A RU 2014146274A RU 2615811 C2 RU2615811 C2 RU 2615811C2
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stream
ammonia
dust
urea
stage
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RU2014146274A
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English (en)
Russian (ru)
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RU2014146274A (ru
Inventor
Маттиас ПОТТХОФФ
Харальд ФРАНЦРАЕ
Люк Альберт ВАНМАРКЕ
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Уде Фертилайзе Текнолоджи Б.В.
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Application filed by Уде Фертилайзе Текнолоджи Б.В. filed Critical Уде Фертилайзе Текнолоджи Б.В.
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    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/14—Separation; Purification; Stabilisation; Use of additives
    • C07C273/16—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/54—Nitrogen compounds
    • B01D53/58—Ammonia
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/73—After-treatment of removed components
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C05C9/005—Post-treatment
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C05C9/02—Fertilisers containing urea or urea compounds containing urea-formaldehyde condensates
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2258/00—Sources of waste gases
    • B01D2258/02—Other waste gases
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Treating Waste Gases (AREA)
  • Gas Separation By Absorption (AREA)
  • Fertilizers (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
RU2014146274A 2012-05-08 2013-05-02 Способ гранулирования мочевины с применением системы очистки газа RU2615811C2 (ru)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12003585.2 2012-05-08
EP12003585.2A EP2662349A1 (en) 2012-05-08 2012-05-08 Urea granulation process with scrubbing system
PCT/EP2013/001292 WO2013167245A1 (en) 2012-05-08 2013-05-02 Urea granulation process with scrubbing system

Publications (2)

Publication Number Publication Date
RU2014146274A RU2014146274A (ru) 2016-06-27
RU2615811C2 true RU2615811C2 (ru) 2017-04-11

Family

ID=48470891

Family Applications (1)

Application Number Title Priority Date Filing Date
RU2014146274A RU2615811C2 (ru) 2012-05-08 2013-05-02 Способ гранулирования мочевины с применением системы очистки газа

Country Status (12)

Country Link
US (2) US9493407B2 (enExample)
EP (2) EP2662349A1 (enExample)
JP (1) JP2015522503A (enExample)
KR (1) KR20150030198A (enExample)
CN (2) CN107459372A (enExample)
AR (1) AR090974A1 (enExample)
BR (1) BR112014027819A2 (enExample)
CA (1) CA2872529A1 (enExample)
IN (1) IN2014DN10096A (enExample)
MY (1) MY171086A (enExample)
RU (1) RU2615811C2 (enExample)
WO (1) WO2013167245A1 (enExample)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016012925A1 (en) * 2014-07-20 2016-01-28 Sabic Global Technologies B.V. Methods for determining low sulfate concentrations in synthetic urea samples, produced in a manufacturing process and containing high levels of impurities
EP3020702A1 (en) * 2014-11-12 2016-05-18 Casale SA Urea finishing process with acid scrubbing
KR101577573B1 (ko) 2014-11-27 2015-12-15 휴켐스주식회사 질산암모늄 제조 공정용 스크러버 시스템
JPWO2016159336A1 (ja) * 2015-04-01 2018-02-01 東洋エンジニアリング株式会社 尿素製造方法
CA3034342A1 (en) * 2016-10-13 2018-04-19 Koch Agronomic Services, Llc Recovery and reuse of components from urea finishing waste streams
CN110325289B (zh) 2016-12-28 2022-04-08 沙特基础工业全球技术公司 从吹扫气流中回收溶剂
EP3366670A1 (en) * 2017-02-27 2018-08-29 Casale Sa A process and system to capture ammonia from a purge gas of a urea plant
JP6851869B2 (ja) * 2017-03-17 2021-03-31 東洋エンジニアリング株式会社 尿素の造粒方法
CN107715676A (zh) * 2017-10-10 2018-02-23 鲁西化工集团股份有限公司煤化工分公司 一种降低尿素造粒塔尾气氨含量的生产工艺
CN111111407A (zh) * 2019-12-16 2020-05-08 安徽德利来环保科技有限公司 一种车用尿素溶液的生产工艺
JP7277672B2 (ja) 2019-12-30 2023-05-19 スタミカーボン・ベー・フェー 尿素仕上げからのアンモニア除去
AU2020416567B2 (en) * 2019-12-30 2023-06-15 Stamicarbon B.V. Urea production with multiple evaporators
JP7296015B2 (ja) * 2019-12-30 2023-06-21 スタミカーボン・ベー・フェー 冷却凝縮部を備えた尿素プラント
EP3848341B1 (de) * 2020-01-08 2024-03-06 thyssenkrupp Fertilizer Technology GmbH Verfahren und vorrichtung zur herstellung eines düngemittels
CN111318042A (zh) * 2020-03-03 2020-06-23 中海石油华鹤煤化有限公司 一种生产改性尿素的装置系统及方法
CN117120414B (zh) * 2021-04-07 2026-02-27 卡萨乐有限公司 尿素生产工艺和设备
CN113101682B (zh) * 2021-05-28 2023-03-24 新疆心连心能源化工有限公司 减少蒸发掉缩合物稳定尿素生产的装置及处理方法
WO2023161236A1 (en) * 2022-02-22 2023-08-31 Tessenderlo Group Nv Methods for the production of a solid urea-thiosulfate fertilizer
WO2023161232A1 (en) * 2022-02-22 2023-08-31 Tessenderlo Group Nv Methods for the production of nitrogen fertilizer and nitrogen-sulfur fertilizer
WO2025244534A1 (en) * 2024-05-23 2025-11-27 Stamicarbon B.V. Technical grade urea granulate
WO2026037775A1 (en) 2024-08-14 2026-02-19 Casale Sa Urea granulation process and method of revamping

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU206590A1 (ru) * В. С. Гаврилов, А. Е. Кузнецова, И. А. Свист , Ф. М. Гриценко Способ получения мочевиноформальдегидныхудобрений
US4507129A (en) * 1982-01-07 1985-03-26 Norsk Hydro A.S. Method of cleaning dust-containing gas mixtures from a urea plant
US5686647A (en) * 1994-11-18 1997-11-11 Norsk Hydro A.S Process for the preparation of urea
WO2010060535A1 (en) * 2008-11-28 2010-06-03 Uhde Fertilizer Technology B.V. Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules

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CA1041484A (en) * 1974-12-20 1978-10-31 Silvio Vargiu Process for the preparation of urea-formaldehyde condensates to be used as fertilizers
US4370198A (en) 1980-03-13 1983-01-25 Mta Muszaki Kemiai Kutato Intezet Method and apparatus for the recovery of the solid material content of solutions and/or suspensions as granules in a gas fluidized bed
NL1002862C2 (nl) 1996-04-15 1997-10-17 Dsm Nv Werkwijze voor het bereiden van granules.
JPH09313860A (ja) 1996-05-27 1997-12-09 Shigeru Saito 湿式同時除害、除塵ガス処理装置及び方法
JP2000001466A (ja) 1998-06-12 2000-01-07 Toyo Eng Corp 排ガス中の尿素ダスト及びアンモニアの回収・利用方法
JP2000279736A (ja) * 1999-03-29 2000-10-10 Toyo Eng Corp 尿素ダスト及びアンモニアを含有する流体の処理装置、それを用いた処理方法及びそれを付設した尿素製造装置
NL1020665C2 (nl) 2002-05-23 2003-11-25 Dsm Nv Werkwijze voor het verwijderen van ammoniak uit een ammoniak-bevattende gasstroom.
DE10346519A1 (de) 2003-10-02 2005-05-04 Uhde Gmbh Verfahren zur Entfernung von Ammoniak und Staub aus einem Abgas, das bei der Herstellung von Düngemitteln anfällt
ES2391400T3 (es) * 2005-03-02 2012-11-26 Yara International Asa Reactor tubular e instalación para la fabricación de especialmente sulfato amónico-urea
ITMI20072206A1 (it) * 2007-11-21 2009-05-22 Snam Progetti Metodo per il recupero di ammoniaca da una corrente gassosa in un processo di sintesi di urea
EP2119489A1 (en) * 2008-05-14 2009-11-18 Uhde Fertilizer Technology B.V. Method for reducing aerosol emissions in a urea granulation plant
TW201032887A (en) * 2009-01-13 2010-09-16 Saipem Spa Process for the recovery of ammonia from a gaseous stream
BRPI1009270A2 (pt) 2009-03-17 2016-05-03 Bioecon Int Holding Nv processo para converter um material contendo polissacarídeo a um aditivo de combustível ou a um material substituto de combustível, e, uso de açúcares dianidro derivados

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU206590A1 (ru) * В. С. Гаврилов, А. Е. Кузнецова, И. А. Свист , Ф. М. Гриценко Способ получения мочевиноформальдегидныхудобрений
US4507129A (en) * 1982-01-07 1985-03-26 Norsk Hydro A.S. Method of cleaning dust-containing gas mixtures from a urea plant
US5686647A (en) * 1994-11-18 1997-11-11 Norsk Hydro A.S Process for the preparation of urea
WO2010060535A1 (en) * 2008-11-28 2010-06-03 Uhde Fertilizer Technology B.V. Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules

Also Published As

Publication number Publication date
AR090974A1 (es) 2014-12-17
US9493407B2 (en) 2016-11-15
US20150133689A1 (en) 2015-05-14
JP2015522503A (ja) 2015-08-06
BR112014027819A2 (pt) 2017-06-27
CN107459372A (zh) 2017-12-12
IN2014DN10096A (enExample) 2015-08-21
CN104321292B (zh) 2017-12-05
EP2847144B1 (en) 2018-04-04
EP2662349A1 (en) 2013-11-13
CA2872529A1 (en) 2013-11-14
CN104321292A (zh) 2015-01-28
US9745256B2 (en) 2017-08-29
US20160376230A1 (en) 2016-12-29
KR20150030198A (ko) 2015-03-19
WO2013167245A1 (en) 2013-11-14
RU2014146274A (ru) 2016-06-27
EP2847144A1 (en) 2015-03-18
HK1201515A1 (en) 2015-09-04
MY171086A (en) 2019-09-24

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