MX356674B - Proceso novedoso para preparar sílices. - Google Patents
Proceso novedoso para preparar sílices.Info
- Publication number
- MX356674B MX356674B MX2014007591A MX2014007591A MX356674B MX 356674 B MX356674 B MX 356674B MX 2014007591 A MX2014007591 A MX 2014007591A MX 2014007591 A MX2014007591 A MX 2014007591A MX 356674 B MX356674 B MX 356674B
- Authority
- MX
- Mexico
- Prior art keywords
- acid
- concentration
- production method
- precipitated
- silica production
- Prior art date
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000000377 silicon dioxide Substances 0.000 title abstract 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 abstract 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 abstract 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- 235000019253 formic acid Nutrition 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/126—Preparation of silica of undetermined type
- C01B33/128—Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
- C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Paper (AREA)
Abstract
La invención se refiere a proceso novedoso para preparar sílices, que comprende la reacción de un silicato con al menos un ácido, donde el ácido utilizado en al menos uno de sus pasos es un ácido concentrado.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1104089A FR2984871B1 (fr) | 2011-12-23 | 2011-12-23 | Nouveau procede de preparation de silices |
| FR1200217A FR2985994B1 (fr) | 2012-01-25 | 2012-01-25 | Nouveaux procede de preparation de silices precipitees |
| PCT/EP2012/076206 WO2013092745A1 (fr) | 2011-12-23 | 2012-12-19 | Procede de preparation de silices precipitees |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2014007591A MX2014007591A (es) | 2015-03-19 |
| MX356674B true MX356674B (es) | 2018-06-08 |
Family
ID=47501255
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014007591A MX356674B (es) | 2011-12-23 | 2012-12-19 | Proceso novedoso para preparar sílices. |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US9550682B2 (es) |
| EP (1) | EP2794479B1 (es) |
| JP (1) | JP5868520B2 (es) |
| KR (1) | KR20140111297A (es) |
| CN (1) | CN104136371B (es) |
| AU (1) | AU2012357112A1 (es) |
| BR (1) | BR112014015235B1 (es) |
| CA (1) | CA2859570C (es) |
| IN (1) | IN2014CN04607A (es) |
| MX (1) | MX356674B (es) |
| MY (1) | MY180098A (es) |
| RU (1) | RU2607741C2 (es) |
| TW (1) | TWI498284B (es) |
| WO (1) | WO2013092745A1 (es) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2984870B1 (fr) | 2011-12-23 | 2014-03-21 | Rhodia Operations | Nouveau procede de preparation de silices precipitees. |
| FR2985992B1 (fr) | 2012-01-25 | 2015-03-06 | Rhodia Operations | Nouveau procede de preparation de silices precitees |
| FR2985990B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres |
| FR2985993B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985991B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR3017609B1 (fr) * | 2014-02-14 | 2016-03-18 | Rhodia Operations | Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres |
| FR3017610B1 (fr) * | 2014-02-14 | 2016-03-18 | Rhodia Operations | Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres |
| FR3018070B1 (fr) * | 2014-02-28 | 2017-09-15 | Rhodia Operations | Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres |
| WO2018202756A1 (en) * | 2017-05-05 | 2018-11-08 | Rhodia Operations | Precipitated silica and process for its manufacture |
| EP3619164B1 (en) * | 2017-05-05 | 2024-11-27 | Rhodia Operations | Precipitated silica and process for its manufacture |
| CN119873845A (zh) | 2018-11-08 | 2025-04-25 | 罗地亚经营管理公司 | 沉淀二氧化硅及其制造方法 |
| KR102819122B1 (ko) * | 2018-11-08 | 2025-06-12 | 로디아 오퍼레이션스 | 침전 실리카 및 이의 제조 방법 |
| CN109607555B (zh) * | 2019-01-02 | 2019-08-09 | 广州市飞雪材料科技有限公司 | 一种高磨擦高透明牙膏用二氧化硅及其制备方法 |
| CN109480097B (zh) * | 2019-01-03 | 2022-02-01 | 山东联科科技股份有限公司 | 一种酸化剂载体用二氧化硅微球的制备方法 |
| CA3235727A1 (en) | 2021-10-26 | 2023-05-04 | Evonik Operations Gmbh | Precipitated silica, process for production thereof and use thereof |
| CN118742514A (zh) * | 2021-12-23 | 2024-10-01 | 罗地亚经营管理公司 | 沉淀二氧化硅及其制造方法 |
| CN115571886B (zh) * | 2022-10-14 | 2023-12-05 | 福建正盛无机材料股份有限公司 | 一种低吸油、低比表面积二氧化硅的制备方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1506330A (fr) | 1966-05-24 | 1967-12-22 | Fr Des Silicates Speciaux Sifr | Perfectionnements apportés aux procédés de fabrication de silice et produits obtenus par ces procédés |
| DE3114493A1 (de) * | 1981-04-10 | 1982-10-28 | Degussa Ag, 6000 Frankfurt | "faellungskieselsaeuren und verfahren zu ihrer herstellung" |
| DE3639845A1 (de) * | 1986-11-21 | 1988-06-01 | Degussa | Faellungskieselsaeuren, verfahren zu ihrer herstellung und verwendung |
| FR2678259B1 (fr) | 1991-06-26 | 1993-11-05 | Rhone Poulenc Chimie | Nouvelles silices precipitees sous forme de granules ou de poudres, procedes de synthese et utilisation au renforcement des elastomeres. |
| DE19526476A1 (de) | 1995-07-20 | 1997-01-23 | Degussa | Fällungskieselsäure |
| RU2179153C1 (ru) * | 2000-06-07 | 2002-02-10 | Закрытое акционерное общество "Хорс" | Способ получения диоксида кремния |
| EP1324947A2 (en) * | 2000-10-13 | 2003-07-09 | University of Cincinnati | Methods for synthesizing precipitated silica and use thereof |
| DE10112441A1 (de) * | 2001-03-15 | 2002-09-19 | Degussa | Kieselsäure durch Fällung mit konstanter Alkalizahl und deren Verwendung |
| PT1419106T (pt) * | 2001-08-13 | 2016-12-27 | Rhodia Chimie Sa | Processo de preparação de sílicas, sílicas com distribuição granulométrica e/ou repartição porosa específicas e suas utilizações, em particular no reforço de polímeros |
| WO2010022544A1 (en) * | 2008-09-01 | 2010-03-04 | Evonik Degussa Gmbh | Process for preparing precipitated silicas, precipitated silicas and their use |
| FR2949454B1 (fr) * | 2009-09-03 | 2011-09-16 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2984870B1 (fr) | 2011-12-23 | 2014-03-21 | Rhodia Operations | Nouveau procede de preparation de silices precipitees. |
| FR2985991B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985993B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985990B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres |
| FR2985992B1 (fr) | 2012-01-25 | 2015-03-06 | Rhodia Operations | Nouveau procede de preparation de silices precitees |
-
2012
- 2012-12-19 CA CA2859570A patent/CA2859570C/fr not_active Expired - Fee Related
- 2012-12-19 EP EP12809807.6A patent/EP2794479B1/fr active Active
- 2012-12-19 BR BR112014015235-7A patent/BR112014015235B1/pt not_active IP Right Cessation
- 2012-12-19 MX MX2014007591A patent/MX356674B/es active IP Right Grant
- 2012-12-19 JP JP2014547985A patent/JP5868520B2/ja not_active Expired - Fee Related
- 2012-12-19 CN CN201280070513.9A patent/CN104136371B/zh not_active Expired - Fee Related
- 2012-12-19 KR KR1020147020129A patent/KR20140111297A/ko not_active Abandoned
- 2012-12-19 US US14/367,455 patent/US9550682B2/en not_active Expired - Fee Related
- 2012-12-19 WO PCT/EP2012/076206 patent/WO2013092745A1/fr not_active Ceased
- 2012-12-19 AU AU2012357112A patent/AU2012357112A1/en not_active Abandoned
- 2012-12-19 IN IN4607CHN2014 patent/IN2014CN04607A/en unknown
- 2012-12-19 RU RU2014130284A patent/RU2607741C2/ru not_active IP Right Cessation
- 2012-12-19 MY MYPI2014701701A patent/MY180098A/en unknown
- 2012-12-22 TW TW101149380A patent/TWI498284B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| AU2012357112A1 (en) | 2014-07-10 |
| MY180098A (en) | 2020-11-22 |
| KR20140111297A (ko) | 2014-09-18 |
| JP5868520B2 (ja) | 2016-02-24 |
| BR112014015235A8 (pt) | 2017-06-13 |
| EP2794479A1 (fr) | 2014-10-29 |
| WO2013092745A1 (fr) | 2013-06-27 |
| TW201339095A (zh) | 2013-10-01 |
| CA2859570A1 (fr) | 2013-06-27 |
| RU2014130284A (ru) | 2016-02-10 |
| CN104136371B (zh) | 2017-03-15 |
| US9550682B2 (en) | 2017-01-24 |
| CA2859570C (fr) | 2016-10-18 |
| US20150266742A1 (en) | 2015-09-24 |
| BR112014015235A2 (pt) | 2017-06-13 |
| CN104136371A (zh) | 2014-11-05 |
| TWI498284B (zh) | 2015-09-01 |
| EP2794479B1 (fr) | 2020-04-08 |
| IN2014CN04607A (es) | 2015-09-18 |
| BR112014015235B1 (pt) | 2020-12-08 |
| JP2015506327A (ja) | 2015-03-02 |
| MX2014007591A (es) | 2015-03-19 |
| RU2607741C2 (ru) | 2017-01-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |