RU2607741C2 - Новый способ получения диоксидов кремния - Google Patents
Новый способ получения диоксидов кремния Download PDFInfo
- Publication number
- RU2607741C2 RU2607741C2 RU2014130284A RU2014130284A RU2607741C2 RU 2607741 C2 RU2607741 C2 RU 2607741C2 RU 2014130284 A RU2014130284 A RU 2014130284A RU 2014130284 A RU2014130284 A RU 2014130284A RU 2607741 C2 RU2607741 C2 RU 2607741C2
- Authority
- RU
- Russia
- Prior art keywords
- acid
- concentration
- silicate
- weight
- reaction medium
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/126—Preparation of silica of undetermined type
- C01B33/128—Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
- C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Paper (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1104089A FR2984871B1 (fr) | 2011-12-23 | 2011-12-23 | Nouveau procede de preparation de silices |
| FR11/04089 | 2011-12-23 | ||
| FR12/00217 | 2012-01-25 | ||
| FR1200217A FR2985994B1 (fr) | 2012-01-25 | 2012-01-25 | Nouveaux procede de preparation de silices precipitees |
| PCT/EP2012/076206 WO2013092745A1 (fr) | 2011-12-23 | 2012-12-19 | Procede de preparation de silices precipitees |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2014130284A RU2014130284A (ru) | 2016-02-10 |
| RU2607741C2 true RU2607741C2 (ru) | 2017-01-10 |
Family
ID=47501255
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2014130284A RU2607741C2 (ru) | 2011-12-23 | 2012-12-19 | Новый способ получения диоксидов кремния |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US9550682B2 (enExample) |
| EP (1) | EP2794479B1 (enExample) |
| JP (1) | JP5868520B2 (enExample) |
| KR (1) | KR20140111297A (enExample) |
| CN (1) | CN104136371B (enExample) |
| AU (1) | AU2012357112A1 (enExample) |
| BR (1) | BR112014015235B1 (enExample) |
| CA (1) | CA2859570C (enExample) |
| IN (1) | IN2014CN04607A (enExample) |
| MX (1) | MX356674B (enExample) |
| MY (1) | MY180098A (enExample) |
| RU (1) | RU2607741C2 (enExample) |
| TW (1) | TWI498284B (enExample) |
| WO (1) | WO2013092745A1 (enExample) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2984870B1 (fr) | 2011-12-23 | 2014-03-21 | Rhodia Operations | Nouveau procede de preparation de silices precipitees. |
| FR2985993B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985992B1 (fr) | 2012-01-25 | 2015-03-06 | Rhodia Operations | Nouveau procede de preparation de silices precitees |
| FR2985990B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres |
| FR2985991B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR3017610B1 (fr) * | 2014-02-14 | 2016-03-18 | Rhodia Operations | Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres |
| FR3017609B1 (fr) | 2014-02-14 | 2016-03-18 | Rhodia Operations | Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres |
| FR3018070B1 (fr) * | 2014-02-28 | 2017-09-15 | Rhodia Operations | Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres |
| PL3619165T3 (pl) | 2017-05-05 | 2025-06-09 | Rhodia Operations | Krzemionka strącona i sposób jej wytwarzania |
| US11554963B2 (en) | 2017-05-05 | 2023-01-17 | Rhodia Operations | Precipitated silica and process for its manufacture |
| CN112996750B (zh) * | 2018-11-08 | 2025-10-28 | 罗地亚经营管理公司 | 沉淀二氧化硅及其制造方法 |
| US12134564B2 (en) | 2018-11-08 | 2024-11-05 | Rhodia Operations | Precipitated silica and process for its manufacture |
| CN109607555B (zh) * | 2019-01-02 | 2019-08-09 | 广州市飞雪材料科技有限公司 | 一种高磨擦高透明牙膏用二氧化硅及其制备方法 |
| CN109480097B (zh) * | 2019-01-03 | 2022-02-01 | 山东联科科技股份有限公司 | 一种酸化剂载体用二氧化硅微球的制备方法 |
| JP2024540049A (ja) | 2021-10-26 | 2024-10-31 | エボニック オペレーションズ ゲーエムベーハー | 沈降シリカ、その製造方法およびその使用 |
| WO2023118281A1 (en) * | 2021-12-23 | 2023-06-29 | Rhodia Operations | Precipitated silica and process for its manufacture |
| CN115571886B (zh) * | 2022-10-14 | 2023-12-05 | 福建正盛无机材料股份有限公司 | 一种低吸油、低比表面积二氧化硅的制备方法 |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1506330A (fr) * | 1966-05-24 | 1967-12-22 | Fr Des Silicates Speciaux Sifr | Perfectionnements apportés aux procédés de fabrication de silice et produits obtenus par ces procédés |
| EP0520862A1 (fr) * | 1991-06-26 | 1992-12-30 | Rhone-Poulenc Chimie | Procédé de préparation de silice précipitée, silices précipitées obtenues et leur utilisation au renforcement des élastomères |
| EP0754650A1 (de) * | 1995-07-20 | 1997-01-22 | Degussa Ag | Fällungskieselsäure |
| RU2179153C1 (ru) * | 2000-06-07 | 2002-02-10 | Закрытое акционерное общество "Хорс" | Способ получения диоксида кремния |
| WO2003016215A1 (fr) * | 2001-08-13 | 2003-02-27 | Rhodia Chimie | Procede de preparation de silices, silices a distribution granulometrique et/ou repartition poreuse particulieres et leurs utilisations, notamment pour le renforcement de polymeres |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3114493A1 (de) * | 1981-04-10 | 1982-10-28 | Degussa Ag, 6000 Frankfurt | "faellungskieselsaeuren und verfahren zu ihrer herstellung" |
| DE3639845A1 (de) * | 1986-11-21 | 1988-06-01 | Degussa | Faellungskieselsaeuren, verfahren zu ihrer herstellung und verwendung |
| WO2002030818A2 (en) * | 2000-10-13 | 2002-04-18 | University Of Cincinnati | Methods for synthesizing precipitated silica and use thereof |
| DE10112441A1 (de) * | 2001-03-15 | 2002-09-19 | Degussa | Kieselsäure durch Fällung mit konstanter Alkalizahl und deren Verwendung |
| CN102137813A (zh) * | 2008-09-01 | 2011-07-27 | 赢创德固赛有限责任公司 | 制备沉淀二氧化硅的方法、沉淀二氧化硅及其用途 |
| FR2949454B1 (fr) * | 2009-09-03 | 2011-09-16 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2984870B1 (fr) | 2011-12-23 | 2014-03-21 | Rhodia Operations | Nouveau procede de preparation de silices precipitees. |
| FR2985992B1 (fr) | 2012-01-25 | 2015-03-06 | Rhodia Operations | Nouveau procede de preparation de silices precitees |
| FR2985993B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985991B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985990B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres |
-
2012
- 2012-12-19 MX MX2014007591A patent/MX356674B/es active IP Right Grant
- 2012-12-19 BR BR112014015235-7A patent/BR112014015235B1/pt not_active IP Right Cessation
- 2012-12-19 MY MYPI2014701701A patent/MY180098A/en unknown
- 2012-12-19 CN CN201280070513.9A patent/CN104136371B/zh not_active Expired - Fee Related
- 2012-12-19 US US14/367,455 patent/US9550682B2/en not_active Expired - Fee Related
- 2012-12-19 WO PCT/EP2012/076206 patent/WO2013092745A1/fr not_active Ceased
- 2012-12-19 AU AU2012357112A patent/AU2012357112A1/en not_active Abandoned
- 2012-12-19 EP EP12809807.6A patent/EP2794479B1/fr active Active
- 2012-12-19 KR KR1020147020129A patent/KR20140111297A/ko not_active Abandoned
- 2012-12-19 JP JP2014547985A patent/JP5868520B2/ja not_active Expired - Fee Related
- 2012-12-19 RU RU2014130284A patent/RU2607741C2/ru not_active IP Right Cessation
- 2012-12-19 CA CA2859570A patent/CA2859570C/fr not_active Expired - Fee Related
- 2012-12-19 IN IN4607CHN2014 patent/IN2014CN04607A/en unknown
- 2012-12-22 TW TW101149380A patent/TWI498284B/zh not_active IP Right Cessation
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1506330A (fr) * | 1966-05-24 | 1967-12-22 | Fr Des Silicates Speciaux Sifr | Perfectionnements apportés aux procédés de fabrication de silice et produits obtenus par ces procédés |
| EP0520862A1 (fr) * | 1991-06-26 | 1992-12-30 | Rhone-Poulenc Chimie | Procédé de préparation de silice précipitée, silices précipitées obtenues et leur utilisation au renforcement des élastomères |
| EP0754650A1 (de) * | 1995-07-20 | 1997-01-22 | Degussa Ag | Fällungskieselsäure |
| RU2179153C1 (ru) * | 2000-06-07 | 2002-02-10 | Закрытое акционерное общество "Хорс" | Способ получения диоксида кремния |
| WO2003016215A1 (fr) * | 2001-08-13 | 2003-02-27 | Rhodia Chimie | Procede de preparation de silices, silices a distribution granulometrique et/ou repartition poreuse particulieres et leurs utilisations, notamment pour le renforcement de polymeres |
Non-Patent Citations (3)
| Title |
|---|
| ВОЛКОВ А.И. и др., Большой химический справочник, Минск, Современная школа, 2005, с.391, таблица 10, с.392, таблица 11. ГОСТ 5848-73, Кислота муравьиная, дата введения 01.07.1974. * |
| ГРОШЕВА Л.П., Растворы. Расчет составов. Разбавление, смешение, концентрирование растворов. Расчет состава и характеристик твердых материалов. Методическое пособие, Новгородский государственный университет, Великий Новгород, 2006, с.7. * |
| ГРОШЕВА Л.П., Растворы. Расчет составов. Разбавление, смешение, концентрирование растворов. Расчет состава и характеристик твердых материалов. Методическое пособие, Новгородский государственный университет, Великий Новгород, 2006, с.7. ВОЛКОВ А.И. и др., Большой химический справочник, Минск, Современная школа, 2005, с.391, таблица 10, с.392, таблица 11. ГОСТ 5848-73, Кислота муравьиная, дата введения 01.07.1974. * |
Also Published As
| Publication number | Publication date |
|---|---|
| BR112014015235B1 (pt) | 2020-12-08 |
| CA2859570A1 (fr) | 2013-06-27 |
| CA2859570C (fr) | 2016-10-18 |
| BR112014015235A8 (pt) | 2017-06-13 |
| MX2014007591A (es) | 2015-03-19 |
| MY180098A (en) | 2020-11-22 |
| RU2014130284A (ru) | 2016-02-10 |
| CN104136371A (zh) | 2014-11-05 |
| AU2012357112A1 (en) | 2014-07-10 |
| US20150266742A1 (en) | 2015-09-24 |
| MX356674B (es) | 2018-06-08 |
| JP2015506327A (ja) | 2015-03-02 |
| TWI498284B (zh) | 2015-09-01 |
| WO2013092745A1 (fr) | 2013-06-27 |
| TW201339095A (zh) | 2013-10-01 |
| IN2014CN04607A (enExample) | 2015-09-18 |
| EP2794479A1 (fr) | 2014-10-29 |
| CN104136371B (zh) | 2017-03-15 |
| KR20140111297A (ko) | 2014-09-18 |
| EP2794479B1 (fr) | 2020-04-08 |
| BR112014015235A2 (pt) | 2017-06-13 |
| JP5868520B2 (ja) | 2016-02-24 |
| US9550682B2 (en) | 2017-01-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20191220 |